Deuterium more than just for locking: Part II. H Topshim. Donna Baldisseri Boston Massachusetts Pre-ENC Workshops 2014, March 22

Size: px
Start display at page:

Download "Deuterium more than just for locking: Part II. H Topshim. Donna Baldisseri Boston Massachusetts Pre-ENC Workshops 2014, March 22"

Transcription

1 Deuterium more than just for locking: Part II 2 H Topshim Donna Baldisseri Boston Massachusetts Pre-ENC Workshops 2014, March 22

2 Topshim Fully automated Reliable Easy to use Customizable Good, rapid results M. Weiger, T. Speck, M. Fey Gradient shimming with spectrum optimisation JMR 182, (2006) 2

3 Using Topshim 1. Open data set 2. Lock for correct solvent with *lock Topshim automatically selects the desired shim method depending on the solvent 3. Start shimming *Lock parameters have been optimized, especially lock phase. 3

4 Using Topshim spectrum optimization M. Weiger, T. Speck, M. Fey Gradient shimming with spectrum optimisation JMR 182, (2006)

5 2 H Topshim 5

6 Advanced 2 H Topshim Useful parameters Customizing a new solvent Convection Compensation Topshim Tips 6

7 Useful Parameters Additional parameters: not checked checked 7

8 Useful Parameters Command line arguments can be added here when the box is checked 8

9 Useful Parameters ordmax= sets the maximum total order of shim functions (default = 5) ordmax=3 limits shimming to Z-Z3 (1mm and 1.7mm probes) topshim ordmax=8 (SmartProbe) 1H or 2H explicitly sets shimming nucleus lockoff enables shimming with system unlocked o1p= explicitly sets excitation frequency in PPM topshim 1H lockoff o1p=2.49 (DMSO-h6) selwid= enables selective excitation of a bandwidth expressed in PPM Useful when shimming on a solvent with multiple signals topshim o1p=1.93 selwid=0.5 (CD3CN+D2O) zrange sets the range in CM in the Z direction used for shimming topshim zrange=-0.8,0.8 (short sample) 9

10 Useful Parameters durmax= maximum duration per 1D field map acquisition rga force receiver gain optimization before shimming topshim ordmax=8 rga durmax=60 (CDCl3 in SmartProbe) tune* also shim on the lock before or after gradient shimming (tuneb shims X,Y,Z,XZ,YZ before running gradient shimming) topshim tuneaz (shims Z after running gradient shimming) shigemi used to eliminate unreliable data at axial Shigemi tube walls when 1D shimming calreset reset all calibration results for the current probe cal force the execution of all calibration procedures for the current probe; a water sample must be used plot saves data after completion in <TopSpin_home>/data/topshimData 10 read about more in the Topshim manual!

11 Advanced 2 H Topshim Useful parameters Customizing a new solvent Convection Compensation Topshim Tips 11

12 2 H Topshim adding a new solvent

13 New Solvent 2 H Shimming Mixed Solvent - (mixture of CD 3 CN and D2O) edsolv edlock 13

14 New Solvent 2 H Shimming

15 New Solvent 2 H Shimming

16 New Solvent 2 H Shimming CH3CN+D2O rg=2.8 CD3CN+D2O rg=16 * * +WET

17 Advanced 2 H Topshim Useful parameters Customizing a new solvent Convection Compensation Topshim Tips 17

18 2 H Topshim convection compensation Convection from temperature gradients Raising temperature + filling height too high = problems 18

19 2 H Topshim convection compensation Sample temperature After changing the sample you need to wait for a sufficiently long time (e.g. 60 to 120 sec) to allow the sample to reach a stable temperature, depending on the difference of the room and the sample target temperature. Otherwise a shim setting optimal at the initial temperature may not be appropriate at a later stage. Furthermore, operating close to the boiling point of a sample should be avoided as this may cause serious signal loss during the shimming acquisition due to convection. The latter problem can also be associated with temperature gradients in the probe. Finally, you should always make sure that the gas flow is set correctly as specified for your probe. Topshim manual, pg. 21

20 2 H Topshim convection compensation In order to eliminate / reduce convection: Sample filling height =< 40 mm Increase VT gas flow (if possible) Spin sample (if possible) Lower sample temperature (if possible) Use solvent with higher viscosity (if possible) Use Shigemi or smaller sample diameter

21 2 H Topshim convection compensation The convcomp parameter sets a flag for Topshim to use convection compensation. imgegpcv1d, imgegpcvsp1d2h (gradshim pulse programs) (Topspin versions > TS2.1PL5)

22 2 H Topshim convection compensation α d15 Z G d ppm 1 H α TE 2 d15 2 TE 2 d15 2 B 0,ω 0 G d ppm

23 2 H Topshim convection compensation Convection scenario: lineshape sample (0.3% CHCl 3 in Acetone-d 6 ) 62 mm filling height (40mm for 5mm probe) R.T. 40 C (ca. 10sec) (>60sec) 400 l/hr (CryoProbe) (670 l/hr for 5mm CP) no convcomp with convcomp

24 2 H Topshim convection compensation Topshim manual in Topspin, pg. 38: mm probes Samples with a large diameter are prone to convection in the sample which may hamper the gradient shimming procedure. Therefore, it is advantageous to perform 3D shimming on a sample which has a higher viscosity than H2O. A very good candidate is the Bruker standard sample ASTM constisting of 40% p-dioxane in 60% C6D6. With this sample field mapping is performed on the 1H peak at ppm which is achieved with the following command: topshim 3d 1h o1p=3.475 Alternatively, the already provided parameter file can be used topshim 3d astm See also for a detailed description of the parameters.

