Background Statement for SEMI Draft document 4657B NEW STANDARD: SPECIFICATIONS FOR TUNGSTEN HEXAFLUORIDE (WF 6 )
|
|
- Benjamin Jonas Stewart
- 5 years ago
- Views:
Transcription
1 Background Statement for SEMI Draft document 4657B NEW STANDARD: SPECIFICATIONS FOR TUNGSTEN HEXAFLUORIDE (WF 6 ) Note: This background statement is not part of the balloted item. It is provided solely to assist the recipient in reaching an informed decision based on the rationale of the activity that preceded the creation of this document. Note: Recipients of this document are invited to submit, with their comments, notification of any relevant patented technology or copyrighted items of which they are aware and to provide supporting documentation. In this context, patented technology is defined as technology for which a patent has issued or has been applied for. In the latter case, only publicly available information on the contents of the patent application is to be provided. The Gases Committee has been combining the common SEMI Gases into single specifications to make it an orderly and efficient way that would facilitate ease of use or reference. The committee took advantage of the common traits in all the existing specifications to reduce the total volume of specs and to reinforce their commonalities. In the past ballot cycles, the committee has successfully combined Oxygen, Hydrogen and Nitrogen gases below SEMI C , SPECIFICATIONS AND GUIDELINES FOR OXYGEN SEMI C , SPECIFICATIONS AND GUIDELINES FOR HYDROGEN SEMI C , SPECIFICATIONS AND GUIDELINES FOR NITROGEN In a continuing process, this ballot proposal is to combine SEMI C SPECIFICATION FOR TUNGSTEN HEXAFLUORIDE (WF6) IN CYLINDERS, 99.8% QUALITY and SEMI C STANDARD FOR TUNGSTEN HEXAFLUORIDE, % QUALITY In this document, the committee carried out the following steps: First, new Purpose, Scope sections and other mandatory sections were added to the ballot. Its purpose is to modify the titles of the combine standards for a given gases into a single stand-alone specification. This is being accomplished as follows: 1) Collect and group all gases standards and combined into one specification for each gases that includes all grades. 2) Combine all relevant gases tables into a single table in the consolidated specification 3) Re-designate the combined specifications with a single designation (C3.xx) for each gas. 4) Reference the previous SEMI designation numbers (C3.yy) for grades at the top of each column in the table. This involves reformatting the standards, updating any technical information, format according to SEMI editorial guidelines, and obtaining approval of the committee by balloting. NOTE: If this ballot is approved, SEMI C3.26 and C3.52 will be submitted for withdrawal in subsequent meeting. The results of this ballot will be reviewed and adjudicated by NA Facilities and Gases Committee during their meetings late March 2011 in San Jose, CA. Check for the latest meeting schedule. For question on the ballot, contact SEMI Staff, Kevin Nguyen at knguyen@semi.org
2 SEMI Draft Document 4657B NEW STANDARD: SPECIFICATIONS FOR TUNGSTEN HEXAFLUORIDE (WF 6 ) 1 Purpose 1.1 The purpose of this document is to provide specifications for tungsten hexafluoride (WF 6 ) that are used in the semiconductor industry. 2 Scope 2.1 This document covers requirements for tungsten hexafluoride used in the semiconductor industry. NOTICE: SEMI Standards and Safety Guidelines do not purport to address all safety issues associated with their use. It is the responsibility of the users of the documents to establish appropriate safety and health practices, and determine the applicability of regulatory or other limitations prior to use. 3 Description 3.1 Tungsten hexafluoride is a colorless gas or colorless liquid. It is shipped as a liquefied gas under its own vapor pressure. 4 Limitations 4.1 None 5 Referenced Standards and Documents 5.1 SEMI Standards SEMI C1 Guide for the Analysis of Liquid Chemicals SEMI C3 Specifications for Gases SEMI C10 Guide for Determination of Method Detection Limits NOTICE: Unless otherwise indicated, all documents cited shall be the latest published versions. 6 Terminology 6.1 Terminology appropriate to this standard is defined in SEMI C3. 7 Requirements 7.1 Purity and other requirements for tungsten hexafluoride are given in Table 1. Page 1 Doc. 4657B SEMI
3 Table 1 Impurity and Other Requirements for Tungsten Hexafluoride (WF 6 ) Previous SEMI Reference # C (Specification) C (Specification) Grade 99.9% % Impurities Maximum Acceptable Level (ppm) #1 Carbon Tetrafluoride (CF 4 ) 10 1 Carbon Dioxide (CO 2 ) -- 1 Carbon Monoxide (CO) -- 1 Hydrogen Fluoride (HF) Nitrogen (N 2 ) 50 5 Oxygen (O 2 ) + Argon (Ar) 50 1 Sulfur Hexafluoride (SF 6 ) 10 1 Silicon Tetrafluoride (SiF 4 ) 10 1 TOTAL LISTED IMPURITIES Impurities Maximum Acceptable Level (ppm w) Cobalt (Co) & Manganese (Mn) Lead (Pb) -- Chromium (Cr), Zinc (Zn), & Uranium (U) Calcium (Ca) & Magnesium (Mg) Nickel (Ni), Copper (Cu), Sodium (Na), & Potassium (K) Iron (Fe) -- Thorium (Th) -- Molybdenum (Mo) #1: An analysis of significant figures has not been considered. The number of significant figures will be based on analytical accuracy and the precision of the provided procedure. 8 Properties of Tungsten Hexafluoride (WF 6 ) Table 2 Properties of Tungsten Hexafluoride (for information only) Metric Units US Units CAS # Molecular weight Boiling point at 1 atm 17.1 C 62.8 F Density of gas at 22.8 C (73 F) and 1 atm 12.9 kg/m lb/ft 3 Specific gravity of gas Density of liquid at boiling point 3440 kg/m lb/ft 3 9 Analytical Procedures for Tungsten Hexafluoride, 99.9% Purity 9.1 Nitrogen and Oxygen + Argon This procedure is for the determination of nitrogen and oxygen + argon in tungsten hexafluoride using a gas chromatograph with a thermal conductivity detector. Page 2 Doc. 4657B SEMI
4 9.1.1 Detection Limits 10 ppm (mol/mol) nitrogen, and 10 ppm (mol/mol) oxygen + argon Instrument Parameters Columns: (See Figures 1, 2) Column 1: Porapak S, 80/100 mesh, 1.5 m (5 ft) by 6.4 mm (1/4 in) OD, 5.1 mm (0.2 in) ID, ss or equivalent. Column 2: Molecular sieve 5A, 80/100 mesh, 1.8 m (6 ft) by 4.8 mm (3/16 in) OD, 3.7 mm (0.147 in) ID, ss or equivalent Column Flow: 30 ml/min helium Sample Volume: 2 ml Temperatures Detector: 70 C Column: 40 C Calibration Standard 50 ppm (mol/mol) nitrogen, 50 ppm (mol/mol) oxygen, balance helium Operating Procedures Determine the times for valve switching and signal changes, and enter into the run table. An example of a run table follows. Table 3 Example of a Run Time Position Function 0 min. 1 Purge sample through loop. Backflush Porapak column. Connect MS column to the TCD. 1 min. 2 Inject sample onto Porapak column. Allow oxygen + argon and nitrogen to elute from the Porapak column to the MS column. Sequentially elute the oxygen + argon and nitrogen from the MS column to the TCD. 4 min. 1 Backflush Porapak column to vent for 8 minutes Set the valves in Position 1 (Figure 1) Flow the calibration standard through the 10-port valve. Analyze standard using the conditions described above. Record retention times and peak areas Flow the sample to be tested through the 10-port valve for 1 minute. Analyze in the same manner as in The standard is again run as in Calculate the concentrations of nitrogen and oxygen + argon in the sample, using the formula below. The result may not exceed the specifications in table 1 of this Standard. Sample Peak Area Standard Peak Area Concentration of Standard = Concentration of Sample (1) 9.2 Carbon Tetrafluoride, Hydrogen Fluoride, Silicon Tetrafluoride, and Sulfur Hexafluoride This procedure is for the determination of these gases in tungsten hexafluoride using infrared spectrophotometry. NOTE 1: Actual detection limits will be determined by the noise level and the resolution of the spectrometer. One way is to reduce the noise level is to use a Fourier Transform Infrared Spectrometer Detection Limits 10 ppm (mol/mol) carbon tetrafluoride, 1000 ppm (mol/mol) hydrogen fluoride, 10 ppm (mol/mol) silicon tetrafluoride and 10 ppm (mol/mol) sulfur hexafluoride. Page 3 Doc. 4657B SEMI
