Supporting Information
|
|
|
- Nathaniel Young
- 6 years ago
- Views:
Transcription
1 Supporting Information Bioassay-Guided Isolation of Prenylated Xanthone derivatives from the Leaves of Garcinia oligantha Yue-Xun Tang,,, Wen-Wei Fu,,, Rong Wu,, Hong-Sheng Tan,, Zhen-Wu Shen, and Hong-Xi Xu *,, School of Pharmacy, Shanghai University of Traditional Chinese Medicine, Cai Lun Lu 00, Shanghai 00, People s Republic of China Engineering Research Center of Shanghai Colleges for TCM New Drug Discovery, Cai Lun Lu 00, Shanghai 00, People's Republic of China Correspondence: Prof. Hong-Xi Xu, PhD, School of Pharmacy, Shanghai University of Traditional Chinese Medicine, Cai Lun Lu 00, Shanghai 00, China. xuhongxi88@gmail.com Tel: Fax: 86 08
2 List of Supporting Information Part Experimental Section. Computational details Part Results and HRESIMS, ECD, IR, and NMR spectra of compounds Table S. Cytotoxic IC 0 values of crude extracts and key fractions against cancer cell lines Figure CS. ptimized geometries of predominant conformers for (R)- (a h) Table CS. Calculated relative energies (Kcal/mol) and Boltzmann distributions of the optimized compound at BLYP/6-G(d, p) level in gas phase Figure CS. ptimized geometries of predominant conformers for (R, 7R, as, S)- (a g) at the BLYP/6-G(d, p) level in gas phase Table CS. Calculated relative energies (Kcal/mol) and Boltzmann distributions of the optimized compound at BLYP/6-G(d, p) level in gas phase Figure CS. ptimized geometries of predominant conformers for (R, 6R, 8S)-6 (a-h) at the BLYP/6-G(d, p) level in gas phase Table CS. Calculated relative energies (Kcal/mol) and Boltzmann distributions of the optimized compound 6 at BLYP/6-G(d, p) level in gas phase Figure CS. ptimized geometries of predominant conformers for (8S)-7 (a-i) at the BLYP/6- G(d, p) level in gas phase Table CS. Calculated relative energies (Kcal/mol) and Boltzmann distributions of the optimized compound 7 at BLYP/6-G(d, p) level in gas phase Figure S. Structures of gaudichaudione H () and cantleyanone A () Figure S. Key correlations observed in the HMBC and H- H CSY NMR spectra of -
3 Figure S. Key correlations observed in the HMBC and H- H CSY NMR spectra of compounds 8- Figure S. ECD spectra of compounds, - Figure S6. X-ray crystallographic structure of compound 8 liganthin H () Figure S7. HRESIMS spectrum of Figure S8. Experimental ECD spectrum of Figure S. UV spectrum of spectrum of Figure S. IR (KBr, disc) spectrum of Figure S. H NMR spectrum (pyridine-d, 600 MH Z ) of Figure S. C NMR spectrum (pyridine-d, 0 MH Z ) of Figure S. DEPT NMR spectrum (pyridine-d, 0 MH Z ) of Figure S. HSQC NMR spectrum (pyridine-d, 600 MH Z, 0 MH Z ) of Figure S. HMBC NMR spectrum (pyridine-d, 600 MH Z, 0 MH Z ) of Figure S6. H- H CSY spectrum (pyridine-d, 600 MHz) of Figure S7. NSEY NMR spectrum (pyridine-d, 600 MH Z ) of liganthin I () Figure S8. HRESIMS spectrum of Figure S. UV spectrum of Figure S0. IR (KBr, disc) spectrum of Figure S. H NMR spectrum (pyridine-d, 600 MH Z ) of
4 Figure S. C NMR spectrum (pyridine-d, 0 MH Z ) of Figure S. DEPT NMR spectrum (pyridine-d, 0 MH Z ) of Figure S. HSQC NMR spectrum (pyridine-d, 600 MH Z, 0 MH Z ) of Figure S. HMBC NMR spectrum (pyridine-d, 600 MH Z, 0 MH Z ) of Figure S6. H- H CSY spectrum (pyridine-d, 600 MH Z ) of liganthin J () Figure S7. HRESIMS spectrum of Figure S8. UV spectrum of Figure S. IR (KBr, disc) spectrum of Figure S0. H NMR spectrum (CDCl, 600 MH Z ) of Figure S. C NMR spectrum (CDCl, 0 MH Z ) of Figure S. DEPT NMR spectrum (CDCl, 0 MH Z ) of Figure S. HSQC NMR spectrum (CDCl, 600 MH Z, 0 MH Z ) of Figure S. HMBC NMR spectrum (CDCl, 600 MH Z, 0 MH Z ) of Figure S. H- H CSY spectrum (CDCl, 600 MH Z ) of liganthin K (): Figure S6. HRESIMS spectrum of Figure S7. UV spectrum of Figure S8. IR (KBr, disc) spectrum of Figure S. H NMR spectrum (CDCl, 600 MH Z ) of Figure S0. C NMR spectrum (CDCl, 0 MH Z ) of
5 Figure S. DEPT NMR spectrum (CDCl, 0 MH Z ) of Figure S. HSQC NMR spectrum (CDCl, 600 MH Z, 0 MH Z ) of Figure S. HMBC NMR spectrum (CDCl, 600 MH Z, 0 MH Z ) of Figure S. H- H CSY NMR spectrum (CDCl, 600 MH Z ) of liganthone B (): Figure S. HRESIMS spectrum of Figure S6. Experimental ECD spectrum of Figure S7. UV spectrum of Figure S8. IR (KBr, disc) spectrum of Figure S. H NMR spectrum (CDCl, 600 MH Z ) of Figure S0. C NMR spectrum (CDCl, 0 MH Z ) of Figure S. DEPT NMR spectrum (CDCl, 0 MH Z ) of Figure S. HSQC NMR spectrum (CDCl, 600 MH Z, 0 MH Z ) of Figure S. HMBC NMR spectrum (CDCl, 600 MH Z, 0 MH Z ) of Figure S. H- H CSY NMR spectrum (CDCl, 600 MH Z, 0 MH Z ) of Figure S. NSEY NMR spectrum (CDCl, 600 MH Z ) of liganthic Acid A (6): Figure S6. HRESIMS spectrum of 6 Figure S7. Experimental ECD spectrum of 6 Figure S8. UV spectrum of 6 Figure S. IR (KBr, disc) spectrum of 6