25 Advanced 2 H Topshim Useful parameters Customizing a new solvent Convection Compensation Topshim Tips 25

26 Topshim Tips Check 2 H pulse length Poor initial B 0 homogeneity Shims can be too bad for Topshim to get data good enough to use for the calculation. Try running topshim with sample spinning. Try topshim tuneb to improve initial homogeneity. S/N too low Try running topshim durmax=30, 60, or even 120 Examine Topshim data topshim plot 26

27 Topshim Tips fmc Fid #1 is acquired with a longer echo time than fid #2. Using multiple display, profiles should have similar intensity. If long echo time spectrum is <0.5 then there may be homogeneity issues, which can be addressed with: topshim tuneb topshim 3d For 2 H, check pulse length.

28 Topshim Tips Errors and possible causes: no signal at all or no signal in centre Incorrect routing or RF cable not connected Protonated or incorrect lock solvent signal-to-noise is too low Incorrect 2 H pulse Insufficient lock solvent the (Z) gradient does not work Gradient cable not connected or gradient amplifier off too many points lost during fit Starting shims are too bad Convection And finally: *topshim plot (<Topspin_home)/data/topshimData) *topshim log (<Topspin_home>/prog/curdir/<user>) *Just send it to us (center@bruker.com)!

29 29

Shimming with VnmrJ 3.1 Software for Peak NMR Performance

Shimming with VnmrJ 3.1 Software for Peak NMR Performance Shimming with VnmrJ 3.1 Software for Peak NMR Performance Application Note Author Ron Crouch Agilent Technologies 13000 Weston Parkway Cary, NC 27513 USA Shimming is the term used to describe the process

More information

Pulsed-Field Gradient Shimming With VNMR

Pulsed-Field Gradient Shimming With VNMR PFG Shimming With VNMR Page 65 Pulsed-Field Gradient Shimming With VNMR cg fry: created 99.01.27 updated 99.02.01 I. General Discussion Pulsed-field gradients allow analytically accurate, automated adjustments

More information

Things to know before operating an NMR spectrometer André Boltjes, University of Groningen DD NMR Lab v

Things to know before operating an NMR spectrometer André Boltjes, University of Groningen DD NMR Lab v Things to know before operating an NMR spectrometer André Boltjes, University of Groningen DD NMR Lab v1.0 2013 I. A tour of an NMR lab. Figure 1 shows a picture of our Avance DRX 500. Although each NMR

More information

PINMRF Checkout Quiz - Bruker/TopSpin Version

PINMRF Checkout Quiz - Bruker/TopSpin Version PINMRF Checkout Quiz - Bruker/TopSpin Version Please carefully read every question and select the best answer(s). Some questions may have more than one correct answer. To receive full credit you must mark

More information

Variable Temperature Operation

Variable Temperature Operation Variable Temperature Operation AVIII 400 MHz Spectrometer November 11, 2012 The CBC NMR Laboratory University of Delaware AVIII 400 User Guide: Variable Temperature Operation 1 INTRODUCTION... 5 1.1 SAFETY...

More information

Fast 3D gradient shimming by only 2 2 pixels in XY plane for NMR-solution samples

Fast 3D gradient shimming by only 2 2 pixels in XY plane for NMR-solution samples Fast 3D gradient shimming by only 2 2 pixels in XY plane for NMR-solution samples Guangcao Liu, Xiaobo Qu, Shuhui Cai, Zhiyong Zhang, Zhiwei Chen, Congbo Cai, Zhong Chen Department of Electronic Science,

More information

User guide for the NMR spectrometer AVA300

User guide for the NMR spectrometer AVA300 1 User guide for the NMR spectrometer AVA300 Dear User! You are using a highly frequented NMR spectrometer, which has been installed in 2002. About 26000 spectra are measured here per year. Please respect

More information

DCIF Training Guide Variable Temperature Bruker B400 (last update )

DCIF Training Guide Variable Temperature Bruker B400 (last update ) DCIF Training Guide Variable Temperature Bruker B400 (last update 20100421) As with all of the other DCIF tutorials, the conventions used in this guide are as follows: Boldface type indicates commands

More information

NMR Service. How to Prepare Samples for NMR

NMR Service. How to Prepare Samples for NMR NMR Service How to Prepare Samples for NMR In NMR, unlike other types of spectroscopy, the quality of the sample has a profound effect on the quality of the resulting spectrum. If you follow a few simple

More information

User guide for the NMR spectrometer AVA400Stud

User guide for the NMR spectrometer AVA400Stud 1 User guide for the NMR spectrometer AVA400Stud Dear User! You are using a modern NMR spectrometer, which has been installed in 2009. About 12500 spectra are measured here per year. Please respect the

More information

Typically NMR Sample Configuration

Typically NMR Sample Configuration Typically NMR Sample Configuration = B o Solvent column ~ 3 as long as detection region. Copyright 003-014 UWChemMRF All Rights Reserved. Last updated Sept 15, 014. The following slides are useful as an

More information

Step By Step Instructions for VT Experiments on the Bruker 300 MHz Spectrometer

Step By Step Instructions for VT Experiments on the Bruker 300 MHz Spectrometer Step By Step Instructions for VT Experiments on the Bruker 300 MHz Spectrometer (1) Use the drop down menu to create a new experiment/dataset for acquiring the room temperature 1D spectrum. The name of

More information

Standard Operational Procedure for Capillary Electrophoresis

Standard Operational Procedure for Capillary Electrophoresis Page 1 of 14 Standard Operational Procedure for Capillary Electrophoresis *Please ask an experienced operator for training before you use the CE if you can. A demo is most probably more efficient than

More information

VT PLUS HF performance verification of Bunnell Life-Pulse HFJV (High Frequency Jet Ventilator)