5 9.2.2 Instrument Parameters Cell path length: 10 cm Sample Cell Pressure: 1 atmosphere Wavenumbers: Table 4 Wavenumber of Chemicals Component Wavenumber (cm -1 ) Carbon Tetraflouride (CF 4 ) 1283 Hydrogen Fluoride (HF) 4076 Silicon Tetrafluoride (SiF 4 ) 1029 Sulfur Hexafluoride (SF 6 ) Calibration Standards 1% (mol/mol) hydrogen fluoride in tungsten hexafluoride, 20 ppm (mol/mol) silicon tetrafluoride in nitrogen, 20 ppm (mol/mol) each carbon tetrafluoride and sulfur hexafluoride in nitrogen Operating Procedures Flow each calibration gas through the system for 1 minute. Pressurize the cell to 1 atmosphere. Record the absorbance of each calibration standard at the wavenumber listed in Flow the sample gas through the system for 1 minute. Pressurize the cell to 1 atmosphere. Record the absorbance at each of the appropriate wavenumbers. Calculate the concentration of each gas, using the formula below. The results may not exceed the specification in table 1 of this standard. Measured Absorbance of the Sample Measured Absorbance of the Standard Concentration Concentration = of Standard of Sample (2) NOTE 2: Tungsten hexafluoride interferes with the direct absorbance reading for silicon tetrafluoride. The absorbance for silicon tetrafluoride is determined by compensating for the interfering absorbance from the tungsten hexafluoride. Compensation is made by subtracting the absorbance contributed to this band by tungsten hexafluoride band at 930 cm -1. This absorbance is halved and subtracted from the total peak absorbance at 1040 cm -1, resulting in the peak absorbance for silicon tetrafluoride. NOTE 3: Actual detection limits will be determined by the noise level and the resolution of the spectrometer. One way is to reduce the noise level is to use a Fourier Transform Infrared Spectrometer. NOTE 4: All gases used in the analysis of the sample should not contain more than 10% of the specified value of the component of interest, unless otherwise stated. NOTE 5: As tungsten hexafluoride has a low vapor pressure, the cylinder should be kept at room temperature (20 C) for at least 8 hours prior to analysis. NOTE 6: Observe proper safety procedures for handling and disposing of tungsten hexafluoride. NOTE 7: Prior to introducing tungsten hexafluoride purge the sample lines and instrument tubing with helium to remove moisture. NOTE 8: Upon completing the analysis, cap off the manifold and instrument lines or purge the system with helium. Page 4 Doc. 4657B SEMI
6 Figure 1 Setup for Position 1 Helium Carrier Porapak Column Vent MS5A Column Sample Out Sample In T.C. DET Position Position 2: 1: V1 Sample is turned is purging through loop Sample Porapak flows S column through is backflushing sample loop to the Porapak MS5A column S column connected and then to to detector MS5A column Figure 2 Setup for Position 2 Page 5 Doc. 4657B SEMI
7 10 Analytical Procedures for Tungsten Hexafluoride, % Purity NOTE 9: All gases used in the analysis of the sample should contain not more than 10% of the specified value of the component of interest unless otherwise specified Carbon Tetrafluoride, Silicon Tetrafluoride, Carbon Dioxide, and Sulfur Hexafluoride This procedure is for the determination of carbon tetrafluoride, silicon tetrafluoride, carbon dioxide, and sulfur hexafluoride in tungsten hexafluoride using a gas chromatograph equipped with a helium ionization detector. A backflush is used in order to protect the detector from the main component Detection Limits 0.3 ppm (mole/mole) carbon tetrafluoride, 1 ppm (mole/mole) silicon tetrafluoride, 0.1 ppm (mole/mole) carbon dioxide, and 0.5 ppm (mole/mole) sulfur hexafluoride Instrument Parameters Columns: Column 1: 10% Kel F Nr10 on Chromosorb T, 4.0 m (13 ft) by 3.2 mm (1/8 in) nickel or equivalent, Column 2: Preconditioned HAYESEP Q, 60/80 mesh, 3 m (10 ft) by 3.2 mm (1/8 in) or equivalent. The column should be treated by repeated WF 6 sample injections at 125 C Carrier Flow 26 ml/min helium, 6.0 grade Temperatures: Detector: 50 C Column Oven: 50 C Sample Volume 2 ml Calibration Standards 1 and 2 ppm (mole/mole) carbon tetrafluoride, carbon dioxide, and sulfur hexafluoride in helium (see Figures 3 and 4). 2 ppm silicon tetrafluoride in helium or permeation device (see Figure 5) Operating Procedure Attach a suitable pressure regulator to the standard cylinders. Connect the regulator to the dedicated WF 6 handling system which is connected to the chromatographic sampling valve Purge the sampling lines with the standard for at least one minute Inject the standard into the gas chromatograph. Record the retention times and peak areas. Order of elution for the above mentioned standard is carbon tetrafluoride, silicon tetrafluoride, carbon dioxide, and sulfur hexafluoride Inject the WF 6 sample to be analyzed in the same manner as the calibration standard. Record the retention times and peak areas Compare the average peak areas of the calibration standard to that of the detected peak in tungsten hexafluoride. Calculate the concentration of each impurity using the standard and sample peak areas and the standard concentration. The results may not exceed the specifications in table Oxygen and Argon, Nitrogen, and Carbon Monoxide This procedure is for the determination of oxygen and argon, nitrogen, and carbon monoxide in tungsten hexafluoride using a gas chromatograph equipped with a helium ionization detector. A backflush is used in order to protect the detector from the main component Detection Limits 5 ppm (mol/mol) oxygen + argon, 5 ppm (mol/mol) nitrogen, and 1 ppm (mol/mol) carbon monoxide Instrument Parameters Page 6 Doc. 4657B SEMI
