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1 1 of 5 5/14/2009 1:55 PM HOME PRODUCT LINES ORDER MY BASKET SEARCH TECH SUPPORT ABOUT US You are here: Home Login welcome, you're no Search center MATERIAL SAFETY DATA SHEET (Trimethylsilyl)diazomethane, ca. 2.0M solution in hexanes Section 1 - Chemical Product and Company Identification Quick order Product code: Quantity: Cross Reference Please enter the product you want to cross reference Terms and conditions Privacy Thermo Fisher Scientific Inc MSDS Name: (Trimethylsilyl)diazomethane, ca. 2.0M solution in hexanes Catalog Numbers: , , Synonyms: Company Identification: BVBA Janssen Pharmaceuticalaan 3a 2440 Geel, Belgium Company Identification: (USA) One Reagent Lane Fair Lawn, NJ For information in the US, call: 800-ACROS-01 For information in Europe, call: Emergency Number, Europe: Emergency Number US: CHEMTREC Phone Number, US: CHEMTREC Phone Number, Europe: Section 2 - Composition, Information on Ingredients CAS# Chemical Name: % EINECS# Symbols: Hexane 65% F XN N (Trimethylsilyl)diazomethane 35% unlisted Risk Phrases: /20 51/ Text for R-phrases: see Section 16 T F N Symbols: Risk Phrases: /20 51/ Section 3 - s Identification

2 2 of 5 5/14/2009 1:55 PM EMERGENCY OVERVIEW Highly flammable. Toxic by inhalation. Irritating to skin. Harmful : danger of serious damage to health by prolonged e inhalation. Possible risk of impaired fertility. Toxic to aquatic organisms, may cause long-term adverse effects in environment. Harmful: may cause lung damage if swallowed. Vapours may cause drowsiness and dizzine Potential Health Effects Eye: Causes mild eye irritation. Causes redness and pain. Skin: Causes skin irritation. May be absorbed through the skin in harmful amounts. May cause dermatitis. Ingestion: Aspiration hazard. May cause lung damage. Inhalation: Exposure produces central nervous system depression. Toxic if inhaled. Inhalation of vapors may cause d dizziness. Chronic: May impair fertility. Section 4 - First Aid Measures Eyes: Skin: Ingestion: Inhalation: Notes to Physician: Flush eyes with plenty of water for at least 15 minutes, occasionally lifting the upper and lower eyeli aid. Do NOT allow victim to rub eyes or keep eyes closed. Flush skin with plenty of water for at least 15 minutes while removing contaminated clothing and sho aid if irritation develops or persists. Get medical aid. Wash mouth out with water. Get medical aid immediately. Remove from exposure and move to fresh air immediately. If not breat artificial respiration. If breathing is difficult, give oxygen. Section 5 - Fire Fighting Measures General Information: Extinguishing Media: As in any fire, wear a self-contained breathing apparatus in pressure-demand, MSHA/NIOSH (approv equivalent), and full protective gear. Vapors can travel to a source of ignition and flash back. Will bu fire. Containers may explode in the heat of a fire. Flammable liquid and vapor. Use water spray to cool fire-exposed containers. Use water spray, dry chemical, carbon dioxide, or Section 6 - Accidental Release Measures General Information: Spills/Leaks: Use proper personal protective equipment as indicated in Section 8. Absorb spill with inert material (e.g. vermiculite, sand or earth), then place in suitable container. Re sources of ignition. Use a spark-proof tool. Do not let this chemical enter the environment. Section 7 - Handling and Storage Handling: Use spark-proof tools and explosion proof equipment. Avoid breathing dust, vapor, mist, or gas. Avoid cont eyes. Take precautionary measures against static discharges. Use and store under nitrogen. Use only in a c hood. Storage: Keep away from sources of ignition. Store in a cool, dry place. Store in a tightly closed container. Keep und blanket. Flammables-area. Section 8 - Exposure Controls, Personal Protection Engineering Controls: Facilities storing or utilizing this material should be equipped with an eyewash facility and a safety shower. U general or local explosion-proof ventilation to keep airborne levels to acceptable levels. Exposure Limits CAS# : United Kingdom, WEL - TWA: 20 ppm TWA; 72 mg/m3 TWA United Kingdom, WEL - STEL: 60 mg/m3 STEL United States OSHA: 500 ppm TWA; 1800 mg/m3 TWA Belgium - TWA: 50 ppm VLE; 179 mg/m3 VLE France - VME: 50 ppm VME; 170 mg/m3 VME Germany: 50 ppm TWA; 180 mg/m3 TWA Japan: 40 ppm OEL; 140 mg/m3 OEL Malaysia: 50 ppm TWA; 176 mg/m3 TWA Netherlands: 25 ppm MAC; 90 mg/m3 MAC Russia: 300 mg/m3 TWA (vapour) Spain: 50 ppm VLA-ED; 179 mg/m3 VLA-ED CAS# :