VT PLUS HF performance verification of Bunnell Life-Pulse HFJV (High Frequency Jet Ventilator) VT PLUS HF performance verification of Bunnell Life-Pulse HFJV (High Frequency Jet Ventilator) VT PLUS HF provides a special mode for evaluating the performance of high frequency ventilators while connected

More information

BEST KNOWN METHODS. Transpector XPR3 Gas Analysis System. 1 of 6 DESCRIPTION XPR3 APPLICATIONS PHYSICAL INSTALLATION

BEST KNOWN METHODS. Transpector XPR3 Gas Analysis System. 1 of 6 DESCRIPTION XPR3 APPLICATIONS PHYSICAL INSTALLATION BEST KNOWN METHODS Transpector XPR3 Gas Analysis System DESCRIPTION The Transpector XPR3 is a third-generation, quadrupole-based residual gas analyzer that operates at PVD process pressures and is the

More information

9408 Series Dissolved Oxygen Systems. Dissolved oxygen systems designed for reliable operation with minimal operating costs

9408 Series Dissolved Oxygen Systems. Dissolved oxygen systems designed for reliable operation with minimal operating costs Data sheet DS/9408 EN Rev. M 9408 Series Dissolved oxygen systems designed for reliable operation with minimal operating costs Reduced sensor fouling design minimizes operational costs Low maintenance,

More information

Agilent Dimension Software for ELSD User Manual

Agilent Dimension Software for ELSD User Manual Agilent Dimension Software for ELSD User Manual Agilent Dimension Software for ELSD User Manual Agilent Technologies Notices Agilent Technologies, Inc. 2011 No part of this manual may be reproduced in

More information

Bruker BioSpin NMR CASE. System Requirements Manual. Version. NMR Spectroscopy. think forward

Bruker BioSpin NMR CASE. System Requirements Manual. Version. NMR Spectroscopy. think forward Bruker BioSpin NMR CASE System Requirements Manual Version 012 think forward NMR Spectroscopy Copyright by Bruker BioSpin NMR GmbH All rights reserved. No part of this publication may be reproduced, stored

More information

SHIMADZU LC-10/20 PUMP

SHIMADZU LC-10/20 PUMP SHIMADZU LC-10/20 PUMP Clarity Control Module ENG Code/Rev.: M091/70C Date: 24.10.2017 Phone: +420 251 013 400 DataApex Ltd. Fax: +420 251 013 401 Petrzilkova 2583/13 clarity@dataapex.com 158 00 Prague

More information

Adiabatic Compensation for Digiquartz Intelligent Transmitters

Adiabatic Compensation for Digiquartz Intelligent Transmitters Adiabatic Compensation for Digiquartz Intelligent Transmitters Paroscientific, Inc. 4500 148 th Ave. N.E. Redmond, WA 98052, USA Tel: (425) 883-8700 Fax: (425) 867-5407 www.paroscientific.com support@paroscientific.com

More information

VersaFlow Vortex 100 Vortex Flow Meter Technical Datasheet. Specification. The all-in-one solution. Highlights. Industries.

VersaFlow Vortex 100 Vortex Flow Meter Technical Datasheet. Specification. The all-in-one solution. Highlights. Industries. VersaFlow Vortex 100 Vortex Flow Meter Technical Datasheet 34-VF-03-05 September 3rd, 2008 Specification The all-in-one solution The VERSAFLOW is the only vortex flowmeter with integrated pressure and

More information

UsER manual for Watersens ph -REDOX

UsER manual for Watersens ph -REDOX UsER manual for Watersens -REDOX Cl 8 1 2 6 3 3 7 7 4 4 4 4 Parts List 1 Redox Probe 1 x 2 PH Probe 1 x 5 Tube Weight 2 x 6 Connection Valve 1 x chlorine 3 Chlorine and Pumps 2 x 7 Dosing Valve 2 x 5 5

More information

Hydro-Control V User Guide

Hydro-Control V User Guide Hydro-Control V User Guide Hydronix Part no: HD0193 Version 2.3.0 Revision date: July 2006 1 COPYRIGHT Neither the whole or any part of the information contained in nor the product described in this documentation

More information

Updated: Variable Temperature

Updated: Variable Temperature Updated: 2016-11-02 Variable Temperature Sample Preparation Make sure the probe is rated for the ultimate/final temperature Fully degas the sample, particularly if going to low temperature Be aware of

More information

An Advice about Shimming in High-Resolution Nuclear Magnetic Resonance

An Advice about Shimming in High-Resolution Nuclear Magnetic Resonance An Advice about Shimming in High-Resolution Nuclear Magnetic Resonance V.V Korostelev Kaliningrad University, Kaliningrad, Russia Abstract Three methods of active shimming in high-resolution NMR in existence

More information

Sensor for Air Bubble Detection at Liquid Filled Tubes. SONOCHECK Type ABD06.xx. Operating Manual

Sensor for Air Bubble Detection at Liquid Filled Tubes. SONOCHECK Type ABD06.xx. Operating Manual Sensor for Air Bubble Detection at Liquid Filled Tubes SONOCHECK Type ABD06.xx Operating Manual Manufacturer: Model: Type: SONOTEC Ultraschallsensorik Halle GmbH Air Bubble Detector ABD06.xx SONOTEC Ultraschallsensorik

More information

ABB MEASUREMENT & ANALYTICS DATA SHEET series Dissolved oxygen systems

ABB MEASUREMENT & ANALYTICS DATA SHEET series Dissolved oxygen systems ABB MEASUREMENT & ANALYTICS DATA SHEET 9408 series Dissolved oxygen systems Measurement made easy Dissolved oxygen systems designed for reliable operation with minimal operating costs Reduced sensor fouling

More information

Datasheet: K-30 ASCII Sensor

Datasheet: K-30 ASCII Sensor Datasheet: K-30 ASCII Sensor The K30 ASCII sensor is a low cost, infrared and maintenance free transmitter module intended to be built into different host devices that require CO2 monitoring data. The