8 Columns: Column 1: 10% Kel F Nr 10 on Chromosorb T, 4.0 m (13 ft) by 3.2 mm (1/8 in) nickel or equivalent. Column 2: Preconditioned HAYESEP Q, 60/80 mesh, 3 m (10 ft) by 3.2 mm (1/8 in) or equivalent. The columns should be treated by repeated WF 6 sample injections at 125 C. Column 3: Molecular sieve 5 A, 60/80 mesh, 2 m (6 ft) by 3.2 mm (1/8 in) Carrier Flow 26 ml/min helium, 6.0 grade Temperatures: Detector: 50 C Column Oven: 50 C Sample Volume 2 ml Calibration Standards 1 and 2 ppm (mole/mole) oxygen, nitrogen, and carbon monoxide in helium (see Figure 6) Operating Procedure Attach a suitable pressure regulator to the standard cylinder. Connect the regulator to the dedicated WF 6 handling system, which is connected to the chromatographic sampling valve Purge the sampling lines with the standard for at least one minute Inject the standard into the gas chromatograph. Switch the valves in order to operate in the same conditions as the WF 6 sample analysis. Record the retention times and peak areas. Order of elution for the above mentioned standard is oxygen and argon, nitrogen, and carbon monoxide Inject the WF 6 sample in the same manner as the calibration standard. Record the retention times and peak areas Compare the average peak areas of the calibration standard to that of the detected peak in the tungsten hexafluoride. Calculate the concentration of each impurity using the standard and sample areas and the standard concentration. The results may not exceed the specifications in table Hydrogen Fluoride This procedure is for the determination of hydrogen fluoride in tungsten hexafluoride using Fourier Transform Infra Red (FTIR) analyzer Detection Limit 0.5 ppm (mole/mole) Instrument Parameters cell with CaF 2 windows HF band: 4038,8 cm -1 resolution: 2 cm -1 path length: 12 cm Calibration Standard ppm (mol/mol) hydrogen fluoride. Calibrate with low vapor pressure hydrogen fluoride or permeation device Operating Procedure Carefully dry the cell before sampling tungsten hexafluoride. Then purge it with tungsten hexafluoride and record the concentration. When it is steady, that means the line is purged and the true hydrogen fluoride concentration is obtained Elemental Impurities This procedure is for the determination of Ca, Co, Cr, Cu, Fe, K, Mg, Mn, Mo, Na, Ni, Pb, Th, U, and Zn in the nonvolatile residue of liquid phases tungsten hexafluoride (WF 6 ) and analyzed by Inductively Coupled Plasma Mass Spectrometry (ICPMS). Page 7 Doc. 4657B SEMI
9 Detection Limits (ppb wt/wt) Ca: 1.5; Co: 0.1; Cr: 0.8, Cu: 0.5; Fe: 1; K: 1.5; Mg: 0.1, Mn: 0.1, Mo: 0.5; Na: 0.6; Ni: 1; Pb: 0.1; Th, U: 0.01; and Zn: Sampling Apparatus Figure 7 shows the sampling apparatus used for obtaining a liquid phase sample of WF 6. The sampling apparatus consists of: Cylinder Inverter, PFA Vessels, PFA Valves, and PFA Tubing. The whole sampling system is placed inside a hood Water At least 18 MΩ DI water should be used for all dilutions, blanks, and washing Reagents All reagents are of the highest purity available minimizing background metal contamination. The following reagents are needed to prepare the sample and standards: Aqueous Ammonia, Aqueous HNO 3, Aqueous HF, and NIST traceable ICP standards Sampling Liquid Tungsten Hexafluoride Place about 400 ml of DI water in each of the hydrolysis vessels. Obtain the weight of each of the hydrolysis vessels Assemble the apparatus as shown in Figure 3. Do not tighten the cylinder CGA connection. All PFA parts should be clean and dried prior to assembly Open valves V2, V3, V4 and V5. Set the house nitrogen pressure to approximately 15 psig (205 kpa). Purge the system with nitrogen for about 15 minutes. TIGHTEN THE CYLINDER CGA CONNECTION Close V2. The system should now be under pressure. Check for leaks and repair if necessary Open V1 and evacuate the system for approximately 10 minutes Close all valves Fill sample vessel by opening cylinder valve and valve V5. Fill the sample vessel approximately 2/3 full. Close cylinder valve Close V5. Open V2, V4, and V6. This will carry the WF 6 vapors to the hydrolysis vessel Purge the system with nitrogen for a few minutes after the WF 6 liquid in the sample cup has totally evaporated Close all valves. Remove the hydrolysis vessels and weigh the vessels The weight gain in the hydrolysis vessel will give the weight of the sampled WF 6. Typically the weight gain of the second and third vessels will be less than 1% of the weight gain of the first hydrolysis vessel Remove the sample vessel and dissolve the residue Sample Preparation Add 20 ml DI water to a 100 ml volumetric flask Open the sample cup and add 5 ml of aqueous ammonia to the cup Swirl in the cup and place in a 100 ml volumetric flask. Page 8 Doc. 4657B SEMI
10 Add 5 ml Nitric Acid to the cup Swirl and place in the same 100 ml volumetric flask Add 5 ml Hydrofluoric Acid to the cup Swirl and place in the same 100 ml volumetric flask as before Dilute the solution with DI water up to the mark of the 100 ml volumetric flask Analyze for metals in the sample ICPMS Analysis Procedure This procedure is used to analyze for trace Na, K, Cr, Fe, Th and U using multi point calibration. Other elements can be analyzed using a single point calibration. Elements for which stable standards can not be obtained, can be analyzed using interpolation and a knowledge of the instrument response function. The ICPMS should be calibrated using matrix matched multi-element standards. At least one spiked sample should be analyzed as part of the analytical procedure. The recovery of the spikes should be within ± 25%. At least three standards and a blank should be used for the calibration. Regression based approach should be used to calculate the response factors. The limit of detection (LOD) should be calculated following SEMI C10, Guide for Determination of Method Detection Limits The concentration of impurities in gas phase WF 6 is given by Conc. in Solution Wt.of Solution Conc. in WF6 = (3) Weight of Sampled WF 6 Figure 3 CF 4 and SF 6 Standards in He Page 9 Doc. 4657B SEMI
11 Figure 4 CO 2 Standards in He Figure 5 SiF 4 Standard in He Page 10 Doc. 4657B SEMI
12 Figure 6 O 2, N 2, and CO Standards in He Page 11 Doc. 4657B SEMI
13 To Vent Hydrolysis Vessels Anti Suckback Vessel V6 V4 PFA Vessel Figure 7 Sampling System for WF 6 V5 V3 V2 V1 Vacuum Pump House Nitrogen NOTICE: SEMI makes no warranties or representations as to the suitability of the standards set forth herein for any particular application. The determination of the suitability of the standard is solely the responsibility of the user. Users are cautioned to refer to manufacturer s instructions, product labels, product data sheets, and other relevant literature respecting any materials or equipment mentioned herein. These standards are subject to change without notice. The user s attention is called to the possibility that compliance with this standard may require use of copyrighted material or of an invention covered by patent rights. By publication of this standard, SEMI takes no position respecting the validity of any patent rights or copyrights asserted in connection with any item mentioned in this standard. Users of this standard are expressly advised that determination of any such patent rights or copyrights, and the risk of infringement of such rights, are entirely their own responsibility. Page 12 Doc. 4657B SEMI
This standard is due for Five Year Review. This process is required by the SEMI Regulations to ensure that the standard is still valid.