3 3 of 5 5/14/2009 1:55 PM Personal Protective Equipment Eyes: Wear chemical splash goggles. Skin: Wear appropriate protective gloves to prevent skin exposure. Clothing: Wear appropriate protective clothing to prevent skin exposure. Respirators: Follow the OSHA respirator regulations found in 29 CFR or European Standard EN 149. Use a N European Standard EN 149 approved respirator if exposure limits are exceeded or if irritation or other sy experienced. Section 9 - Physical and Chemical Properties Physical State: Liquid Color: clear yellow Odor: mild odor ph: Not available Vapor Pressure: Not available Viscosity: Not available Boiling Point: 96 deg ( F) Freezing/Melting Point: Not available Autoignition Temperature: Not available Flash Point: -23 deg C ( deg F) Explosion Limits: Lower: Not available Explosion Limits: Upper: Not available Decomposition Temperature: Not available Solubility in water: Insoluble Specific Gravity/Density: Molecular Formula: C4H10N2Si Molecular Weight: Section 10 - Stability and Reactivity Chemical Stability: Conditions to Avoid: Incompatibilities with Other Materials ous Decomposition Products ous Polymerization Stable under normal temperatures and pressures. Incompatible materials, ignition sources. Strong oxidizing agents. Nitrogen oxides, carbon monoxide, carbon dioxide, silicon dioxide Will not occur. Section 11 - Toxicological Information RTECS#: CAS# : MN CAS# : None listed LD50/LC50: RTECS: CAS# : Draize test, rabbit, eye: 10 mg Mild; Inhalation, mouse: LC50 = mg/m3/2h; Inhalation, rat: LC50 = ppm/4h; Inhalation, rat: LC50 = mg/m3/3m; Oral, rat: LD50 = 25 gm/kg;. RTECS: CAS# :. Carcinogenicity: Hexane - Not listed as a carcinogen by ACGIH, IARC, NTP, or CA Prop 65. (Trimethylsilyl)diazomethane - Not listed as a carcinogen by ACGIH, IARC, NTP, or CA Prop 65. Other: The toxicological properties have not been fully investigated. Section 12 - Ecological Information Not available Section 13 - Disposal Considerations Dispose of in a manner consistent with federal, state, and local regulations. Section 14 - Transport Information

4 4 of 5 5/14/2009 1:55 PM Shipping Name: Class: UN Number: Packing Group: IATA IMO RID/ADR FLAMMABLE FLAMMABLE FLAMMABLE LIQUID, TOXIC, LIQUID, TOXIC, LIQUID, TOXIC, N.O.S.* N.O.S. N.O.S. 3 (6.1) 3 (6.1) 3 (6.1) II II II USA RQ: CAS# : 5000 lb final RQ; 2270 kg final RQ European/International Regulations European Labeling in Accordance with EC Directives Symbols: T F N Risk Phrases: R 11 Highly flammable. R 23 Toxic by inhalation. R 38 Irritating to skin. R 48/20 Harmful : danger of serious damage to health by prolonged exposure through inhalation. R 51/53 Toxic to aquatic organisms, may cause long-term adverse effects in the aquatic environment. R 62 Possible risk of impaired fertility. R 65 Harmful: may cause lung damage if swallowed. R 67 Vapours may cause drowsiness and dizziness. Safety Phrases: S 9 Keep container in a well-ventilated place. S 16 Keep away from sources of ignition - No smoking. S 29 Do not empty into drains. S 33 Take precautionary measures against static discharges. S 36/37 Wear suitable protective clothing and gloves. S 45 In case of accident or if you feel unwell, seek medical advice immediately (show the label where p S 61 Avoid release to the environment. Refer to special instructions/safety data sheets. S 62 If swallowed, do not induce vomiting: seek medical advice immediately and show this container o WGK (Water Danger/Protection) Canada US Federal TSCA CAS# : 1 CAS# : Not available CAS# is listed on Canada's DSL List Section 15 - Regulatory Information CAS# is listed on the TSCA Inventory. CAS# is not listed on the TSCA Inventory. It is for research and development use only. Section 16 - Other Information Text for R-phrases from Section 2 R 11 Highly flammable. R 38 Irritating to skin. R 48/20 Harmful : danger of serious damage to health by prolonged exposure through inhalation.

5 5 of 5 5/14/2009 1:55 PM R 62 Possible risk of impaired fertility. R 51/53 Toxic to aquatic organisms, may cause long-term adverse effects in the aquatic environment. R 65 Harmful: may cause lung damage if swallowed. R 67 Vapours may cause drowsiness and dizziness. MSDS Creation Date: 11/13/1996 Revision #3 Date 11/06/2008 Revisions were made in Sections: 3, 4, 7, 9, 14 The information above is believed to be accurate and represents the best information currently available to us. However, we mak warranty of merchantibility or any other warranty, express or implied, with respect to such information, and we assume no liabili resulting from its use. Users should make their own investigations to determine the suitability of the information for their particu purposes. In no event shall the company be liable for any claims, losses, or damages of any third party or for lost profits or any s indirect, incidental, consequential, or exemplary damages howsoever arising, even if the company has been advised of the possib such damages

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