More information

Technical Data Sheet MF010-O-LC

Technical Data Sheet MF010-O-LC Technical Data Sheet MF010-O-LC - 1 - 1. Properties The oxygen measuring system MF010-O-LC determines the oxygen content in gas mixtures up to a temperature of 250 C. It is particularly suitable for the

More information

AUTOMATIC VAPOR PRESSURE TESTER REID METHOD, DEMI SIZE MODEL AVP-30 INSTRUCTION MANUAL. Rev

AUTOMATIC VAPOR PRESSURE TESTER REID METHOD, DEMI SIZE MODEL AVP-30 INSTRUCTION MANUAL. Rev AUTOMATIC VAPOR PRESSURE TESTER REID METHOD, DEMI SIZE MODEL AVP-30 INSTRUCTION MANUAL Rev. 1.02 080314 TANAKA SCIENTIFIC LTD. TOKYO, JAPAN TABLE OF CONTENTS 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. INTRODUCTION

More information

BI-680 Online Dissolved Oxygen Controller Instruction Manual

BI-680 Online Dissolved Oxygen Controller Instruction Manual BI-680 Online Dissolved Oxygen Controller Instruction Manual BANTE INSTRUMENTS CO., LTD BI-680 Online Dissolved Oxygen Controller 1 Introduction Thank you for selecting the BI-680 online dissolved oxygen

More information

2600T Series Pressure Transmitters Plugged Impulse Line Detection Diagnostic. Pressure Measurement Engineered solutions for all applications

2600T Series Pressure Transmitters Plugged Impulse Line Detection Diagnostic. Pressure Measurement Engineered solutions for all applications Application Description AG/266PILD-EN Rev. C 2600T Series Pressure Transmitters Plugged Impulse Line Detection Diagnostic Pressure Measurement Engineered solutions for all applications Increase plant productivity

More information

PMI Pulse Decay Permeameter for Shale Rock Characterization Yang Yu, Scientist Porous Materials Inc., 20 Dutch Mill Road, Ithaca NY 14850

PMI Pulse Decay Permeameter for Shale Rock Characterization Yang Yu, Scientist Porous Materials Inc., 20 Dutch Mill Road, Ithaca NY 14850 PMI Pulse Decay Permeameter for Shale Rock Characterization Yang Yu, Scientist Porous Materials Inc., 20 Dutch Mill Road, Ithaca NY 14850 This document describes the application of Pulse Decay Permeameter

More information

Bante821 Portable Dissolved Oxygen Meter Instruction Manual

Bante821 Portable Dissolved Oxygen Meter Instruction Manual Bante821 Portable Dissolved Oxygen Meter Instruction Manual BANTE INSTRUMENTS CO., LTD Bante821 Portable Dissolved Oxygen Meter 1 Introduction Thank you for selecting the Bante821 portable dissolved oxygen

More information

Console Acceptance Tests & Specifications. MERCURYplus NMR Spectrometer Systems Pub. No , Rev. B0902

Console Acceptance Tests & Specifications. MERCURYplus NMR Spectrometer Systems Pub. No , Rev. B0902 Console Acceptance Tests & Specifications MERCURYplus NMR Spectrometer Systems Pub. No. 01-999186-00, Rev. B0902 Console Acceptance Tests & Specifications MERCURYplus NMR Spectrometer Systems Pub. No.

More information

Calibration Procedure

Calibration Procedure Management Procedure 2565 Revision: A Date Issued: October 30, 2017 Date Revised: Calibration Procedure DeFelsko Corporation PosiTector RTR-3D Replica Tape Reader Probe Table of Contents 1 Introduction

More information

Using Modbus Protocol with the ALTUS Net Oil Computer. Instruction Manual

Using Modbus Protocol with the ALTUS Net Oil Computer. Instruction Manual Using Modbus Protocol with the ALTUS Net Oil Computer Instruction Manual November 2000 Using Modbus Protocol with the ALTUS Net Oil Computer Instruction Manual November 2000 For technical assistance,

More information

DOscan10 Pocket Dissolved Oxygen Tester Instruction Manual

DOscan10 Pocket Dissolved Oxygen Tester Instruction Manual DOscan10 Pocket Dissolved Oxygen Tester Instruction Manual BANTE INSTRUMENTS CO., LTD DOscan10 Pocket Dissolved Oxygen Tester 1 Thank you for selecting the DOscan10 pocket dissolved oxygen tester. This

More information

Setting a New Standard in Flash Chromatography Performance

Setting a New Standard in Flash Chromatography Performance Setting a New Standard in Flash Chromatography Performance What s New Faster Flow rates, up to 300 ml/min Higher pressures, up to 300 psi (20 bar) Bigger touchscreen, 12 or 15 inches Wider Dynamic Range

More information

User manual CF8-D/W-IN

User manual CF8-D/W-IN User manual CF8-D/W-IN General The sensor CF8-D/W-IN is used to measure the carbon dioxide concentration inside incubators. All functions can be modified from a PC with the communication cable. UMA 48

More information

Triaxial automated systems

Triaxial automated systems Triaxial automated systems Pressure ranges: 0-1MPa (0-10 bar) 0-2MPa (0-20 bar) 0-3MPa (0-30 bar) 0-4MPa (0-40 bar) 0-5MPa (0-50 bar) Volume capacity: 230cc Interface: Touchscreen / USB connection (other

More information

Vortex flowmeters. Product family introduction Principle of operation Product review Applications Key product features

Vortex flowmeters. Product family introduction Principle of operation Product review Applications Key product features Vortex flowmeters introduction Product review s Key product features This document should not be duplicated, used, distributed, or disclosed for any purpose unless authorized by Siemens. Page 1 Vortex