Background Statement for SEMI Draft Document 5211 REVISION OF SEMI C3.58-0303 SPECIFICATION FOR OCTAFLUOROCYCLOBUTANE, C 4 F 8, ELECTRONIC GRADE IN CYLINDERS, 99.999% QUALITY Note: This background statement
More informationMETHOD 3C - DETERMINATION OF CARBON DIOXIDE, METHANE, NITROGEN, AND OXYGEN FROM STATIONARY SOURCES
METHOD 3C - DETERMINATION OF CARBON DIOXIDE, METHANE, NITROGEN, AND OXYGEN FROM STATIONARY SOURCES 1. Applicability and Principle 1.1 Applicability. This method applies to the analysis of carbon dioxide
More informationDetector Carrier Gas Comments Detector anode purge or reference gas. Electron Capture Nitrogen Maximum sensitivity Nitrogen Argon/Methane
Gas requirements Gases for packed columns The carrier gas you use depends upon the type of detector and the performance requirements. Table 520-1 lists gas recommendations for packed column use. In general,
More information800.Keen.Gas
C 2 H 2 ACETYLENE Acetylene is a colorless and tasteless gas with a garlic-like odor. It is flammable and can be an asphyxiant. In order to prevent explosive decomposition, acetylene is supplied in cylinders
More informationCommercial Practice Test Method Internal Vapor Analysis of Hermetic Devices
Commercial Practice Test Method Internal Vapor Analysis of Hermetic Devices Oneida Research Services, Inc. 8282 Halsey Road Whitesboro, NY 13492 Phone: (315) 736-5480 FAX: (315) 736-9321 1.0 Purpose The
More informationSUBSTATION MAINTENANCE ELECTRICAL OPERATING PROCEDURE
Page 1 of 6 A. PURPOSE AND SCOPE This procedure establishes safe working practices for handling sulfur hexafluoride (SF 6 ) gas and release minimization practices. This document also specifies methods
More informationPERFORMANCE SPECIFICATION PROPELLANT, HYDROGEN
METRIC 17 May 2013 SUPERSEDING MIL-PRF-27201D 07 February 2007 PERFORMANCE SPECIFICATION PROPELLANT, HYDROGEN This specification is approved for use by all Departments and Agencies of the Department of
More informationGaseous oxygen technical grade Specification
CDC 09 (5010) P3 Rev. TZS 217:1984 FINALIZED TANZANIA STANDARD Gaseous oxygen technical grade Specification TANZANIA BUREAU OF STANDARDS. 2 nd edition TBS 2017 0. FOREWORD 0.1. This Tanzania Draft Standard
More informationSvensk läkemedelsstandard
Svensk läkemedelsstandard 2018.2 Nitrogen Postadress/Postal address: P.O. Box 26, SE-751 03 Uppsala, SWEDEN Besöksadress/Visiting address: Dag Hammarskjölds väg 42, Uppsala Telefon/Phone: +46 (0)18 17
More informationVIC offers a variety of Calibrated Gas Leaks
CALIBRATED GAS LEAKS VIC offers a high quality line of calibrated gas leaks traceable to National Institute of Standards Technology (NIST). Calibrated gas leaks are used to provide a controlled delivery
More informationGases&Technology. Measurement of Impurities in Helium Using the Dielectric Barrier Discharge Helium Ionization Detector. FEATURE.
Gases&Technology FEATURE Measurement of Impurities in Helium Using the Dielectric Barrier Discharge Helium Ionization Detector. B Y M A T T H E W M O N A G L E Abstract Bulk gases are often delivered to
More informationSupporting Information for Micro-Collection of. Gases in a Capillary Tube: Preservation of Spatial
Supporting Information for Micro-Collection of Gases in a Capillary Tube: Preservation of Spatial and Temporal Resolution AUTHOR INFORMATION Kristin A. Herrmann Favela, 1 * Pieter Tans, 2 Thomas Jaeckle,
More informationAPPLICATION NOTE. GC Integrated Permeation Device
GC Integrated Permeation Device GC-integrated Design PPB to PPM Level Calibration No Cylinders or Regulators Required Option for Dual Ovens Cost Effective, Safe, Clean, Flexible, NIST Traceable Keywords:
More informationLaboratory Hardware. Custom Gas Chromatography Solutions WASSON - ECE INSTRUMENTATION. Engineered Solutions, Guaranteed Results.
Laboratory Hardware Custom Gas Chromatography Solutions Engineered Solutions, Guaranteed Results. WASSON - ECE INSTRUMENTATION Laboratory Hardware Wasson-ECE Instrumentation offers hardware-only solutions
More informationPERFORMANCE SPECIFICATION PROPELLANT PRESSURIZING AGENT, NITROGEN
METRIC 07 August 2013 SUPERSEDING MIL-PRF-27401F 10 January 2008 PERFORMANCE SPECIFICATION PROPELLANT PRESSURIZING AGENT, NITROGEN Comments, suggestions, or questions on this document should be addressed
More informationLaboratory Hardware. Custom Gas Chromatography Solutions WASSON - ECE INSTRUMENTATION. Custom solutions for your analytical needs.
