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1 Laboratory Directors: Mark J. DeMeo, M.D.; Richard R. Wilber, M.D. Identification: 104 DOB: Sex: Account #: Requisition #: Collected by: DR. SHAWN JENNINGS Accession #: Collected: Received: Reported: 06/18/ /22/2016 9:49 AM 06/24/2016 5:15 PM Specimen Type: Urine Final Result Summary None Detected; none of the analytes tested were detected. Client: Ultimate Fitness Events - USA 600 Golden Gate St Lake Orion, MI Phone: (248) Tests Ordered Anabolic Steroids and Agents Drug Result Drug Tests Screen Confirmation Method Cutoff Method Cutoff Anabolic Steroids and Agents 1-Androstendiol, 1-Androstendione or 1-Testosterone 4-Hydroxytestosterone, Formestane &/or 6a-Methylandrostendione metabolite Androstendiol, Androstendione or GC/MS 6 T/E Ratio Testosterone (T/E Ratio) Bolasterone metabolite Boldenone Calusterone Clenbuterol (anabolic agent) GC/MS 1 ng/ml Clostebol Danazol Dehydrochlormethyltestosterone Desoxymethyltestosterone Drostanolone &/or metabolites Epitestosterone (masking agent) GC/MS 200 ng/ml Estra-4,9-dien-3,17-dione Fluoxymesterone Formebolone Furazabol metabolite Halodrol metabolite Mestanolone metabolite Mesterolone Methandriol Methandrostenolone Methasterone &/or metabolite Methenolone &/or Methyl-1-testosterone &/or Methyltestosterone Mibolerone metatabolite Nandrolone, 19-Norandrostenedione or 19-Norandrost Norclostebol Norethandrolone Oxabolone &/or Page 1 of 2 Printed 6/26/2016 5:07 AM ST14

2 Oxandrolone &/or metabolite Oxymesterone Oxymetholone Probenecid (masking agent) GC/MS 100 ng/ml Prostanozol Stanozolol Stenbolone &/or Testolactone (anti-estrogen) metabolite Trenbolone metabolite GC/MS 10 ng/ml Laboratory Directors: Mark J. DeMeo, M.D.; Richard R. Wilber, M.D. Comments: Analytical testing has been performed in accordance to all Redwood Toxicology Laboratory standard operating procedures and final results have been reviewed by laboratory certifying scientists. Director of Sports Testing: Victor Uralets, Ph.D. Method Index EA - Enzyme Assay EIA - Enzyme-Immunoassay ELISA - Enzyme-Linked Immunosorbent Assay RIA - Radio-Immunoassay TLC - Thin Layer Chromatography GC-FID - Gas Chromatography - Flame Ionization Detector GC/MS - Gas Chromatography / Mass Spectrometry LC/MS/MS - Liquid Chromatography Tandem Mass Spectrometry Specimens are disposed of as follows: Negatives - after two days; Positives - after three months. Page 2 of 2 Printed 6/26/2016 5:07 AM ST14

3 Laboratory Directors: Mark J. DeMeo, M.D.; Richard R. Wilber, M.D. Identification: 400 DOB: Sex: Account #: Requisition #: Collected by: DR. SHAWN JENNINGS Accession #: Collected: Received: Reported: 06/18/ /22/2016 9:49 AM 06/24/2016 5:15 PM Specimen Type: Urine Final Result Summary None Detected; none of the analytes tested were detected. Client: Ultimate Fitness Events - USA 600 Golden Gate St Lake Orion, MI Phone: (248) Tests Ordered Anabolic Steroids and Agents Drug Result Drug Tests Screen Confirmation Method Cutoff Method Cutoff Anabolic Steroids and Agents 1-Androstendiol, 1-Androstendione or 1-Testosterone 4-Hydroxytestosterone, Formestane &/or 6a-Methylandrostendione metabolite Androstendiol, Androstendione or GC/MS 6 T/E Ratio Testosterone (T/E Ratio) Bolasterone metabolite Boldenone Calusterone Clenbuterol (anabolic agent) GC/MS 1 ng/ml Clostebol Danazol Dehydrochlormethyltestosterone Desoxymethyltestosterone Drostanolone &/or metabolites Epitestosterone (masking agent) GC/MS 200 ng/ml Estra-4,9-dien-3,17-dione Fluoxymesterone Formebolone Furazabol metabolite Halodrol metabolite Mestanolone metabolite Mesterolone Methandriol Methandrostenolone Methasterone &/or metabolite Methenolone &/or Methyl-1-testosterone &/or Methyltestosterone Mibolerone metatabolite Nandrolone, 19-Norandrostenedione or 19-Norandrost Norclostebol Norethandrolone Oxabolone &/or Page 1 of 2 Printed 6/26/2016 5:07 AM ST15