More information

D-Opto. Dissolved Oxygen Sensor. Operation Manual (Software Version 1.0)

D-Opto. Dissolved Oxygen Sensor. Operation Manual (Software Version 1.0) D-Opto Dissolved Oxygen Sensor Operation Manual (Software Version 1.0) Table of contents 1 Introduction...3 1.1 Optical Sensor Technology...3 2 Software...4 2.1 Installation...4 2.2 Operation...4 3 Operation...9

More information

HOBO MX Water Level Logger (MX2001-0x) Manual

HOBO MX Water Level Logger (MX2001-0x) Manual HOBO MX Water Level Logger (MX2001-0x) Manual HOBO MX Water Level Logger Models: MX2001-01 or MX2001-01-Ti (Titanium), 9-meter/30-foot depth) MX2001-02, 30-meter/100-foot depth MX2001-03, 76-meter/250-foot

More information

Calculating Total Uncertainty of Temperature Calibration with a Dry Block. Calibration White Paper. Beamex.

Calculating Total Uncertainty of Temperature Calibration with a Dry Block. Calibration White Paper. Beamex. Beamex Calibration White Paper info@beamex.com Calculating Total Uncertainty of Temperature Calibration with a Dry Block World-class calibration solutions Calculating Total Uncertainty of Temperature Calibration

More information

SPECIFICATION FOR AN MRBR 9.4 TESLA/310MM/AS CRYO-COOLED MAGNET SYSTEM

SPECIFICATION FOR AN MRBR 9.4 TESLA/310MM/AS CRYO-COOLED MAGNET SYSTEM SPECIFICATION FOR AN MRBR 9.4 TESLA/310MM/AS CRYO-COOLED MAGNET SYSTEM Prepared by:- Magnex Scientific Limited The Magnet Technology Centre 6 Mead Road Oxford Industrial Park Yarnton, Oxford OX5 1QU, UK

More information

Improving the Measurement Accuracy of Water Partial Pressure Using the Major Constituent Analyzer

Improving the Measurement Accuracy of Water Partial Pressure Using the Major Constituent Analyzer Improving the Measurement Accuracy of Water Partial Pressure Using the Major Constituent Analyzer Ben D. Gardner, Phillip M. Erwin, Wai Tak Lee, Amber M. Tissandier, Souzan M. Thoresen Hamilton Sundstrand

More information

GCMSD-Headspace Analysis SOP

GCMSD-Headspace Analysis SOP Before you start GCMSD-Headspace Analysis SOP Method and Sequences names are restricted to 50 characters (MSD program will crash otherwise) The GC oven and Injection Ports need to be cooled to 50 oc to

More information

Thermal Profiling the Reflow Process

Thermal Profiling the Reflow Process Thermal Profiling the Reflow Process The Nomadics TCProfile system is a cost-effective instrument to measure the temperature characteristics of any process where the thermal profile is important to the

More information

D-Opto Dissolved Oxygen Sensor Operation Manual for the D-Opto 4-20mA

D-Opto Dissolved Oxygen Sensor Operation Manual for the D-Opto 4-20mA D-Opto Dissolved Oxygen Sensor Operation Manual for the D-Opto 4-20mA Software version 2.6 Table of contents 1 Introduction...3 1.1 Optical Sensor Technology...3 1.2 Installation...4 1.3 Operation...5

More information

Technical Bulletin, Communicating with Gas Chromatographs

Technical Bulletin, Communicating with Gas Chromatographs Last Updated: 13- July-2010 TB-080000C Technical Bulletin, Communicating with Gas Chromatographs OMNI FLOW COMPUTERS, INC. 12620 West Airport Boulevard, Suite 100 Sugar Land, Texas 77478 United States

More information

Manual for Using RES1b, the DCIF Instrumentation Reservation Software

Manual for Using RES1b, the DCIF Instrumentation Reservation Software Manual for Using RES1b, the DCIF Instrumentation Reservation Software NOTE: There is a new remote login procedure. The program will assign a new 6-digit user ID, use the 6-digit UID for reservations. Your

More information

Series Environmental Chambers

Series Environmental Chambers 3119-600 Series Environmental Chambers Challenges in Non-Ambient Testing Testing at non-ambient temperatures adds another layer of challenges to your testing laboratory. Ensuring you get accurate and stable

More information

RSKtools for Matlab processing RBR data

RSKtools for Matlab processing RBR data Table of Contents Introduction... 1 RSKtools help... 1 Getting set up... 1 Remove atmospheric pressure from measured total pressure... 2 Correct for A2D zero-order hold... 2 Low-pass filtering... 3 Alignment

More information

Three Columns Gas Chromatograph Analysis Using Correlation between Component's Molecular Weight and Its Response Factor

Three Columns Gas Chromatograph Analysis Using Correlation between Component's Molecular Weight and Its Response Factor Three Columns Gas Chromatograph Analysis Using Correlation between Component's Molecular Weight and Its Response Factor Anwar Sutan, Metco Services Ltd. Charles Johnson, Metco Services Ltd. Jason Laidlaw,

More information

6 Common Hydrodynamic Testing Mistakes

6 Common Hydrodynamic Testing Mistakes 6 Common Hydrodynamic Testing Mistakes Joe McMahen Many common mistakes made during hydrodynamic testing are easily avoided. Below are 6 Hydrodynamic Testing mistakes we see regularly along with guidance

More information

Drilling Efficiency Utilizing Coriolis Flow Technology

Drilling Efficiency Utilizing Coriolis Flow Technology Session 12: Drilling Efficiency Utilizing Coriolis Flow Technology Clement Cabanayan Emerson Process Management Abstract Continuous, accurate and reliable measurement of drilling fluid volumes and densities