Laboratory Hardware Custom Gas Chromatography Solutions Custom solutions for your analytical needs. Laboratory Hardware Wasson-ECE Instrumentation offers hardware-only solutions for advanced chromatography
More informationASTM 3612/TOGA/Dissolved Gas GC Revised October 2013
The SRI ASTM 3612/TOGA/ Dissolved Gas GC configuration ( TOGA GC ) permits measurement of gasses dissolved in water, oil or other liquids, and is based on the requirements of ASTM method 3612, option C,
More informationISO INTERNATIONAL STANDARD
INTERNATIONAL STANDARD ISO 16017-1 First edition 2000-11-15 Indoor, ambient and workplace air Sampling and analysis of volatile organic compounds by sorbent tube/thermal desorption/capillary gas chromatography
More informationDate of Shipment: Xxxxx 00, 20xx 3402c National Institute of Advanced Industrial Science and Technology National Metrology Institute of
Date of Shipment: Xxxxx 00, 20xx 3402c01151112-170831 National Metrology Institute of Japan Reference Material Certificate NMIJ CRM 3402-c01 Sulfur Dioxide This certified reference material (CRM) was produced
More informationGCMSD-Headspace Analysis SOP
Before you start GCMSD-Headspace Analysis SOP Method and Sequences names are restricted to 50 characters (MSD program will crash otherwise) The GC oven and Injection Ports need to be cooled to 50 oc to
More informationASTM WK Standard Test Method for Dissolved Gases. Anne Jurek Applications Chemist
ASTM WK 43267 Standard Test Method for Dissolved Gases Anne Jurek Applications Chemist Rationale Hydraulic Fracturing is becoming more and more common. Nearby water well can be affected during the fracking
More informationCORESTA RECOMMENDED METHOD Nº 67
CORESTA RECOMMENDED METHOD Nº 67 DETERMINATION OF WATER IN THE MAINSTREAM SMOKE OF CIGARS BY GAS CHROMATOGRAPHIC ANALYSIS (November 2005) 1. FIELD OF APPLICATION The method is applicable to the particulate
More informationISO INTERNATIONAL STANDARD
INTERNATIONAL STANDARD ISO 6974-4 First edition 2000-04-01 Natural gas Determination of composition with defined uncertainty by gas chromatography Part 4: Determination of nitrogen, carbon dioxide and
More informationMultiple Gas#5 GC configuration Jan 2016
History: Unfortunately there is no single column that can separate: Hydrogen Oxygen Nitrogen Methane CO CO2 Ethane Water Propane Butane Pentane Over the years SRI Instruments has devised several solutions
More informationTitle: Standard Operating Procedure for Measurement of Ethylene (C 2 H 4 ) in Ambient Air by Reduced Gas Detection (RGD)
Procedure No: SOP-026 Revision No: 1.0 January 24, 2011 Page No.: 1 of 10 1. INTRODUCTION AND SCOPE To obtain timely data for the purpose of air quality assessment, air quality trend reporting and to meet
More informationGas Mixture Two Components. Gas Mixtures Two Components
Gas Mixture Two Components Two Components Contents Two-Component Mixtures Ammonia...M4 Argon...M5 Benzene...M6 n-butane...m7 Carbon Dioxide...M8 Carbon Monoxide...M10 Chlorine...M12 Ethane...M13 Ethylene
More informationHigh-purity gases. Customer-oriented offering highest quality
High-purity gases Customer-oriented offering highest quality From A for argon to X for xenon, Messer offers an extensive range of high-purity gases. This ranges from the air gases (nitrogen, oxygen and
More informationAdvancements in Gas Chromatography Analyzers - Keeping up with New Technology. Chuck Runkle Gas Phase Product Specialist ASTS June 2013
Advancements in Gas Chromatography Analyzers - Keeping up with New Technology Chuck Runkle Gas Phase Product Specialist ASTS June 0 Capillary Flow Technology -- solves difficult application problems easily
More informationSTANDARD OPERATING PROCEDURES
PAGE: 1 of 9 CONTENTS 1.0 SCOPE AND APPLICATION 2.0 METHOD SUMMARY 3.0 SAMPLE PRESERVATION, CONTAINERS, HANDLING AND STORAGE 3.1 Canister Receipt 3.2 Canister Storage 4.0 INTERFERENCE AND POTENTIAL PROBLEMS
More informationAutomated Determination of Dissolved Gases in Water Anne Jurek. Abstract: Discussion:
Automated Determination of Dissolved Gases in Water Anne Jurek Abstract: The RSK-175 standard operating procedure was developed in order to determine the amount of dissolved gas in water. Due to the expansion
More informationAppendix D: SOP of INNOVA 1412 Photoacoustic Multi-Gas Monitor. Description and Principle of Operation
Page 1 of 19 : SOP of INNOVA 1412 Photoacoustic Multi-Gas Monitor Description and Principle of Operation The photoacoustic multi-gas monitor (INNOVA 1412, Innova AirTech Instruments, Denmark) is a highly
More informationPERFORMANCE SPECIFICATION PROPELLANT PRESSURIZING AGENT, ARGON
METRIC 07 August 2013 SUPERSEDING MIL-PRF-27415B 08 February 2007 PERFORMANCE SPECIFICATION PROPELLANT PRESSURIZING AGENT, ARGON Comments, suggestions, or questions on this document should be addressed
More information(2 pts) Draw the line of best fit through the data and estimate the concentration of Fe in your sample solution.
Name: 1. You are asked to measure the percent iron in a steel sample you believe to be about 50% Fe by mass. You dissolve four replicate samples in nitric acid and dilute them by mass to a concentration
More informationGenerating Calibration Gas Standards
Technical Note 1001 Metronics Inc. Generating Calibration Gas Standards with Dynacal Permeation Devices Permeation devices provide an excellent method of producing known gas concentrations in the PPM and
More informationMajor Design Features
Major Design Features 3Flex Features Design Benefits Discussion 316 SS fittings and pneumatically actuated, hard-seal valves Provides virtually leak-free gas management with the lowest outgassing rate
More informationSuperior Result from Analytical Instruments The constant purity of the nitrogen improves system stability and ensures reproducible results
Nitrogen Generator Whisper-N2 Series Features Membrane Technology Superior Result from Analytical Instruments The constant purity of the nitrogen improves system stability and ensures reproducible results
More informationDevelopment of DMS and Acetonitrile, and Formaldehyde gas standards. Gwi Suk Heo, Yong Doo Kim, Mi-Eon Kim, and Hyunjin Jin
Development of DMS and Acetonitrile, and Formaldehyde gas standards Gwi Suk Heo, Yong Doo Kim, Mi-Eon Kim, and Hyunjin Jin The amount of chemical substances in cylinder container Purity uncertainty Gravimetry
More informationTitle: Standard Operating Procedure for Dasibi Model 5008 Gas Dilution Calibrator
Procedure No: SOP-034 Revision No: 1.0 Revised Dec. 29, 2010 Page No.: 1 of 10 1. INTRODUCTION AND SCOPE This procedure is intended to describe the operations of the Dasibi model 5008 calibrator. The Dasibi
More informationSTANDARD OPERATING PROCEDURES
PAGE: 1 of 14 CONTENTS 1.0 SCOPE AND APPLICATION 2.0 METHOD SUMMARY 3.0 SAMPLE PRESERVATION, CONTAINERS, HANDLING AND STORAGE 4.0 INTERFERENCE AND POTENTIAL PROBLEMS 5.0 EQUIPMENT/APPARATUS 6.0 REAGENTS
More informationGases and welding distributors continue
Specialty Gas Instrumentation By Ray Borzio, Mike Lee, and Scott Varian Gases and welding distributors continue to have a significant future in the production, delivery, and related services for specialty
More informationacrolein, acetaldehyde and acetone( cm -1 ); methanol (1306 cm -1 ); ethylene (949 cm -1 ); and isoprene (893 cm -1 ).