6 Figure S60. H NMR spectrum (CDCl, 600 MH Z ) of 6 Figure S6. C NMR spectrum (CDCl, 0 MH Z ) of 6 Figure S6. DEPT NMR spectrum (CDCl, 0 MH Z ) of 6 Figure S6. HSQC NMR spectrum (CDCl, 600 MH Z, 0 MH Z ) of 6 Figure S6. HMBC NMR spectrum (CDCl, 600 MH Z, 0 MH Z ) of 6 Figure S6. TCSY NMR spectrum (CDCl, 600 MH Z ) of 6 Figure S66. NSEY NMR spectrum (CDCl, 600 MH Z ) of 6 liganthic Acid B (7): Figure S67. HRESIMS spectrum of 7 Figure S68. Experimental ECD spectrum of 7 Figure S6. UV spectrum of 7 Figure S70. IR (KBr, disc) spectrum of 7 Figure S7. H NMR spectrum (DMS-d 6, 600 MH Z ) of 7 Figure S7. C NMR spectrum (DMS-d 6, 0 MH Z ) of 7 Figure S7. DEPT NMR spectrum (DMS-d 6, 0 MH Z ) of 7 Figure S7. HSQC NMR spectrum (DMS-d 6, 600 MH Z, 0 MH Z ) of 7 Figure S7. HMBC NMR spectrum (DMS-d 6, 600 MH Z, 0 MH Z ) of 7 Figure S76. TCSY NMR spectrum (DMS-d 6, 600 MH Z ) of 7 Figure S77. NSEY NMR spectrum (DMS-d 6, 600 MH Z ) of 7 liganthic Acid C (8): Figure S78. HRESIMS spectrum of 8 6
7 Figure S7. Experimental ECD spectrum of 8 Figure S80. UV spectrum of 8 Figure S8. IR (KBr, disc) spectrum of 8 Figure S8. H NMR spectrum (CDCl, 600 MH Z ) of 8 Figure S8. C NMR spectrum (CDCl, 0 MH Z ) of 8 Figure S8. DEPT NMR spectrum (CDCl, 0 MH Z ) of 8 Figure S8. HSQC NMR spectrum (CDCl, 600 MH Z, 0 MH Z ) of 8 Figure S86. HMBC NMR spectrum (CDCl, 600 MH Z, 0 MH Z ) of 8 Figure S87. TCSY NMR spectrum (CDCl, 600 MH Z ) of 8 Figure S88. NSEY NMR spectrum (CDCl, 600 MH Z ) of 8 liganthaxthanone A (): Figure S8. HRESIMS spectrum of Figure S0. UV spectrum of Figure S. IR (KBr, disc) spectrum of Figure S. H NMR spectrum (DMS-d 6, 600 MH Z ) of Figure S. C NMR spectrum (DMS-d 6, 0 MH Z ) of Figure S. DEPT NMR spectrum (DMS-d 6, 0 MH Z ) of Figure S. HSQC NMR spectrum (DMS-d 6, 600 MH Z, 0 MH Z ) of Figure S6. HMBC NMR spectrum (DMS-d 6, 600 MH Z, 0 MH Z ) of Figure S7. H- H CSY NMR spectrum (DMS-d 6, 600 MH Z ) of liganthaxthanone B (): 7
8 Figure S8. HRESIMS spectrum of Figure S. UV spectrum of Figure S0. IR (KBr, disc) spectrum of Figure S. H NMR spectrum (DMS-d 6, 600 MH Z ) of Figure S. C NMR spectrum (DMS-d 6, 0 MH Z ) of Figure S. DEPT NMR spectrum (DMS-d 6, 0 MH Z ) of Figure S. HSQC NMR spectrum (DMS-d 6, 600 MH Z, 0 MH Z ) of Figure S. HMBC NMR spectrum (DMS-d 6, 600 MH Z, 0 MH Z ) of Figure S6. H- H CSY NMR spectrum (DMS-d 6, 600 MH Z ) of 8
9 Supporting Information Available Part Experimental section. Computational details The theoretical calculations for compounds and -7 were performed using Gaussian 0. Conformational analysis was initially carried out using Maestro in Schrödinger 0 conformational searching together with the PLS_00 molecular mechanics methods. The optimized conformation geometries and thermodynamic parameters of all conformations were provided. The top twenty lowest-energy conformers of the PLS_00 conformers were optimized further at the BLYP/6-G (d, p) level. The minimum nature of the structure was confirmed by frequency calculations at the same computational level. The theoretical calculation of ECD was performed using time-dependent density functional theory (TDDFT) at the BLYP/6-G (d, p) level in MeH with PCM model. The calculated ECD curves were generated using SpecDis.6. References: () Gaussian 0, Revision E.0,M. J. Frisch, G. W. Trucks, H. B. Schlegel, G. E. Scuseria, M. A. Robb, J. R. Cheeseman, G. Scalmani, V. Barone, B. Mennucci, G. A. Petersson, H. Nakatsuji, M. Caricato, X. Li, H. P. Hratchian, A. F. Izmaylov, J. Bloino, G. Zheng, J. L. Sonnenberg, M. Hada, M. Ehara, K. Toyota, R. Fukuda, J. Hasegawa, M. Ishida, T. Nakajima, Y. Honda,. Kitao, H. Nakai, T. Vreven, J. A. Montgomery, Jr., J. E. Peralta, F. gliaro, M. Bearpark, J. J. Heyd, E. Brothers, K. N. Kudin, V. N. Staroverov, T. Keith, R. Kobayashi, J. Normand, K. Raghavachari, A. Rendell, J. C. Burant, S. S. Iyengar, J. Tomasi, M. Cossi, N. Rega, J. M. Millam, M. Klene, J. E. Knox, J. B. Cross, V. Bakken, C. Adamo, J. Jaramillo, R. Gomperts, R. E. Stratmann,. Yazyev, A. J. Austin, R. Cammi, C. Pomelli, J. W. chterski, R. L. Martin, K. Morokuma, V. G. Zakrzewski, G. A. Voth, P. Salvador, J. J. Dannenberg, S. Dapprich, A. D. Daniels,. Farkas, J. B. Foresman, J. V. rtiz, J. Cioslowski, and D. J. Fox, Gaussian, Inc., Wallingford CT, 0.
10 () T. Bruhn, A. Schaumlöffel, Y. Hemberger, G. Bringmann, SpecDis version.6, University of Wuerzburg, Germany, 0. Part Results and HRESIMS, IR, NMR, and ECD spectra of compounds Table S. Cytotoxic tests of the key fractions Table S. Cytotoxic IC 0 Values of Crude Extracts and Key Fractions against Cancer Cell Lines a Fraction PC- A.0 B. B >0 Paclitaxel 0.0 a.results are expressed as mean IC 0 values in µg/ml (extracts) or µm (paclitaxel). A: Petroleum ether extracts from the leaves of G. oligantha; B: EtAc-soluble portion of the 0% EtH extract from the leaves of G. oligantha; B: H -soluble portion of the 0% EtH extract from the leaves of G. oligantha. Figure CS ptimized geometries of predominant conformers for (R)- (a h) ptimized geometries of predominant conformers for (a h) at the BLYP/6-G (d, p) level in the gas phase.