More information

Bruker Sample Transport

Bruker Sample Transport Bruker BioSpin Bruker Sample Transport BST Installation and Technical Manual Version 002 think forward NMR Spectroscopy Copyright by Bruker BioSpin NMR GmbH All rights reserved. No part of this publication

More information

KEM Scientific, Inc. Instruments for Science from Scientists

KEM Scientific, Inc. Instruments for Science from Scientists KEM Scientific, Inc. Instruments for Science from Scientists J-KEM Scientific, Inc. 6970 Olive Blvd. St. Louis, MO 63130 (314) 863-5536 Fax (314) 863-6070 E-Mail: jkem911@jkem.com Precision Vacuum Controller,

More information

NanoSight NS300. NanoSight NS300. Operation instructions. Laser Spectroscopy Labs, UCI

NanoSight NS300. NanoSight NS300. Operation instructions. Laser Spectroscopy Labs, UCI NanoSight NS300 Operation instructions Injection/flushing brief overview: 1. Do not exceed flow of 1 ml per 20 seconds. 2. Inject two 1 ml syringes with nano-pure or DI water. 3. If the water does not

More information

INSTRUCTION MANUAL xbox One SPS-X3 VER 4.0

INSTRUCTION MANUAL xbox One SPS-X3 VER 4.0 INSTRUCTION MANUAL xbox One SPS-X3 VER 4.0 Congratulations, welcome to the GamerModz Family! You are now a proud owner of a GamerModz Custom Modded Controller. The SPS-X3 - VER 4.0 FOR XBOX ONE has been

More information

How to make my Air Glide S work properly

How to make my Air Glide S work properly How to make my Air Glide S work properly Originally written by Horst Rupp. Many thanks to Richard Frawley who edited and retranslated this article into proper English. 2014/11/21. The basic prerequisite

More information

no peaks missing peaks too small peaks increasing retention decreasing retention

no peaks missing peaks too small peaks increasing retention decreasing retention GC Troubleshooting We can help you. 1. Observation: no peaks no peaks missing peaks too small peaks increasing retention decreasing retention declining baseline rising baseline bleeding plateaus interfering

More information

FORMATION TESTER MOBILITY. Lachlan Finlayson, Chief Petrophysicist Petrofac Engineering & Production Services Engineering Services Consultancy

FORMATION TESTER MOBILITY. Lachlan Finlayson, Chief Petrophysicist Petrofac Engineering & Production Services Engineering Services Consultancy FORMATION TESTER MOBILITY Lachlan Finlayson, Chief Petrophysicist Petrofac Engineering & Production Services Engineering Services Consultancy 1 Introduction Petrofac Formation Testers Pretest Procedure

More information

Quick Start Setup Instructions for Raven LRC & AgXcel Harness for NH3 Profile plus GX40 Synergist

Quick Start Setup Instructions for Raven LRC & AgXcel Harness for NH3 Profile plus GX40 Synergist PLEASE NOTE: Your setup may vary. These screen shots represents a typical AgXcel Liquid Fertilizer System setup. See the Raven LRC Operator s Manual for safety information and additional setup and operating

More information

Bante820 Portable Dissolved Oxygen Meter Instruction Manual

Bante820 Portable Dissolved Oxygen Meter Instruction Manual Bante820 Portable Dissolved Oxygen Meter Instruction Manual BANTE INSTRUMENTS CO., LTD Bante820 Portable Dissolved Oxygen Meter 1 Introduction Thank you for selecting the Bante820 portable dissolved oxygen

More information

Energy capture performance

Energy capture performance Energy capture performance Cost of energy is a critical factor to the success of marine renewables, in order for marine renewables to compete with other forms of renewable and fossil-fuelled power generation.

More information

TapeStation Tips & Tricks

TapeStation Tips & Tricks TapeStation Tips & Tricks Agilent Technologies 1 CHECKPOINTS BEFORE STARTING A SCREENTAPE RUN 2 Before the ScreenTape run begins The following quick and easy steps show how to set up a run and assure proper

More information

SPLIT HOPKINSON PRESSURE BAR OPERATIONS MANUAL 5/9/2014

SPLIT HOPKINSON PRESSURE BAR OPERATIONS MANUAL 5/9/2014 B Calibration of Split Hopkinson Pressure Bar Setup: Calibration is performed by comparing the wave speed of the initial pulse versus the reflected pulse and calculating the Energy Ratio. This ratio gives

More information

D-Opto Dissolved Oxygen Sensor Operation Manual

D-Opto Dissolved Oxygen Sensor Operation Manual D-Opto Dissolved Oxygen Sensor Operation Manual Software version 2.6 Contents 1. Introduction..... 1 Optical Sensor Technology.... 1 Features...... 1 2. D-Opto Specifications. 2 Specifications... 2 3.

More information

Determination of Capillary pressure & relative permeability curves

Determination of Capillary pressure & relative permeability curves Determination of Capillary pressure & relative permeability curves With Refrigerated Centrifuge Multi speed centrifuge experiments Introduction As the porous diaphragm method (see Vinci s CAPRI), the centrifuge

More information

A review of best practices for Selection, Installation, Operation and Maintenance of Gas meters for Flare Applications used for Managing facility

A review of best practices for Selection, Installation, Operation and Maintenance of Gas meters for Flare Applications used for Managing facility A review of best practices for Selection, Installation, Operation and Maintenance of Gas meters for Flare Applications used for Managing facility mass balance and compliance 1. What, When and Why? 2. Flare

More information

UNITY 2 TM. Air Server Series 2 Operators Manual. Version 1.0. February 2008

UNITY 2 TM. Air Server Series 2 Operators Manual. Version 1.0. February 2008 UNITY 2 TM Air Server Series 2 Operators Manual Version 1.0 February 2008 1. Introduction to the Air Server Accessory for UNITY 2...2 1.1. Summary of Operation...2 2. Developing a UNITY 2-Air Server method