acrolein, acetaldehyde and acetone(1550 1800 cm -1 ); methanol (1306 cm -1 ); ethylene (949 cm -1 ); and isoprene (893 cm -1 ). 5 Figure 4a 6 Figure 4b Figure 4c 7 Figure 5 Questions in Student Handout
More informationAlkylphosphines. Storage and Handling Recommendations
Alkylphosphines Storage and Handling Recommendations 2 The Phosphine Specialties Group has been producing phosphine and phosphine derivatives on a large scale for a number of years and the handling procedures
More informationSvensk läkemedelsstandard
Svensk läkemedelsstandard 2019.0 Carbon dioxide Postadress/Postal address: P.O. Box 26, SE-751 03 Uppsala, SWEDEN Besöksadress/Visiting address: Dag Hammarskjölds väg 42, Uppsala Telefon/Phone: +46 (0)18
More informationREFINERY GAS ANALYSIS BY GAS CHROMATOGRAPHY
REFINERY GAS ANALYSIS BY GAS CHROMATOGRAPHY UOP Method SCOPE This automated method is for determining the composition of refinery gas samples or expanded liquefied petroleum gas (LPG) samples obtained
More informationSEMI E is due for its Five Year Review. This process is required by the SEMI Regulations to ensure that the standard is still valid.
Background Statement for SEMI Draft Document 4677 REAPPROVAL OF SEMI E66-1103 TEST METHOD FOR DETERMINING PARTICLE CONTRIBUTION BY MASS FLOW CONTROLLERS Note: This background statement is not part of the
More informationThis test shall be carried out on all vehicles equipped with open type traction batteries.
5.4. Determination of hydrogen emissions page 1 RESS-6-15 5.4.1. This test shall be carried out on all vehicles equipped with open type traction batteries. 5.4.2. The test shall be conducted following
More informationUltimate Performance in Gas Chromatography
Ultimate Performance in Gas Chromatography by Randall Bramston-Cook Lotus Consulting 5781 Campo Walk Long Beach, California 90803 310/569-0128 Fax 714/898-7461 Email ebramstoncook@msn.com August 7, 2007
More informationUser manual. TC-20 Sample conditioning and dry-purge rig. QUI-0003 Version 6.3 September
Version 6.3 September 2013 User manual TC-20 Sample conditioning and dry-purge rig Page 2 Contents 1. Introduction to the TC-20... 3 1.1 Tube conditioning... 3 1.2 Dry-purging... 3 2. Required services...
More informationDr. Rogers Chapter 5 Homework Chem 111 Fall 2003
Dr. Rogers Chapter 5 Homework Chem 111 Fall 2003 From textbook: 7-33 odd, 37-45 odd, 55, 59, 61 1. Which gaseous molecules (choose one species) effuse slowest? A. SO 2 (g) B. Ar(g) C. NO(g) D. Ne(g) E.
More informationCalcimeter Instruction Manual
Hohner (UK - Canada - Texas) Calcimeter Instruction Manual The Hohner Calcimeter is based on industry standard versions, and is used to measure the calcium carbonate and magnesium carbonate in samples.
More informationno peaks missing peaks too small peaks increasing retention decreasing retention
GC Troubleshooting We can help you. 1. Observation: no peaks no peaks missing peaks too small peaks increasing retention decreasing retention declining baseline rising baseline bleeding plateaus interfering
More informationGas Laws. 2 HCl(aq) + CaCO 3 (s) H 2 O(l) + CO 2 (g) + CaCl 2 (aq) HCl(aq) + NaHCO 3 (s) H 2 O(l) + CO 2 (g) + NaCl(aq)
Gas Laws Introduction: Although we cannot see gases, we can observe their behavior and study their properties. For example, we can watch a balloon filled with helium gas floating in air and conclude that
More informationDemystifying the Process of Calibrating your Thermal Desorption Gas Chromatography System using Compressed Gas Standards.
Demystifying the Process of Calibrating your Thermal Desorption Gas Chromatography System using Compressed Gas Standards. Jamie Brown R&D Scientist Supelco 595 North Harrison RD. Bellefonte, PA 16823 National
More informationMETHOD 204F--VOLATILE ORGANIC COMPOUNDS CONTENT IN LIQUID INPUT STREAM (DISTILLATION APPROACH) 1.1 Applicability. This procedure is applicable for
METHOD 204F--VOLATILE ORGANIC COMPOUNDS CONTENT IN LIQUID INPUT STREAM (DISTILLATION APPROACH) 1. INTRODUCTION 1.1 Applicability. This procedure is applicable for determining the input of volatile organic
More informationModel Description
LEAKHUNTER Plus LEAKHUNTER Plus Model 8066 Description The MATHESON LEAKHUNTER Plus is a truly universal leak detector. Extensive R&D has produced a multi-functional leak detector engineered to perform
More informationPharmaceutical Grade Nitrogen & Gardner Denver / CompAir PSA Nitrogen Gas Generation Systems
Pharmaceutical Grade Nitrogen & Gardner Denver / CompAir PSA Nitrogen Gas Generation Systems The purpose of this document is to clarify the specification for pharmaceutical grade nitrogen gas and confirm
More informationSvensk läkemedelsstandard
Svensk läkemedelsstandard 2017.2 Nitrous oxide Postadress/Postal address: P.O. Box 26, SE-751 03 Uppsala, SWEDEN Besöksadress/Visiting address: Dag Hammarskjölds väg 42, Uppsala Telefon/Phone: +46 (0)18
More informationHiQ laboratory gas generators.