11 Table CS. Calculated relative energies (Kcal/mol) and Boltzmann distributions of the optimized at BLYP/6-G (d, p) level in the gas phase. Calculated Relative Energies (Kcal/mol) and Boltzmann distributions of the optimized at BLYP/6-G (d, p) level in the gas phase. Conformation G ΔE % a b c d e f g h ΔE: Relative to a; %: Boltzmann distributions, using the relative Gibbs free energies as weighting factors at T = 8. K and atm Figure CS. ptimized geometries of predominant conformers for (R, 7R, as, S)- (a g) at the BLYP/6-G (d, p) level in the gas phase ptimized geometries of predominant conformers for (a g) at the BLYP/6-G (d, p) level in the gas phase
12 Table CS. Calculated relative energies (Kcal/mol) and Boltzmann distributions of the optimized at BLYP/6-G (d, p) level in the gas phase. Calculated relative energies (Kcal/mol) and Boltzmann distributions of the optimized at BLYP/6-G (d, p) level in the gas phase. Conformation G ΔE % a b c d e f g ΔE: Relative to a; %: Boltzmann distributions, using the relative Gibbs free energies as weighting factors at T = 8. K and atm Figure CS. ptimized geometries of predominant conformers for (R, 6R, 8S)-6 (a h) at the BLYP/6-G (d, p) level in the gas phase ptimized geometries of predominant conformers for 6 (a h) at the BLYP/6-G (d, p) level in the gas phase
13 Table CS. Calculated relative energies (Kcal/mol) and Boltzmann distributions of the optimized 6 at BLYP/6-G (d, p) level in the gas phase Table CS. Calculated relative energies (Kcal/mol) and Boltzmann distributions of the optimized 6 at BLYP/6-G (d, p) level in the gas phase. Conformation G ΔE % 6a b c d e f g ΔE: Relative to a; %: Boltzmann distributions, using the relative Gibbs free energies as weighting factors at T = 8. K and atm Figure CS. ptimized geometries of predominant conformers for (8S)-7 (a i) at the BLYP/6-G (d, p) level in the gas phase ptimized geometries of predominant conformers for 7 (a i) at the BLYP/6-G (d, p) level in the gas phase
14 Table CS. Calculated relative energies (Kcal/mol) and Boltzmann distributions of the optimized 7 at BLYP/6-G (d, p) level in the gas phase Table CS. Calculated relative energies (Kcal/mol) and Boltzmann distributions of the optimized 7 at BLYP/6-G (d, p) level in the gas phase. Conformation G ΔE % 7a b c d e f g h i ΔE: Relative to a; %: Boltzmann distributions, using the relative Gibbs free energies as weighting factors at T = 8. K and atm Figure S. Structures of gaudichaudione H () and cantleyanone A (). H H Me H Me H gaudichaudione H cantleyanone A Figure S. Key correlations observed in the HMBC and H- H CSY NMR spectra of - H H H H H H H H H H C HMBC H-H CSY
15 Figure S. Key correlations observed in the HMBC and H- H CSY NMR spectra of 8-. H CH H H H H H H H C HMBC H-H CSY 8 Figure S. ECD spectra of compounds, - ECD spectra of compounds oliganthone B (), gaudichaudione H () and cantleyanone ()
16 Figure S6. X-ray crystallographic structure of compound 8 Crystal structure of (±) oliganthic acid C. (a) Crystal packing of 8 showing the nonsuperimposition of (8S)-8 and (8R)-8. (b) RTEP diagram of 8S-oliganthic acid C ((8S)-8) 6
17 Figure S7. HRESIMS spectrum of Figure S8. Experimental ECD spectrum of 7
18 Figure S. UV spectrum of spectrum of Figure S. IR (KBr, disc) spectrum of 8
19 Figure S. H NMR spectrum (pyridine-d, 600 MH Z ) of Pyridine-d H H H Figure S. C NMR spectrum (pyridine-d, 0 MH Z ) of Pyridine-d
20 Figure S. DEPT NMR spectrum (pyridine-d, 0 MH Z ) of Figure S. HSQC NMR spectrum (pyridine- d, 600 MH Z, 0 MH Z ) of {8.7,0.}Pyridine-d f (ppm)
21 Figure S. HMBC NMR spectrum (pyridine-d, 600 MH Z, 0 MH Z ) of {8.7,0.}Pyridine-d f (ppm) 6 Figure S6. H- H CSY spectrum (pyridine-d, 600MHz) of {8.7,8.7}Pyridine-d f (ppm) 6
22 Figure S7. NESY spectrum (pyridine-d, 600MHz) of Figure S8. HRESIMS spectrum of Figure S. UV spectrum of 0. Absorbance (AU) Wavelength (nm)
23 Figure S0. IR (KBr, disc) spectrum of Figure S. H NMR spectrum (pyridine-d, 600 MH Z ) of Pyridine-d H H H
24 Figure S. C NMR spectrum (pyridine-d, 0 MH Z ) of Pyridine-d Figure S. DEPT NMR spectrum (pyridine-d, 0 MH Z ) of
25 Figure S. HSQC NMR spectrum (pyridine-d, 600 MH Z, 0 MH Z ) of {8.7,0.}Pyridine-d f (ppm) Figure S. HMBC NMR spectrum (pyridine-d, 600 MH Z, 0 MH Z ) of {8.7,0.}Pyridine-d f (ppm) 6
26 Figure S6. H- H CSY NMR spectrum (pyridine-d, 600 MH Z ) of {8.7,8.7}Pyridine-d f (ppm) 6 Figure S7. HRESIMS spectrum of 6
27 Figure S8. UV spectrum of Figure S. IR (KBr, disc) spectrum of 7
28 Figure S0. H NMR spectrum (CDCl, 600 MH Z ) of Figure S C NMR spectrum (CDCl, 0 MH Z ) of CDCl
29 Figure S. DEPT NMR spectrum (CDCl, 0 MH Z ) of Figure S. HSQC NMR spectrum (CDCl, 600 MH Z, 0 MH Z ) of {7.6,77.6}CDCl f (ppm) 0
30 Figure S. HMBC NMR spectrum (CDCl, 600 MH Z, 0 MH Z ) of {7.6,77.6}CDCl f (ppm) 0 - Figure S. H- H CSY spectrum (CDCl, 600 MH Z ) of 6 {7.6,7.6}CDCl f (ppm)
31 Figure S6. HRESIMS spectrum of Figure S7. UV spectrum of Absorbance (AU) Wavelength (nm) Figure S8. IR (KBr, disc) spectrum of
32 Figure S. H NMR spectrum (CDCl, 600 MH Z ) of CDCl H H H Figure S0. C NMR spectrum (CDCl, 0 MH Z ) of CDCl
33 Figure S. DEPT NMR spectrum (CDCl, 0 MH Z ) of Figure S. HSQC NMR spectrum (CDCl, 600 MH Z, 0 MH Z ) of {7.6,77.6}CDCl f (ppm)
34 Figure S. HMBC NMR spectrum (CDCl, 600 MH Z, 0 MH Z ) of {7.6,77.6}CDCl f (ppm) 0 Figure S. H- H CSY NMR spectrum (CDCl, 600 MH Z ) of {7.6,7.6}CDCl f (ppm)
35 Figure S. HRESIMS spectrum of Figure S6. Experimental ECD spectrum of
36 Figure S7. UV spectrum of Figure S8. IR (KBr, disc) spectrum of 6
37 Figure S. H NMR spectrum (CDCl, 600 MH Z ) of CDCl H Figure S0. C NMR spectrum (CDCl, 0 MH Z ) of CDCl
38 Figure S. DEPT NMR spectrum (CDCl, 0 MH Z ) of Figure S. HSQC NMR spectrum (CDCl, 600 MH Z, 0 MH Z ) of {7.6,77.6}CDCl f (ppm) 8
39 Figure S. HMBC NMR spectrum (CDCl, 600 MH Z, 0 MH Z ) of {7.6,77.6}CDCl f (ppm) Figure S. H- H CSY spectrum (CDCl, 600 MH Z ) of
40 Figure S. NESY NMR spectrum (CDCl, 600 MH Z ) of {7.6,7.6}CDCl f (ppm) Figure S6. HRESIMS spectrum of 6 0
41 Figure S7. Experimental ECD spectrum of 6 Figure S8. UV spectrum of 6
42 Figure S. IR (KBr, disc) spectrum of 6 Figure S60. H NMR spectrum (CDCl, 600 MH Z ) of CDCl H H H H
43 Figure S6. C NMR spectrum (CDCl, 0 MH Z ) of CDCl Figure S6. DEPT NMR spectrum (CDCl, 0 MH Z ) of 6