More information

MANUAL. P C - C E N T E R Version Copyright by Dinand van het Reve CONTENTS

MANUAL. P C - C E N T E R Version Copyright by Dinand van het Reve CONTENTS P C - C E N T E R Version 4.00 Copyright 1995-2004 by Dinand van het Reve CONTENTS 1. Introduction 2. Installing PC-CENTER 3. Licence 4. Using PC-CENTER 5. Description of 'Small Windows' 6. Main Menu Description

More information

LUMAZOTE T ECHNICAL BRO CHU RE

LUMAZOTE T ECHNICAL BRO CHU RE by Chemiluminescence Standards AST D4629 / ASTM D6069 / ASTM D 5176 / ASTM D 5762 / NF EN 12260 / NF M 07-058 Licence TOTAL LUMAZOTE T ECHNICAL BRO CHU RE ERALY & Associés Phone: +33 (0) 1 77 04 80 97

More information

Complete Range of Force Tensiometers

Complete Range of Force Tensiometers Sigma Complete Range of Force Tensiometers Versatility, automation and accuracy Precision made simple Attension Force Tensiometers are used in research, development and quality control for the study of

More information

U S F O S B u o y a n c y And Hydrodynamic M a s s

U S F O S B u o y a n c y And Hydrodynamic M a s s 1 U S F O S B u o y a n c y And Hydrodynamic M a s s 2 CONTENTS: 1 INTRODUCTION... 3 2 ACCURACY LEVELS... 3 2.1 LEVEL-0... 3 2.2 LEVEL-1... 3 2.3 PANEL MODEL... 3 3 EX 1. SINGLE PIPE. NON FLOODED... 4

More information

REQUIREMENTS AND HAND-OVER DOCUMENTATION FOR ENERGY-OPTIMAL DEMAND-CONTROLLED VENTILATION

REQUIREMENTS AND HAND-OVER DOCUMENTATION FOR ENERGY-OPTIMAL DEMAND-CONTROLLED VENTILATION REQUIREMENTS AND HAND-OVER DOCUMENTATION FOR ENERGY-OPTIMAL DEMAND-CONTROLLED VENTILATION Mads Mysen* 1, Axel Cablé 1, Peter G. Schild 1, and Kari Thunshelle 1 1 SINTEF Building and Infrastructure Forskningsveien

More information

User Manual. asense VAV. CO 2 / temperature sensor with built-in general purpose controller

User Manual. asense VAV. CO 2 / temperature sensor with built-in general purpose controller Gas and Air Sensors User Manual asense VAV CO / temperature sensor with built-in general purpose controller General The IAQ-sensor product asense VAV is used to measure indoor air carbon dioxide concentration

More information

Seton Hall University. 200 MHz MR. SOP manual

Seton Hall University. 200 MHz MR. SOP manual Seton Hall University 200 MHz MR SOP manual NMR Information: Varian Gemini 2000 NMR 1 H Frequency = 200 MHz Original purchase date: 1989 Donated from Merck & Co., Inc., 1998 Software upgrade: 2008 To schedule

More information

0349/MaN. Satron Pasve and Pasve ph

0349/MaN. Satron Pasve and Pasve ph 0349/MaN Satron Pasve and Pasve ph Pasve with Actuator Pasve ph manual Pasve ph with actuator Pasve ph Measuring Flushing Pasve ph, inline model measuring Std-glass PG13.5 Sensors and Adapters Sensor :

More information

USER MANUAL OPERATION AND THE USE OF A CAR WITH. Diego G3 / NEVO SEQUENTIAL GAS INJECTION SYSTEM

USER MANUAL OPERATION AND THE USE OF A CAR WITH. Diego G3 / NEVO SEQUENTIAL GAS INJECTION SYSTEM USER MANUAL OPERATION AND THE USE OF A CAR WITH Diego G3 / NEVO SEQUENTIAL GAS INJECTION SYSTEM Page 2 / 8 Table of csontents 1. STARTING THE ENGINE... 3 2. CONTROL PANEL... 3 2.1 Indication of the current

More information

HOBO U20L Water Level Logger (U20L-0x) Manual

HOBO U20L Water Level Logger (U20L-0x) Manual Test Equipment Depot - 800.517.8431-99 Washington Street Melrose, MA 02176 - TestEquipmentDepot.com HOBO U20L Water Level Logger (U20L-0x) Manual The HOBO U20L Water Level Logger is used for monitoring

More information

Laser Spectrometers for Online Moisture Measurement in Natural Gas. Ken Soleyn GE M&C

Laser Spectrometers for Online Moisture Measurement in Natural Gas. Ken Soleyn GE M&C Laser Spectrometers for Online Moisture Measurement in Natural Gas Ken Soleyn GE M&C ken.soleyn@ge.com Introduction TDLAS (Tunable Diode Lase Absorption Spectroscopy) Moisture Analyzers have become the

More information

SWS Option: Well Pressures. SWS Option: Stretch Correction (Corrected depth) SWS Option: MMD (Magnetic Marks Detection) ASEP Products

SWS Option: Well Pressures. SWS Option: Stretch Correction (Corrected depth) SWS Option: MMD (Magnetic Marks Detection) ASEP Products SWS Option: Well Pressures PART NUMBER L-8531039779 The SmartMonitor can simultaneously measure, display and record depth and up to four different well pressures (for example, Control Line Pressure, Tubing

More information

Time Pressure Dispensing

Time Pressure Dispensing Time Pressure Dispensing by Doug Dixon, GDM Product Manager What is time pressure dispensing? Time pressure is a method of dispensing liquid materials (surface mount adhesives and gasketing materials)