Product information HiQ laboratory gas generators. The convenient alternative for laboratory environments. 02 HiQ laboratory gas generators HiQ laboratory gas generators. Designed with safety and convenience
More informationSpace product assurance
ECSS-Q-ST-70-29C Space product assurance Determination of offgassing products from materials and assembled articles to be used in a manned space vehicle crew compartment ECSS Secretariat ESA-ESTEC Requirements
More informationUnder pressure pushing down
Under pressure pushing down on me When Dalton was conducting his studies, which led him to the atomic-molecular theory of matter, he also included studies of the behaviour of gases. These led him to propose,
More informationPRECISION GAS MIXTURES
PRECISION GAS MIXTURES 2. Company Profile 3. Reactive Gases 4. Regulators 5. Cylinders 6. Gas Mixtures 7. Accessories PRECISION GAS MIXTURES GASCO Affiliates, LLC is a leading manufacturer of Precision
More informationCHAPTER 16 %UHDWKLQJ*DV0L[LQJ3URFHGXUHV
CHAPTER 16 %UHDWKLQJ*DV0L[LQJ3URFHGXUHV 16-1 INTRODUCTION 16-1.1 Purpose. The purpose of this chapter is to familiarize divers with the techniques used to mix divers breathing gas. 16-1.2 Scope. This chapter
More informationLINEAR TRANSFORMATION APPLIED TO THE CALIBRATION OF ANALYTES IN VARIOUS MATRICES USING A TOTAL HYDROCARBON (THC) ANALYZER
LINEAR TRANSFORMATION APPLIED TO THE CALIBRATION OF ANALYTES IN VARIOUS MATRICES USING A TOTAL HYDROCARBON (THC) ANALYZER Michael T Tang, Ph.D. Grace Feng Greg Merideth Rui Huang Matheson Gas Applied Lab
More informationFlare Gas Composition Analysis and QA/QC Lessons Learned and Lessons Lost SPECTRUM ENVIRONMENTAL SOLUTIONS, LLC 1
Flare Gas Composition Analysis and QA/QC Lessons Learned and Lessons Lost HERMAN HOLM SPECTRUM ENVIRONMENTAL SOLUTIONS, LLC 4C CONFERENCE APRIL 2018 SAN ANTONIO, TX SPECTRUM ENVIRONMENTAL SOLUTIONS, LLC
More informationRapid and Reliable Detection of Dissolved Gases in Water
Rapid and Reliable Detection of Dissolved Gases in Water Andrea Caruso and Massimo Santoro Thermo Fisher Scientific, Milan, Italy Application Note 005 Key Words Chromeleon CDS, Environmental, Fracking,
More informationCompressed Gas ER Fundamentals
Compressed Gas ER Fundamentals Jan 2015 Compressed Gases Represent over 66% of RMP Chemicals PHMSA's 2012 Emergency Response Guidebook provides first responders with a go-to manual to help deal with hazmat
More informationZebron Gas Management
Zebron www.phenomenex.com/gasmanagement What are the key benefits of Zebron filters and traps? The high adsorption capacity of the Zebron Filters removes contaminants from mobile phase gases, reducing
More informationGas Laws. 2 HCl(aq) + CaCO 3 (s) H 2 O(l) + CO 2 (g) + CaCl 2 (aq) HCl(aq) + NaHCO 3 (s) H 2 O(l) + CO 2 (g) + NaCl(aq)
Gas Laws Introduction: Although we cannot see gases, we can observe their behavior and study their properties. For example, we can watch a balloon filled with helium gas floating in air and conclude that
More informationVehicle and Engine Emissions Testing
Vehicle and Engine Emissions Testing Calibration gases and equipment for compliance Benefits and Features Guaranteed analytical accuracy facilitates precise instrument calibration to ensure Part 1065,
More informationCarrier Gases in Capillary GC
Carrier Gases in Capillary GC LC Columns and Consumables Mark Sinnott Application Engineer January 15, 2009 CARRIER GAS Mobile Phase Carries the solutes down the column Selection and velocity influences
More informationThe HumiPyc - Model 1 - Gas Pycnometer; Density, Moisture, Permeation Analyzer; RH sensor Calibrator
The HumiPyc - Model 1 - Gas Pycnometer; Density, Moisture, Permeation Analyzer; RH sensor Calibrator Designed, built, and supported by InstruQuest Inc. Temperature controlled, multi-technique volumetric
More informationINSTRUMENT INSTRUMENT YL INSTRUMENT
INSTRUMENT INSTRUMENT INSTRUMENT Nitrogen Generator Whisper-N2 Series Features Membrane Technology Compressed air is forced through a hollow fiber membrane, with selective permeation of the different components
More informationUsing the PreVent System in Time-Saver Mode with the AutoSystem XL Gas Chromatograph and the TurboMass Mass Spectrometer
application Note Gas Chromatography/ Mass Spectrometry Using the PreVent System in Time-Saver Mode with the AutoSystem XL Gas Chromatograph and the TurboMass Mass Spectrometer Overview A mass spectrometer
More informationISO INTERNATIONAL STANDARD. Welding consumables Gases and gas mixtures for fusion welding and allied processes
INTERNATIONAL STANDARD ISO 14175 Second edition 2008-03-01 Welding consumables Gases and gas mixtures for fusion welding and allied processes Produits consommables pour le soudage Gaz et mélanges gazeux
More informationStandard Test Methods for Water Vapor Content of Electrical Insulating Gases by Measurement of Dew Point 1
Designation: D 2029 97 (Reapproved 2003) Standard Test Methods for Water Vapor Content of Electrical Insulating Gases by Measurement of Dew Point 1 This standard is issued under the fixed designation D
More informationMMS Mercury Monitoring System for Natural Gas
MMS Mercury Monitoring System for Natural Gas Natural gas often contains mercury at concentrations that vary from below 1 to above 10000 µg/m 3. Mercury is both toxic and potentially damaging: it can corrode
More informationChemistry 1B Chapter 10 Worksheet - Daley. Name
Name 1) The National Weather Service routinely supplies atmospheric pressure data to help pilots set their altimeters. The units the NWS uses for atmospheric pressure are inches of mercury. A barometric
More information2 Sentry MCL Installation, Operation & Maintenance
Gas Liquid & Slurry Solid & Powder Steam & Water Installation, Operation & Maintenance Manual Original Instructions Liquid Sampling Manual Low-Emission Samplers S-GA-IOM-00249-7 11-17 Sentry MCL 966 Blue
More informationMultiple Tube - Teflon PTFE-Glass Flowmeters
Multiple Tube - Teflon PTFE-Glass Flowmeters xt Model xt Multiple Tube Teflon PTFE-Glass Flowmeters combine the convenience of multiple tube meters with the unique design features of single tube Teflon
More information3. Coupled Techniques in Thermal Analysis
3. Coupled Techniques in Thermal Analysis Coupled Techniques in Thermal Analysis as Evolved Gas Analysis (EGA) TG/FT-IR Technique for analyzing gas evolved from TG with FT-IR TG/MS Technique for analyzing
More informationAgilent 490 Micro GC Natural Gas Analyzer
Agilent 490 Micro GC Natural Gas Analyzer User Manual Agilent Technologies Notices Agilent Technologies, Inc. 2012 No part of this manual may be reproduced in any form or by any means (including electronic
More informationHonors Chemistry - Problem Set Chapter 13 Classify each of these statements as always true, AT; sometimes true, ST; or never true, NT.