44 Figure S6. HSQC NMR spectrum (CDCl, 600 MH Z, 0 MH Z ) of {7.6,77.6}CDCl f (ppm) 0 Figure S6. HMBC NMR spectrum (CDCl, 600 MH Z, 0 MH Z ) of 6 {0.00,-0.00} f (ppm) 0 -
45 Figure S6. TCSY NMR spectrum (CDCl, 600 MH Z ) of 6 {7.6,7.6}CDCl f (ppm) Figure S66. NESY NMR spectrum (CDCl, 600 MH Z ) of 6 0 {7.6,7.6}CDCl f (ppm)
46 Figure S67. HRESIMS spectrum of 7 Figure S68. Experimental ECD spectrum of 7 6
47 Figure S6. UV spectrum of 7 Figure S70. IR (KBr, disc) spectrum of 7 7
48 Figure S7. H NMR spectrum (DMS-d 6, 600 MH Z ) of DMS-d H H H Figure S7. C NMR spectrum (DMS-d 6, 0 MH Z ) of 7 8
49 Figure S7. DEPT NMR spectrum (DMS-d 6, 0 MH Z ) of 7 Figure S7. HSQC NMR spectrum (DMS-d 6, 600 MH Z, 0 MH Z ) of 7 0 {.0,.}DMS-d f (ppm)
50 Figure S7. HMBC NMR spectrum (DMS-d 6, 600 MH Z, 0 MH Z ) of 7 0 {.0,.}Dimethyl Sulfoxide-d f (ppm) Figure S76. TCSY NMR spectrum (DMS-d 6, 600 MH Z ) of 7 {.0,.0}DMS-d f (ppm) 6 0
51 Figure S77. NESY NMR spectrum (DMS-d 6, 600 MH Z ) of 7 {.0,.0}DMS-d f (ppm) Figure S78. HRESIMS spectrum of 8
52 Figure S7. Experimental ECD spectrum of 8 Figure S80. UV spectrum of 8 0. Absorbance (AU) Wavelength (nm)
53 Figure S8. IR (KBr, disc) spectrum of 8 Figure S8. H NMR spectrum (CDCl, 600 MH Z ) of CDCl H H
54 Figure S8. C NMR spectrum (CDCl, 0 MH Z ) of CDCl Figure S8. DEPT NMR spectrum (CDCl, 0 MH Z ) of 8
55 Figure S8. HSQC NMR spectrum (CDCl, 600 MH Z, 0 MH Z ) of 8 B-q {7.6,77.}cdcl f (ppm) Figure S86. HMBC NMR spectrum (CDCl, 600 MH Z, 0 MH Z ) of 8 {-0.00,0.00} f (ppm)
56 Figure S87. TCSY NMR spectrum (CDCl, 600 MH Z ) of 8 Figure S88. NESY NMR spectrum (CDCl, 600 MH Z ) of 8 6
57 Figure S8. HRESIMS spectrum of Figure S0. UV spectrum of Absorbance (AU) Wavelength (nm) Figure S. IR (KBr, disc) spectrum of 7
58 Figure S. H NMR spectrum (DMS-d 6, 600 MH Z ) of DMS-d H H Figure S. C NMR spectrum (DMS-d 6, 0 MH Z ) of DMS-d
59 Figure S. DEPT NMR spectrum (DMS-d 6, 0 MH Z ) of Figure S. HSQC NMR spectrum (DMS-d 6, 600 MH Z, 0 MH Z ) of 0 {.0,.}DMS-d f (ppm)
60 Figure S6. HMBC NMR spectrum (DMS-d 6, 600 MH Z, 0 MH Z ) of 0 {.0,.}Dimethyl Sulfoxide-d f (ppm) Figure S7. H- H CSY NMR spectrum (DMS-d 6, 600 MH Z, 0 MH Z ) of 0 {.0,.0}DMS-d f (ppm)
61 Figure S8. HRESIMS spectrum of Figure S. UV spectrum of 6
62 Figure S0. IR (KBr, disc) spectrum of Figure S. H NMR spectrum (DMS-d 6, 600 MH Z ) of H H H.0 Dimethyl Sulfoxide-d H
63 Figure S. C NMR spectrum (DMS-d 6, 0 MH Z ) of Dimethyl Sulfoxide-d Figure S. DEPT NMR spectrum (DMS-d 6, 0 MH Z ) of 6
64 Figure S. HSQC NMR spectrum (DMS-d 6, 600 MH Z, 0 MH Z ) of 0 {.0,.}DMS-d f (ppm) 6 Figure S. HMBC NMR spectrum (DMS-d 6, 600 MH Z, 0 MH Z ) of {.0,.}DMS-d f (ppm) 6 6
65 Figure S6. H- H CSY NMR spectrum (DMS-d 6, 600 MH Z ) of {.0,.0}DMS-d f (ppm) 6 6
Supporting Information
Supporting Information Sesqui- and Diterpenoids from the Radix of Curcuma aromatica Shengjuan Dong, Baocai Li, Weifeng Dai, Dong Wang, Yi Qin and Mi Zhang* Faculty of Life Science and Technology, Kunming
Bioactive Pentacyclic Triterpenoids from the Leaves of Cleistocalyx operculatus
Bioactive Pentacyclic Triterpenoids from the Leaves of Cleistocalyx operculatus Chen Wang,, Ping Wu, Shuai Tian, Jinghua Xue, Liangxiong Xu, anxiang Li, and Xiaoyi Wei *, Key Laboratory of Plant Resources
SUPPORTING INFORMATION
SUPPORTING INFORMATION Heptaketides from an Endolichenic Fungus Biatriospora sp. and Their Antifungal Activity Yan-Hui Zhou, Ming Zhang, Rong-Xiu Zhu, Jiao-Zhen Zhang, Fei-Xie, Xiao-Bin Li, Wen-Qiang Chang,
LC-MS-Guided Isolation of Insulin Secretion-promoting. Monoterpenoid Carbazole Alkaloids from Murraya
Supporting Information LC-MS-Guided Isolation of Insulin Secretion-promoting Monoterpenoid Carbazole Alkaloids from Murraya microphylla Xiao-Li Ma, Jun Li, Jiao Zheng, Xiao-Pan Gu, Daneel Ferreira, Jordan
Fortunoids A C, Three Sesquiterpenoid Dimers with. Different Carbon Skeletons from Chloranthus fortunei
Supporting Information for Fortunoids A C, Three Sesquiterpenoid Dimers with Different Carbon Skeletons from Chloranthus fortunei Bin Zhou, Qun-Fang Liu, Seema Dalal, Maria B. Cassera, and Jian-Min Yue,
Supporting information
Supporting information Antimicrobial Metabolites from Streptomyces sp. SN0280 Hui Tian, Jamil Shafi, Mingshan Ji,, Yuhui Bi, and Zhiguo Yu *,, College of Plant Protection, Shenyang Agricultural University,
Hawaiienols A D, Highly Oxygenated p-terphenyls from an. Insect-Associated Fungus Paraconiothyrium hawaiiense
Hawaiienols A D, Highly Oxygenated p-terphenyls from an Insect-Associated Fungus Paraconiothyrium hawaiiense Fengxia Ren,, Shenxi Chen,, Yang Zhang, Shuaiming Zhu, Junhai Xiao, Xingzhong Liu, Ruibin Su,*,
Metabolomics-driven Discovery of Meroterpenoids from a Musselderived. Penicillium ubiquetum
Supporting Information Metabolomics-driven Discovery of Meroterpenoids from a Musselderived Penicillium ubiquetum Thi Phuong Thuy oang,, Catherine Roullier,*,, Marie-Claude Boumard, Thibaut Robiou du Pont,
Lipid Peroxidation and Cyclooxygenase Enzyme Inhibitory Compounds
Lipid Peroxidation and Cyclooxygenase Enzyme Inhibitory Compounds from Prangos haussknechtii Amila A. Dissanayake, Baram A. H. Ameen, and Muraleedharan G. Nair,* Bioactive Natural Products and Phytoceuticals
Bafilomycins and Odoriferous Sesquiterpenoids from Streptomyces albolongus Isolated from Elephas maximus Feces
Supporting Information Bafilomycins and Odoriferous Sesquiterpenoids from Streptomyces albolongus Isolated from Elephas maximus Feces Nan Ding,, Yi Jiang, Li Han, Xiu Chen, Jian Ma, Xiaodan Qu, Yu Mu,
Natural Nitric Oxide (NO) inhibitors from the rhizomes of Curcuma phaeocaulis. Supplementary Information
Electronic Supplementary Material (ESI) for rganic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 205 Natural Nitric xide (N) inhibitors from the rhizomes of Curcuma phaeocaulis
Supporting information. Random Structural Modification of a Low Band Gap BODIPY-Based Polymer
Supporting information Random Structural Modification of a Low Band Gap BODIPY-Based Polymer Léo Bucher, a,b Shawkat M. Aly, a Nicolas Desbois, b Paul-Ludovic Karsenti, a Claude P. Gros, b * and Pierre
Supplementary Materials: Bioactive Polycyclic Quinones from Marine Streptomyces sp. 182SMLY
S1 of S26 Supplementary Materials: Bioactive Polycyclic Quinones from Marine Streptomyces sp. 182SMLY Ying Liang, Xin Xie, Lu Chen, Shilun Yan, Xuewei Ye, Komal Anjum, Haocai Huang, Xiao Yuan Lian and