More information

Measuring Discharge in Shallower Rivers: ADCPs go from Rio to Pro

Measuring Discharge in Shallower Rivers: ADCPs go from Rio to Pro Measuring Discharge in Shallower Rivers: ADCPs go from Rio to Pro River monitoring supports many different activities from determining water reserves to designing flood defenses, and even to sports / leisure

More information

Digital Vacuum Regulator

Digital Vacuum Regulator Temperature Control for Research and Industry Digital Vacuum Regulator User s Manual Model DVR-280 INDEX SECTION PAGE 1. QUICK OPERATING INSTRUCTIONS............................. 3 KEM-NET DATA LOGGING

More information

AUK Environmental Sensor. Determining the refractive index of the air. AUK Environmental Sensor

AUK Environmental Sensor. Determining the refractive index of the air. AUK Environmental Sensor AUK Environmental Sensor Environmental influences can be compensated in two ways: 1. "Manual" input of the current data for air temperature, humidity and pressure and the material temperature of the testpiece

More information

ANALYTICAL SCALE HPLC AGILENT SYSTEMS OPERATIONAL QUALIFICATION

ANALYTICAL SCALE HPLC AGILENT SYSTEMS OPERATIONAL QUALIFICATION ANALYTICAL SCALE HPLC AGILENT SYSTEMS OPERATIONAL QUALIFICATION Standard OQ Test Suite This document describes the test program for qualifying LC analytical-scale Agilent systems; the following table lists

More information

Application Notes. SLP85xD Load Cells

Application Notes. SLP85xD Load Cells Application Notes Load Cells Table of Contents 1 Introduction 3 2 Description of the Filling Cycle 4 3 Filling Optimization 7 4 Filling Monitor 8 4.1 Weight-Based Filling Monitor... 8 4.2 Time-Based Filling

More information

Bante810 Benchtop Dissolved Oxygen Meter Instruction Manual

Bante810 Benchtop Dissolved Oxygen Meter Instruction Manual Bante810 Benchtop Dissolved Oxygen Meter Instruction Manual BANTE INSTRUMENTS CO., LTD Bante810 Benchtop Dissolved Oxygen Meter 1 Introduction Thank you for selecting the Bante810 benchtop dissolved oxygen

More information

FRONT DERAILLEUR - CURRENT RANGE

FRONT DERAILLEUR - CURRENT RANGE FRONT DERAILLEUR - CURRENT RANGE (since 2015) (since 2018) (since 2017) (since 2018) WARNING! This technical manual is intended for use by professional mechanics. Anyone who is not a qualified professional

More information

Generating Calibration Gas Standards

Generating Calibration Gas Standards Technical Note 1001 Metronics Inc. Generating Calibration Gas Standards with Dynacal Permeation Devices Permeation devices provide an excellent method of producing known gas concentrations in the PPM and

More information

DEVELOPMENT OF A ROBUST PUSH-IN PRESSUREMETER

DEVELOPMENT OF A ROBUST PUSH-IN PRESSUREMETER DEVELOPMENT OF A ROBUST PUSH-IN PRESSUREMETER Roger Failmezger, P.E. In-Situ Soil Testing, L.C., Lancaster, Virginia, USA ABSTRACT A push-in pressuremeter was developed using slotted steel casing with

More information

USER MANUAL. Intelligent Diagnostic Controller IDC24-A IDC24-AF IDC24-AFL IDC24-F IDP24-A * IDP24-AF * IDP24-AFL * IDP24-F * 1/73

USER MANUAL. Intelligent Diagnostic Controller IDC24-A IDC24-AF IDC24-AFL IDC24-F IDP24-A * IDP24-AF * IDP24-AFL * IDP24-F * 1/73 USER MANUAL Intelligent Diagnostic Controller IDC24-A IDC24-AF IDC24-AFL IDC24-F IDP24-A * IDP24-AF * IDP24-AFL * IDP24-F * *) Require software ID: DID-SW-001 1/73 Table of contents 1 General... 3 1.1

More information

INSTALLATION PROCEDURE FOR OPGW FIBER OPTIC CABLES

INSTALLATION PROCEDURE FOR OPGW FIBER OPTIC CABLES Page 1 of 15 INSTALLATION PROCEDURE FOR OPGW FIBER OPTIC CABLES Page 2 of 15 1. PURPOSE 2. SCOPE 3. REFERENCES 4. GENERAL INDEX 5. PROCEDURES 5.1 Line survey 5.2 Transport, loading, unloading and storage

More information

PMI Advanced Automated. Pulse Decay Permeameter APDP-10K-HP-101. Not just products... Solutions!

PMI Advanced Automated. Pulse Decay Permeameter APDP-10K-HP-101. Not just products... Solutions! PMI Advanced Automated Pulse Decay Permeameter APDP-10K-HP-101 Not just products... Solutions! DESCRIPTION The PMI s Advanced automated pulse decay Permeameter is used to measure gas permeability of samples

More information

Operations Manual. Internal automatic Pressure control for orbital tube welding. By Exel Orbital Systems, Inc. Page

Operations Manual. Internal automatic Pressure control for orbital tube welding. By Exel Orbital Systems, Inc. Page Operations Manual Internal automatic Pressure control for orbital tube welding. By Exel Orbital Systems, Inc. Page SG1 Overview and Dimensions 5.25 / 133 mm PS Power Supply Connection 4.06 / 103 mm Top

More information

Autodesk Moldflow Communicator Process settings

Autodesk Moldflow Communicator Process settings Autodesk Moldflow Communicator 212 Process settings Revision 1, 3 March 211. Contents Chapter 1 Process settings....................................... 1 Profiles.................................................

More information