Honors Chemistry - Problem Set Chapter 13 Classify each of these statements as always true, AT; sometimes true, ST; or never true, NT. 1. Atmospheric pressure is 760 mm Hg. 2. The SI unit of pressure is
More informationUNITY 2 TM. Air Server Series 2 Operators Manual. Version 1.0. February 2008
UNITY 2 TM Air Server Series 2 Operators Manual Version 1.0 February 2008 1. Introduction to the Air Server Accessory for UNITY 2...2 1.1. Summary of Operation...2 2. Developing a UNITY 2-Air Server method
More informationAnalysis of Deuterium Enrichment by Fourier Transform Infrared Spectrometry (FTIR): Practice. Christine Slater PhD
Analysis of Deuterium Enrichment by Fourier Transform Infrared Spectrometry (FTIR): Practice Christine Slater PhD Nutrition Specialist C.Slater@iaea.org International Atomic Energy Agency Preparation of
More informationSuper-Clean Gas Filters from Restek
Super-Clean Gas Filters from Restek Chromatography Products www.restek.com 800-356-688 84-353-300 regulator instrument-grade tubing on/off valve GC carrier gas moisture trap hydrocarbon trap high-capacity
More informationThe Principles of Vacuum Technology
The Principles of Vacuum Technology Vacuum Terminology Vacuum units Vacuum regimes How to measure vacuum. Gauge designs. How to create vacuum Pump classifications and designs UHV compatibility considerations
More informationBest Practice for Identifying Leaks in GC and GC/MS Systems
Best Practice for Identifying Leaks in GC and GC/MS Systems Technical Overview Maintaining a leak-free GC or GC/MS system is critical for obtaining optimal system performance with reliable, reproducible,
More informationOrganic Elemental Analysis Series II Nitrogen Analyzer. proven performance. reliable results
Organic Elemental Analysis 2410 Series II Nitrogen Analyzer proven performance reliable results PerkinElmer 2410 Series II Nitrogen Analyzer Advanced Combustion Method Q U I C K G L A N C E Advanced combustion
More informationDRAFT. Operating Procedures for the NPDGamma Liquid Hydrogen Target in TA-53, Building MPF-35
Operating Procedures for the NPDGamma Liquid Hydrogen Target V0.03 11/26/05 1 DRAFT Operating Procedures for the NPDGamma Liquid Hydrogen Target in TA-53, Building MPF-35 Version 0.03 November 26, 2005
More informationStandard Test Method for Residual Acrylonitrile Monomer Styrene-Acrylonitrile Copolymers and Nitrile Rubber by Headspace Gas Chromatography 1
Designation: D 4322 96 (Reapproved 2001) e1 Standard Test Method for Residual Acrylonitrile Monomer Styrene-Acrylonitrile Copolymers and Nitrile Rubber by Headspace Gas Chromatography 1 This standard is
More informationANALYSIS OF GASES PRODUCED BY THREE UNDERWATER CUTTING DEVICES
Navy Experimental Diving Unit (NEDU) TA 03-01 321 Bullfinch Rd. NEDU TR 03-13 Panama City, FL 32407-7015 July 03 ANALYSIS OF GASES PRODUCED BY THREE UNDERWATER CUTTING DEVICES Navy Experimental Diving
More informationSchool of Chemistry SOP For Operation Of Glove Boxes
School SOP for Operation of Glove Boxes: The following SOP provides guidelines on how to adequately and safely operating a standard laboratory glove box and its associated devices. General Information:
More informationv. Size shall be specified on drawings.
SPECIFICATION FOR VACUUM INSULATED PIPING Part 1 General 1. Submittals a. After award of contract and before executing any manufacturing, shop drawings and specifications shall be submitted to the customer
More informationStandard Test Methods for Leaks Using the Mass Spectrometer Leak Detector in the Detector Probe Mode 1,2
Designation: E 499 95 An American National Standard Standard Test Methods for Leaks Using the Mass Spectrometer Leak Detector in the Detector Probe Mode 1,2 This standard is issued under the fixed designation
More informationIncreasing the productivity of ICP-OES with the Thermo Scientific Qtegra ISDS Software
TECHNICAL NOTE 43225 Increasing the productivity of ICP-OES with the Thermo Scientific Qtegra ISDS Software Authors Dr. Elena Chernetsova, Application Specialist, Thermo Fisher Scientific, Bremen, Germany
More informationLaser Spectrometers for Online Moisture Measurement in Natural Gas. Ken Soleyn GE M&C
Laser Spectrometers for Online Moisture Measurement in Natural Gas Ken Soleyn GE M&C ken.soleyn@ge.com Introduction TDLAS (Tunable Diode Lase Absorption Spectroscopy) Moisture Analyzers have become the
More informationApplication Note AN-107
SPEC Sensor TM Characterization & Calibration Considerations Scope This document is provided to describe the considerations needed to characterize, calibrate, verify and validate the measurement performance
More informationISO INTERNATIONAL STANDARD
INTERNATIONAL STANDARD ISO 16017-2 First edition 2003-05-15 Indoor, ambient and workplace air Sampling and analysis of volatile organic compounds by sorbent tube/thermal desorption/capillary gas chromatography
More informationAPPLICATION NOTE. Fast Analysis of Coal Mine Gas Using the INFICON 3000 Micro GC ABSTRACT
APPLICATION NOTE Fast Analysis of Coal Mine Gas Using the INFICON 3000 Micro GC ABSTRACT The INFICON 3000 Micro GC provides two fast and accurate solutions for the analysis of coal mine gas components.
More informationInternational Journal of Generic Drugs ANALYTICAL METHOD PROCEDURES THIS SOP IS 'SWITCHED : OFF : ON'
DISSOLUTION ASSAY Release & Stability Studies Ed. 04. General Index: 1. PRODUCT SPECIFICATIONS (USP MONOGRAPH) 2. IDENTIFICATION BY HPLC 3. ASSAY - HPLC SETUP 4. STANDARD PREPARATION 5. SYSTEM SUITABILITY
More information