Joo Tae Hwang, Yesol Kim, Hyun-Jae Jang, Hyun-Mee Oh, Chi-Hwan Lim, Seung Woong Lee and Mun-Chual Rho
S1 of S43 Supplementary Materials: Conversion Study of Feruloyl Amides from Portulaca oleracea by UV Light and Their Inhibitory Effect on IL-6-Induced STAT3 Activation Joo Tae Hwang, Yesol Kim, Hyun-Jae
Supplementary Information
Supplementary Information Vitroprocines, new antibiotics against Acinetobacter baumannii, discovered from marine Vibrio sp. QWI 6 using mass spectrometry based metabolomics approach Chih Chuang Liaw 1,2,3
Formation of Nudicaulins In Vivo and In Vitro and the Biomimetic Synthesis and Bioactivity of O-Methylated Nudicaulin Derivatives
Formation of Nudicaulins In Vivo and In Vitro and the Biomimetic Synthesis and Bioactivity of O-Methylated Nudicaulin Derivatives Bettina Dudek 1,, Florian Schnurrer 1,, Hans-Martin Dahse 2, Christian
Marine AChE inhibitors isolated from Geodia baretti: Natural compounds and their synthetic analogs
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2015 Supporting Information Marine AChE inhibitors isolated from Geodia baretti:
Key Laboratory of Material Chemistry for Energy Conversion and Storage (Ministry
Electronic Supplementary Material (ESI) for Dalton Transactions. This journal is The Royal Society of Chemistry 2018 Supporting Information for Dramatically enhanced visible-light driven H 2 evolution
SUPPLEMENTARY MATERIAL TO Solvatochromism of isatin based Schiff bases: An LSER and LFER study
J. Serb. Chem. Soc. 8 (9) S258S266 (26) Supplementary material SUPPLEMENTARY MATERIAL TO Solvatochromism of isatin based Schiff bases: An LSER and LFER study DOMINIK R. BRKIĆ, ALEKSANDRA R. BOŽIĆ, VESNA
A reformative oxidation strategy using high concentration nitric acid for. enhancing emission performance of graphene quantum dots
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2014 A reformative oxidation strategy using high concentration nitric acid for enhancing emission
General Information. Department of Physics, Kansas State University, 116 Cardwell Hall Manhattan, KS 66506, USA. Education
General Information Name Gender Birth Citizenship Major Email Address Qing Liao Male 27/02/1983, China Chinese Physical Electronics liaoqing@phys.ksu.edu Department of Physics, Kansas State University,
Facile synthesis of N-rich carbon quantum dots by spontaneous. polymerization and incision of solvents as efficient bioimaging probes
Electronic Supplementary Material (ESI) for Nanoscale. This journal is The Royal Society of Chemistry 2015 Supporting Information Facile synthesis of N-rich carbon quantum dots by spontaneous polymerization
Section 4.2. Travelling Waves
Section 4.2 Travelling Waves Wave Motion A wave is the motion of a disturbance Mechanical waves require Some source of disturbance A medium that can be disturbed Some physical connection between or mechanism
Real-time Analysis of Industrial Gases with Online Near- Infrared Spectroscopy
Real-time Analysis of Industrial Gases with Online Near- Infrared Branch 5 Petrochemical, Biofuels Keywords Process, NIR, Gases, Gas Cell, Ethylene, Carbon Dioxide, Propane, Butane, Acetylene Summary Near-infrared
LOW PRESSURE EFFUSION OF GASES adapted by Luke Hanley and Mike Trenary
ADH 1/7/014 LOW PRESSURE EFFUSION OF GASES adapted by Luke Hanley and Mike Trenary This experiment will introduce you to the kinetic properties of low-pressure gases. You will make observations on the
LOW PRESSURE EFFUSION OF GASES revised by Igor Bolotin 03/05/12
LOW PRESSURE EFFUSION OF GASES revised by Igor Bolotin 03/05/ This experiment will introduce you to the kinetic properties of low-pressure gases. You will make observations on the rates with which selected
Study on Water Hammer Prevention in Pumping Water Supply Systems by Multi-valves
Study on Water Hammer Prevention in Pumping Water Supply Systems by Multi-valves Manlin Zhu, Xiaohong Zhang, Yanhe Zhang, Tao Wang Institute of Water Resources and Hydro-electric Engineering Xi an University
Supporting Information
Supporting Information An Experimental and Computational Approach to Understanding the Reactions of Acyl Nitroso Compounds in [4+2]-Cycloadditions Duangduan Chaiyaveij, Andrei S. Batsanov, Mark A. Fox,
User guide for the NMR spectrometer AVA400Stud
1 User guide for the NMR spectrometer AVA400Stud Dear User! You are using a modern NMR spectrometer, which has been installed in 2009. About 12500 spectra are measured here per year. Please respect the
Fast method for Ginseng Analyses using Agilent Poroshell 120 Columns Scaled from a Traditional Method
Fast method for Ginseng Analyses using Agilent Poroshell Columns Scaled from a Traditional Method Application Note Pharmaceutical Author Rongjie Fu Agilent Technologies (Shanghai) Co. Ltd. 4 Ying Lun Road
Carbon Dioxide Flooding. Dr. Helmy Sayyouh Petroleum Engineering Cairo University
Carbon Dioxide Flooding Dr. Helmy Sayyouh Petroleum Engineering Cairo University Properties of CO 2... Properties of CO2... CO2 density increases with:.increasing pressure.decreasing temperature Viscosity
Supporting information. for. The Solvent-free Michaelis-Arbuzov Rearrangement under Flow Conditions
Supporting information The Solvent-free Michaelis-Arbuzov Rearrangement under Flow Conditions for Aleksandra Jasiak, * a Grażyna Mielniczak, a Krzysztof wsianik, a Marek Koprowski, a Dorota Krasowska a
Journal of Chemical and Pharmaceutical Research, 2014, 6(3): Research Article
Available online www.jocpr.com Journal of Chemical and Pharmaceutical Research 2014 6(3):304-309 Research Article ISSN : 0975-7384 CODEN(USA) : JCPRC5 World men sprint event development status research
Octahedral Pd Nanocages with Porous Shells Converted by Co(OH) 2 Nanocages with Nanosheet surface as Robust Electrocatalysts for Ethanol Oxidation
Electronic Supplementary Material (ESI) for Journal of Materials Chemistry A. This journal is The Royal Society of Chemistry 2018 Octahedral Pd Nanocages with Porous Shells Converted by Co(OH) 2 Nanocages
Typically NMR Sample Configuration
Typically NMR Sample Configuration = B o Solvent column ~ 3 as long as detection region. Copyright 003-014 UWChemMRF All Rights Reserved. Last updated Sept 15, 014. The following slides are useful as an
EXPERIMENT XI. Careful!! Improper handling of the vacuum line may result in the release of SO 2 which is an irritating and suffocating gas.