4 Oxandrolone &/or metabolite Oxymesterone Oxymetholone Probenecid (masking agent) GC/MS 100 ng/ml Prostanozol Stanozolol Stenbolone &/or Testolactone (anti-estrogen) metabolite Trenbolone metabolite GC/MS 10 ng/ml Laboratory Directors: Mark J. DeMeo, M.D.; Richard R. Wilber, M.D. Comments: Analytical testing has been performed in accordance to all Redwood Toxicology Laboratory standard operating procedures and final results have been reviewed by laboratory certifying scientists. Director of Sports Testing: Victor Uralets, Ph.D. Method Index EA - Enzyme Assay EIA - Enzyme-Immunoassay ELISA - Enzyme-Linked Immunosorbent Assay RIA - Radio-Immunoassay TLC - Thin Layer Chromatography GC-FID - Gas Chromatography - Flame Ionization Detector GC/MS - Gas Chromatography / Mass Spectrometry LC/MS/MS - Liquid Chromatography Tandem Mass Spectrometry Specimens are disposed of as follows: Negatives - after two days; Positives - after three months. Page 2 of 2 Printed 6/26/2016 5:07 AM ST15

5 Laboratory Directors: Mark J. DeMeo, M.D.; Richard R. Wilber, M.D. Identification: 709 DOB: Sex: Account #: Requisition #: Collected by: DR. SHAWN JENNINGS Accession #: Collected: Received: Reported: 06/18/ /22/2016 9:50 AM 06/24/2016 5:15 PM Specimen Type: Urine Final Result Summary None Detected; none of the analytes tested were detected. Client: Ultimate Fitness Events - USA 600 Golden Gate St Lake Orion, MI Phone: (248) Tests Ordered Anabolic Steroids and Agents Drug Result Drug Tests Screen Confirmation Method Cutoff Method Cutoff Anabolic Steroids and Agents 1-Androstendiol, 1-Androstendione or 1-Testosterone 4-Hydroxytestosterone, Formestane &/or 6a-Methylandrostendione metabolite Androstendiol, Androstendione or GC/MS 6 T/E Ratio Testosterone (T/E Ratio) Bolasterone metabolite Boldenone Calusterone Clenbuterol (anabolic agent) GC/MS 1 ng/ml Clostebol Danazol Dehydrochlormethyltestosterone Desoxymethyltestosterone Drostanolone &/or metabolites Epitestosterone (masking agent) GC/MS 200 ng/ml Estra-4,9-dien-3,17-dione Fluoxymesterone Formebolone Furazabol metabolite Halodrol metabolite Mestanolone metabolite Mesterolone Methandriol Methandrostenolone Methasterone &/or metabolite Methenolone &/or Methyl-1-testosterone &/or Methyltestosterone Mibolerone metatabolite Nandrolone, 19-Norandrostenedione or 19-Norandrost Norclostebol Norethandrolone Oxabolone &/or Page 1 of 2 Printed 6/26/2016 5:04 AM ST16