Chem 366-3 Page XI - 1 EXPERIMENT XI INFRARED SPECTRUM OF SO2 (S&G, 5th ed. Expt 36, 6th ed. Expt. 35) 1. Pre-Lab preparation. The description of this experiment has disappeared from the more recent editions
Supplementary Information
Electronic Supplementary Material (ESI) for Journal of Materials Chemistry A. This journal is The Royal Society of Chemistry 2019 Supplementary Information Mo modulation effect on the hydrogen binding
Support Information. Diketopiperazines as cross communication quorum-sensing signals between Cronobacter sakazakii and Bacillus cereus
Support Information Diketopiperazines as cross communication quorum-sensing signals between Cronobacter sakazakii and Bacillus cereus Matheus R. Bofinger; Lucas S. de Sousa, José E. N. Fontes, Anita J.
A New Inhibitor Targeting Signal Transducer and Activator of. Transcription 5 (STAT5) Signaling in Myeloid Leukemias
Supporting Information A New Inhibitor Targeting Signal Transducer and Activator of Transcription 5 (STAT5) Signaling in Myeloid Leukemias Ludovic Juen,,# Marie Brachet-Botineau,,,# Cécile Parmenon, Jérôme
CHEM254 #4 The Synthesis of a Tertiary Alcohol Using a Pre-Made Grignard Reagent 1
CHEM254 #4 The Synthesis of a Tertiary Alcohol Using a Pre-Made Grignard Reagent 1 Background In this project, we will perform a Grignard reaction using a pre-made Grignard reagent. Grignard reagents can
Purpose and Scope: Responsibilities: Warnings and precautions: Background Beers law
Purpose and Scope: This document describes the procedures and policies for using the MSE Bruker FTIR Spectrometer. The scope of this document is to establish user procedures. Instrument maintenance and
A mitochondria-targeted near-infrared probe for colorimetric and. ratiometric fluorescence detection of hypochlorite in living cells
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 216 Electronic Supplementary Information A mitochondria-targeted near-infrared probe for colorimetric
Evgeny A. Katayev and Markus B. Schmid
Supplementary information Control of metal-directed self-assembly by metal-amine interactions Evgeny A. Katayev and Markus B. Schmid Institut für Organische Chemie, Universität Regensburg, Universitätsstr.
Supporting Information
Supporting Information A General Strategy to Fabricate P as Highly Efficient Cocatalyst via Photo-Reduction Deposition for Hydrogen Evolution Yuming Dong a, *, Linggang Kong a, Pingping Jiang a, Guangli
Facile fabrication of well-defined polyaniline microtubes derived. from natural kapok fiber for supercapacitor with long-term.
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2016 Facile fabrication of well-defined polyaniline microtubes derived from natural kapok fiber
state asymmetric supercapacitors
Electronic Supplementary Material (ESI) for Journal of Materials Chemistry A. This journal is The Royal Society of Chemistry 2016 3D hierarchical CoO@MnO 2 core-shell nanohybrid for high-energy solid state
Supporting Information
Electronic Supplementary Material (ESI) for Journal of Materials Chemistry A. This journal is The Royal Society of Chemistry 2017 Supporting Information 3D-composite structure of FeP nanorods supported
Supplementary Material
Electronic Supplementary Material (ESI) for Journal of Materials Chemistry A. This journal is The Royal Society of Chemistry 2018 Supplementary Material Biomass Chitosan Derived Cobalt/Nitrogen Doped Carbon
Three-Dimensional Plasmonic Hydrogel Architecture: Facile Synthesis and Its Macro Scale Effective Space
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 0 Electronic Supporting Information Three-Dimensional Plasmonic Hydrogel Architecture: Facile Synthesis
FOURIER TRANSFORM INFRARED SPECTROSCOPY
Purpose and Scope: This document describes the procedures and policies for using the MSE Bruker FTIR Spectrometer. The scope of this document is to establish user procedures. Instrument maintenance and
Study on the Influencing Factors of Gas Mixing Length in Nitrogen Displacement of Gas Pipeline Kun Huang 1,a Yan Xian 2,b Kunrong Shen 3,c
Applied Mechanics and Materials Online: 2013-06-13 ISSN: 1662-7482, Vols. 321-324, pp 299-304 doi:10.4028/www.scientific.net/amm.321-324.299 2013 Trans Tech Publications, Switzerland Study on the Influencing
Numerical Simulations of a Three-Lane Traffic Model Using Cellular Automata. A. Karim Daoudia and Najem Moussa
CHINESE JOURNAL OF PHYSICS VOL. 41, NO. 6 DECEMBER 2003 Numerical Simulations of a Three-Lane Traffic Model Using Cellular Automata A. Karim Daoudia and Najem Moussa LMSPCPV, Dépt. de Physique, FST, B.P.
Vertical in situ profiles of nitrate and oxygen in the northern Japan Sea
Vertical in situ profiles of nitrate and oxygen in the northern Japan Sea Dmitry D. Kaplunenko, Vyacheslav B. Lobanov, Pavel Ya. Tishchenko and Maria G. Shvetsova V.I.Il'ichev Pacific Oceanological Institute,
A Coal Mine Multi-Point Fiber Ethylene Gas Concentration Sensor
PHOTONIC SENSORS / Vol. 5, No. 1, 215: 67 71 A Coal Mine Multi-Point Fiber Ethylene Gas Concentration Sensor Yubin WEI 1,2, Jun CHANG 1*, Jie LIAN 1, and Tongyu LIU 2 1 School of Information Science and
Developing an Effective Quantification Method of Tongue Deviation Angle to Assess Stroke Patients
2012 4th International Conference on Bioinformatics and Biomedical Technology IPCBEE vol.29 (2012) (2012) ICSIT Press, Singapore Developing an Effective Quantification Method of Tongue Deviation ngle to
Supporting information
Electronic Supplementary Material (ESI) for Journal of Materials Chemistry A. This journal is The Royal Society of Chemistry Please do 2018 not adjust margins Supporting information Self-assembled 3D flower-like
IJPAR Vol.6 Issue 1 Jan - Mar Journal Home page:
IJPAR Vol.6 Issue 1 Jan - Mar -2017 Journal Home page: ISSN:2320-2831 Research article Open Access Optimization of stability indicating RP-HPLC method for the estimation of an anti-cancer drug Sorafenib
Hierachical Nickel-Carbon Structure Templated by Metal-Organic Frameworks for Efficient Overall Water Splitting
Electronic Supplementary Material (ESI) for Energy & Environmental Science. This journal is The Royal Society of Chemistry 2018 Electronic Supplementary Information Hierachical Nickel-Carbon Structure
Biphenyls from the Twigs of Garcinia multiflora and their Anti- Tobacco Mosaic Virus Activities
ORIGINAL ARTICLE Rec. Nat. Prod. 10:5 (2015) 566-571 Biphenyls from the Twigs of Garcinia multiflora and their Anti- Tobacco Mosaic Virus Activities Xingmeng Xu 1,2, Jianlian Shi 1,2, Lan Li 1,2, Donglai
Things to know before operating an NMR spectrometer André Boltjes, University of Groningen DD NMR Lab v
Things to know before operating an NMR spectrometer André Boltjes, University of Groningen DD NMR Lab v1.0 2013 I. A tour of an NMR lab. Figure 1 shows a picture of our Avance DRX 500. Although each NMR
2017, DIILI Publication. Original Paper PREDICTION OF SOLUBILITY OF ETODOLAC IN BINARY SOLVENTS USING EXTENDED HILDEBRAND SOLUBILITY APPROACH
2017, DIILI Publication American Journal of Life Science Researches 2017; 5(3): 70-78 Published online July, 2017 (http://www.diili.org/ojs-2.4.6/index.php/ajlsr/index) ISSN: 2375-7485 (Print); ISSN: 2332-0206
Optimization of Separator Train in Oil Industry
Optimization of Separator Train in Oil Industry Pawan jain a M.E. Petroleum Engineering, Maharashtra Institute of Technology, Pune-411038 ---------------------------------------------------------------------***---------------------------------------------------------------------
Experimental determination of deflagration explosion characteristics of methane air mixture and their verification by advanced numerical simulation
Structures Under Shock and Impact XII 169 Experimental determination of deflagration explosion characteristics of methane air mixture and their verification by advanced numerical simulation M. Mynarz,
Isotopes and Gases. Isotopes as constraints to air sea gas exchange, gas exchange time scales, the various time scales of carbon (isotope) exchange
Isotopes and Gases Isotopes as constraints to air sea gas exchange, gas exchange time scales, the various time scales of carbon (isotope) exchange Isotope effects in gas solution and molecular diffusion
Spin Density Distribution after Electron Transfer from Triethylamine to an [Ir(ppy) 2 (bpy)] + Photosensitizer during Photocatalytic Water Reduction
![Spin Density Distribution after Electron Transfer from Triethylamine to an [Ir(ppy) 2 (bpy)] + Photosensitizer during Photocatalytic Water Reduction](/thumbs/88/116892911.jpg "Spin Density Distribution after Electron Transfer from Triethylamine to an [Ir(ppy) 2 (bpy)] + Photosensitizer during Photocatalytic Water Reduction")
Spin Density Distribution after Electron Transfer from Triethylamine to an [Ir(ppy) 2 (bpy)] + Photosensitizer during Photocatalytic Water Reduction Sergey I. Bokarev,* Dirk Hollmann, Alexandra Pazidis,
Mechanism Analysis and Optimization of Signalized Intersection Coordinated Control under Oversaturated Status
Available online at www.sciencedirect.com ScienceDirect Procedia - Social and Behavioral Scien ce s 96 ( 2013 ) 1433 1442 13th COTA International Conference of Transportation Professionals (CICTP 2013)
Chapter 10 Mr. Davis, M.Ed.
1 THE NATURE OF WAVES Chapter 10 Mr. Davis, M.Ed. Physical Science - 2017 2 Amplitude THE HEIGHT OF A WAVE. THE AMPLITUDE OF A WAVE IS THE MAXIMUM DISTANCE THAT THE PARTICLES OF A MEDIUM VIBRATE FROM THEIR
CHAPTER 185 SAND TRANSPORT UNDER GROUPING WAVES
CHAPTER 185 SAND TRANSPORT UNDER GROUPING WAVES Shinji Sato 1 Abstract Laboratory experiments as well as numerical modeling were conducted for sand transport under non-breaking grouping waves. Experiments
Basketball field goal percentage prediction model research and application based on BP neural network
ISSN : 0974-7435 Volume 10 Issue 4 BTAIJ, 10(4), 2014 [819-823] Basketball field goal percentage prediction model research and application based on BP neural network Jijun Guo Department of Physical Education,
S on equipment and pipelines along with the constant threat to personnel safety justify major investment in H 2
Application Summary Analytes: S (hydrogen sulfide) Detector: OMA-300 S Analyzer Process Stream: natural gas Introduction Raw natural gas contains hydrogen suflide, the level of which varies by field. Due
Waves Questions - CfE
Waves Questions - CfE 1) a) Define what is meant by a transverse wave. b) List nine examples of transverse waves. 2) a) Define what is meant by a longitudinal wave. b) State one example of a longitudinal
(2 pts) Draw the line of best fit through the data and estimate the concentration of Fe in your sample solution.