6 Oxandrolone &/or metabolite Oxymesterone Oxymetholone Probenecid (masking agent) GC/MS 100 ng/ml Prostanozol Stanozolol Stenbolone &/or Testolactone (anti-estrogen) metabolite Trenbolone metabolite GC/MS 10 ng/ml Laboratory Directors: Mark J. DeMeo, M.D.; Richard R. Wilber, M.D. Comments: Analytical testing has been performed in accordance to all Redwood Toxicology Laboratory standard operating procedures and final results have been reviewed by laboratory certifying scientists. Director of Sports Testing: Victor Uralets, Ph.D. Method Index EA - Enzyme Assay EIA - Enzyme-Immunoassay ELISA - Enzyme-Linked Immunosorbent Assay RIA - Radio-Immunoassay TLC - Thin Layer Chromatography GC-FID - Gas Chromatography - Flame Ionization Detector GC/MS - Gas Chromatography / Mass Spectrometry LC/MS/MS - Liquid Chromatography Tandem Mass Spectrometry Specimens are disposed of as follows: Negatives - after two days; Positives - after three months. Page 2 of 2 Printed 6/26/2016 5:04 AM ST16

7 Laboratory Directors: Mark J. DeMeo, M.D.; Richard R. Wilber, M.D. Identification: 802 DOB: Sex: Account #: Requisition #: Collected by: DR. SHAWN JENNINGS Accession #: Collected: Received: Reported: 06/18/ /22/2016 9:50 AM 06/24/2016 5:15 PM Specimen Type: Urine Final Result Summary None Detected; none of the analytes tested were detected. Client: Ultimate Fitness Events - USA 600 Golden Gate St Lake Orion, MI Phone: (248) Tests Ordered Anabolic Steroids and Agents Drug Result Drug Tests Screen Confirmation Method Cutoff Method Cutoff Anabolic Steroids and Agents 1-Androstendiol, 1-Androstendione or 1-Testosterone 4-Hydroxytestosterone, Formestane &/or 6a-Methylandrostendione metabolite Androstendiol, Androstendione or GC/MS 6 T/E Ratio Testosterone (T/E Ratio) Bolasterone metabolite Boldenone Calusterone Clenbuterol (anabolic agent) GC/MS 1 ng/ml Clostebol Danazol Dehydrochlormethyltestosterone Desoxymethyltestosterone Drostanolone &/or metabolites Epitestosterone (masking agent) GC/MS 200 ng/ml Estra-4,9-dien-3,17-dione Fluoxymesterone Formebolone Furazabol metabolite Halodrol metabolite Mestanolone metabolite Mesterolone Methandriol Methandrostenolone Methasterone &/or metabolite Methenolone &/or Methyl-1-testosterone &/or Methyltestosterone Mibolerone metatabolite Nandrolone, 19-Norandrostenedione or 19-Norandrost Norclostebol Norethandrolone Oxabolone &/or Page 1 of 2 Printed 6/26/2016 5:03 AM ST17

8 Oxandrolone &/or metabolite Oxymesterone Oxymetholone Probenecid (masking agent) GC/MS 100 ng/ml Prostanozol Stanozolol Stenbolone &/or Testolactone (anti-estrogen) metabolite Trenbolone metabolite GC/MS 10 ng/ml Laboratory Directors: Mark J. DeMeo, M.D.; Richard R. Wilber, M.D. Comments: Analytical testing has been performed in accordance to all Redwood Toxicology Laboratory standard operating procedures and final results have been reviewed by laboratory certifying scientists. Director of Sports Testing: Victor Uralets, Ph.D. Method Index EA - Enzyme Assay EIA - Enzyme-Immunoassay ELISA - Enzyme-Linked Immunosorbent Assay RIA - Radio-Immunoassay TLC - Thin Layer Chromatography GC-FID - Gas Chromatography - Flame Ionization Detector GC/MS - Gas Chromatography / Mass Spectrometry LC/MS/MS - Liquid Chromatography Tandem Mass Spectrometry Specimens are disposed of as follows: Negatives - after two days; Positives - after three months. Page 2 of 2 Printed 6/26/2016 5:03 AM ST17

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