Name: 1. You are asked to measure the percent iron in a steel sample you believe to be about 50% Fe by mass. You dissolve four replicate samples in nitric acid and dilute them by mass to a concentration
EXPERIMENTAL STUDY ON THE HYDRODYNAMIC BEHAVIORS OF TWO CONCENTRIC CYLINDERS
EXPERIMENTAL STUDY ON THE HYDRODYNAMIC BEHAVIORS OF TWO CONCENTRIC CYLINDERS *Jeong-Rok Kim 1), Hyeok-Jun Koh ), Won-Sun Ruy 3) and Il-Hyoung Cho ) 1), 3), ) Department of Ocean System Engineering, Jeju
JASCO 810 CD SPECTROPLOARIMETER STANDARD OPERATING PROCEDURE
JASCO 810 CD SPECTROPLOARIMETER STANDARD OPERATING PROCEDURE Purpose of this Instrument: This instrument is for measuring differences in the absorption of lefthanded polarized light versus right-handed
Supporting Information
Electronic Supplementary Material (ESI) for Journal of Materials Chemistry A. This journal is The Royal Society of Chemistry 2015 Supporting Information Template-Preparation of Three-Dimensional Molybdenum
A variable-pressure constant-volume method was employed to determine the gas permeation
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2015 S.1. Gas permeation experiments A variable-pressure constant-volume method was employed to
Electronic Supplementary Information (ESI)
Electronic Supplementary Material (ESI) for Journal of Materials Chemistry A. This journal is The Royal Society of Chemistry 2018 Electronic Supplementary Information (ESI) Hierarchically porous Mo-doped
New low temperature technologies of natural gas processing
New low temperature technologies of natural gas processing Salavat Imaev, Vasily Borisov, Sergey Bordachev, ENGO Engineering, Ltd. Abstract Over the past 10 years a number of companies have been working
Phytochemical Investigations on Tribulus longipetalus
Asian Journal of Chemistry; Vol., No. (0), 0-00 http://dx.doi.org/0./ajchem.0. Phytochemical Investigations on Tribulus longipetalus MUHAMMAD IMRAN ANJUM,, EJAZ AHMED,*, AHSAN SHARIF, ABDUL JABBAR, ABDUL
Supporting Information. In-Situ Facile Bubble-Templated Fabrication of New-Type Urchin-Like (Li, Mo)- Doped Lix(Mo0.3V0.7)2O5 for Zn 2+ Storage
Electronic Supplementary Material (ESI) for Journal of Materials Chemistry A. This journal is The Royal Society of Chemistry 2017 Supporting Information In-Situ Facile Bubble-Templated Fabrication of New-Type
Modeling Approaches to Increase the Efficiency of Clear-Point- Based Solubility Characterization
Modeling Approaches to Increase the Efficiency of Clear-Point- Based Solubility Characterization Paul Larsen, Dallin Whitaker Crop Protection Product Design & Process R&D OCTOBER 4, 2018 TECHNOBIS CRYSTALLI
HORIBA Scientific offers many types of training courses tailored to your particular requirements: A la carte training courses at our approved HORIBA Scientific training center. Learn and share your experience
Flexible porous coordination polymers constructed by 1,2-bis(4-pyridyl)hydrazine via solvothermal in situ reduction of 4,4 -Azopyridine
Supporting information Flexible porous coordination polymers constructed by 1,2-bis(4-pyridyl)hydrazine via solvothermal in situ reduction of 4,4 -Azopyridine Xiao-Min Liu, Lin-Hua Xie, Jian-Bin Lin, Rui-Biao
The Nature of Light. Light behaves like a special kind of wave, called an electromagnetic wave.
Notes_1_SNC2DE_09-10 The Nature of Light Light is a form of energy. Light is the only form of energy that can travel like a wave through empty space and through some materials. Light behaves like a special
Zhao Bao Tai Chi Kung Fu (English/Chinese Edition) (English And Chinese Edition) By Wayne Peng
Zhao Bao Tai Chi Kung Fu (English/Chinese Edition) (English And Chinese Edition) By Wayne Peng If you are searching for a ebook Zhao Bao Tai Chi Kung Fu (English/Chinese Edition) (English and Chinese Edition)
Coupling and Analysis of 981 Deep Water Semi-submersible. Drilling Platform and the Mooring System
4th International Conference on Renewable Energy and Environmental Technology (ICREET 2016) Coupling and Analysis of 981 Deep Water Semi-submersible Drilling Platform and the Mooring System XuDong Wang1,
User guide for the NMR spectrometer AVA300
1 User guide for the NMR spectrometer AVA300 Dear User! You are using a highly frequented NMR spectrometer, which has been installed in 2002. About 26000 spectra are measured here per year. Please respect
2014. Multistage throttling characteristics of reverse direction impact of pilot operated check valve
214. Multistage throttling characteristics of reverse direction impact of pilot operated check valve Lei Liu 1, Jiyun Zhao 2 School of Mechanical and Electrical Engineering, China University of Mining
CHAPTER 68. RANDOM BREAKING WAVES HORIZONTAL SEABED 2 HANS PETER RIEDEl. & ANTHONY PAUL BYRNE
CHAPTER 68 RANDOM BREAKING WAVES HORIZONTAL SEABED 2 HANS PETER RIEDEl. & ANTHONY PAUL BYRNE ABSTRACT According to wave theories the depth limited wave height over a horizontal seabed has a wave height
Supporting Information. Mitigating the P2 O2 phase transition of high-voltage
Electronic Supplementary Material (ESI) for Journal of Materials Chemistry A. This journal is The Royal Society of Chemistry 2019 Supporting Information Mitigating the P2 O2 phase transition of high-voltage
Figure Vapor-liquid equilibrium for a binary mixture. The dashed lines show the equilibrium compositions.
Another way to view this problem is to say that the final volume contains V m 3 of alcohol at 5.93 kpa and 20 C V m 3 of air at 94.07 kpa and 20 C V m 3 of air plus alcohol at 100 kpa and 20 C Thus, the
noble-metal-free hetero-structural photocatalyst for efficient H 2
Electronic Supplementary Material (ESI) for Journal of Materials Chemistry A. This journal is The Royal Society of Chemistry 2017 Ni 12 P 5 nanoparticles embedded into porous g-c 3 N 4 nanosheets as a
High performance carbon nanotube based fiber-shaped. supercapacitors using redox additives of polypyrrole and. hydroquinone
Electronic Supplementary Material (ESI) for Journal of Materials Chemistry A. This journal is The Royal Society of Chemistry 2015 Supporting information High performance carbon nanotube based fiber-shaped
Thermo Scientific Model 146i Principle of Operation
Thermo Scientific Model 146i Principle of Operation The Model 146i Multi-gas Calibrator dilutes calibration gases to precise concentrations. The diluted gases are used to perform zero, precision and Level
Heat Transfer Research on a Special Cryogenic Heat Exchanger-a Neutron Moderator Cell (NMC)
Purdue University Purdue e-pubs International Refrigeration and Air Conditioning Conference School of Mechanical Engineering 2010 Heat Transfer Research on a Special Cryogenic Heat Exchanger-a Neutron
Supplementary Information. High areal capacity lithium sulfur battery cathode by. site-selective vapor infiltration of hierarchical
Electronic Supplementary Material (ESI) for Nanoscale. This journal is The Royal Society of Chemistry 2017 Supplementary Information High areal capacity lithium sulfur battery cathode by site-selective
Supporting Information
Copyright WILEY VCH Verlag GmbH & Co. KGaA, 69469 Weinheim, Germany, 2016. Supporting Information for Adv. Energy Mater., DOI: 10.1002/aenm.201502539 From Hollow Carbon Spheres to N-Doped Hollow Porous
2.830J / 6.780J / ESD.63J Control of Manufacturing Processes (SMA 6303) Spring 2008
MIT OpenCourseWare http://ocw.mit.edu 2.830J / 6.780J / ESD.63J Control of Manufacturing Processes (SMA 6303) Spring 2008 For information about citing these materials or our Terms of Use, visit: http://ocw.mit.edu/terms.
2013 Australian open women s singles champion and runner-up technical and tactics features research based on mathematical statistic analysis
ISSN : 0974-7435 Volume 0 Issue 3 BTAIJ, 0(3), 04 [6-60] 03 Australian open women s singles champion and runner-up technical and tactics features research based on mathematical statistic analysis Feng
Supporting Information
Electronic Supplementary Material (ESI) for Journal of Materials Chemistry A. This journal is The Royal Society of Chemistry 2017 Supporting Information Metal-organic framework-derived CoSe2/(NiCo)Se2