High Pressure Equipment Pressure Vessels and Reactors

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2 Vessels and Reacrs Company designs and manufactures a broad range of pressure vessels and reacrs for both bench-scale and pilot plant applications.we have over 0 standard reacr designs which address varied size, material, pressure and temperature requirements. There are many applications that demand ASME approval for work involving pressure vessels.to satisfy this need, HiP produces a variety of pressure vessels and reacrs that meet the requirements of the ASME Vessel Code. Complementing our standard product offering is our capability provide a cusm reacr designed meet your specific needs.our engineering and technical support will help you identify the specific options you need, ranging from exotic materials unusual sizes and connections, and then incorporate the appropriate approvals, including ASME. Index Page Vessel Selection O-Ring Seal Reacrs Series OC Confined Gasket Closure Reacrs - Series GC Bolted Closure Reacrs Clover Leaf Reacrs O-Ring Closure Reacrs Series R Tubular Reacrs Series TOC Micro Reacrs Series MS

3 Reacr Selection Guide Reacr Design O-ring Seal Series OC Confined Gasket Closure Series GC Bolted Closure Series BC Clover Leaf Series CL O-ring Closure Series R Micro Reacrs Series MS Tubular Reacrs Series TOC Cusm Reacrs 0. Description Maximum Maximum Working Standard Temperature () (degrees F) Standard Capacity Simple closure design allows for easy assembly/disassembly and reliable operation.series OC are economical reacrs ideal for low temperature gas or liquid service. 6SS 0 6,000 ml 6,70 ml Series GC is designed for studying high temperature and pressure reactions.the vessels utilize thrust bolts and a thrust ring ensure positive seating of the gasket. 6SS 800 6,000 ml 6,70 ml These versatile reacrs are the standard of the industry for applications involving moderate pressure ranges.standard O-rings may be used in place of the metal gasket for lower temperatures. 6SS ml gal. Quick opening cover design needs only one-eighth of a turn rotation for sealing.ideal for high pressure operations requiring repetitive opening/closing. 0 alloy steel 0 0,000,000 ml,700 ml Designed for extremely high pressure/low temperature operation, series R reacrs feature a threaded closure for easy assembly and disassembly. 0 alloy steel 0 0, ml 0 liters Series MS are fixed bed tubular reacrs designed for a variety of applications such as small volume testing of components and miniature scale reaction tests. 6SS 800 0,000 ml 6 ml 0,000 0 ml liters This line of economical and versatile reacrs satisfy many moderate pressure applications. Accumulars can be cusmized through a variety of options including pisn separars. O-ring 0 0SS confined gasket 800 HiP makes every reacr order, allowing for economical and timely cusmizing.we offer a broad range of exotic metals, sizes and connections meet virtually any requirement. Note: For ASME code stamping of HiP vessels, please consult facry for available reacr designs, materials, and pressure ratings. R /97

4 Vessel Volume Table (cubic inches) Depth (inches) Diameter (inches) " " " " " " " " 0" Volume Equivalents in = 6.9 ml ml = 0.06 in gal = in = 0. ft ft = 78 in = 7.8 gal L = 6.0 in = 0.6 gal 00 Conversions atm kg/cm atm kg/cm R /97 0.

5 OC Series O-Ring Seal Reacrs The OC Series provide a simple closure that is reliable and easy assemble and disassemble.standard material for the body and cover is Type 6 stainless steel.the standard O-ring material is BUNA-N.Temperature is limited by the O-ring 0 F. These reacrs are suitable for either gas or liquid service. Capacities range from ml 6,70 ml. Standard connections are for/ high pressure (coned and threaded) tubing (HF).Models OC- and OC- have one connection in the cover.all other models have two connections in the cover.contact facry if other connections and/or locations are preferred. Series OC Reacrs Catalog No.. COVER. CAP. "O" RING. BODY ALLOY STEEL BUNA-N OC-* OC-* OC- OC-7 OC-9 OC- OC- OC- OC-7 OC-9 OC- OC- OC- OC-7 OC-9 OC- OC- OC- Depth " / / / / / / 0" 0" 0" " 0" " 0" " 0" " 0" " 0" " 0" " 0" " " " " " Capacity Working ml 80 ml 80 ml 600 ml 00 ml,00 ml 800 ml,60 ml,0 ml,0 ml,7 ml,00 ml,060 ml, ml,600 ml,7 ml,00 ml 6,70 ml,800 7,70 6,000 6,000,00,00 9,00 9,00,000,000 0,00 0,00 8,00 8,00 6,00 6,00 *One () opening only in cover 0. R /99

6 Confined Gasket Closure Reacrs The Confined Gasket Closure reacrs listed below are ideally suited for use at elevated temperatures and pressures as shown in the chart.thrust bolts with a hardened thrust ring are supplied insure positive seating of the gasket.torque required on thrust bolts will range from 70 foot pounds, depending upon size of reacr, pressure, temperature and media being pressurized. Torquing of bolts should be done in a crisscross staggered pattern insure uniform seating.a commercial high temperature lubricant should always be applied the bolt threads and outside cap threads facilitate removal of the closure. Standard material for the body, cover and gasket is Type 6 stainless steel.these reacrs are suitable for either gas or liquid service and capacities range from ml 6,70 ml. Standard connections supplied are for / high pressure (coned and threaded) tubing (HF).Models GC- and GC- have one connection in the cover.all other models have two connections in the cover and a thermowell that extends two-thirds of the inside depth. Included with each reacr are eye bolts for lifting and necessary collars and glands for the connections.vise flats are machined on the botm of the body for securing while assembling or disassembling closure. Series GC Reacrs GC- GC- GC- GC-7 GC-9 GC- GC- GC- GC-7 GC-9 GC- GC- GC- GC-7 GC-9 GC- GC- GC- Depth Capacity Working () 00 F 60 F 800 F " / / / / / / 0" 0" 0" " 0" " 0" " 0" " 0" " 0" " 0" " 0" " ml 80 ml 80 ml 600 ml 00 ml,00 ml 800 ml,60 ml,0 ml,0 ml,7 ml,00 ml,060 ml, ml,600 ml,7 ml,00 ml 6,70 ml,800 7,70 6,000 6,000,00,00 9,00 9,00,000,000 0,00 0,00 8,00 8,00 6,00 6,00 " " " ",00 7,000,00,00,00,00 8,00 8,00,000,000 9,000 9,000 7,00 7,00,00,00,00,00,000 6,900,000,000,000,000 8,00 8,00 0,000 0,000 8,000 8,000 6,00 6,00,000, Catalog No. 7. COVER. SET SCREW. CAP. THRUST RING. GASKET 6. GASKET 7. BODY 8. WEEP HOLE COMM. ALLOY ST'L TOOL ST'L COPPER R /97 0.

7 Bolted Closure Reacrs The Bolted Closure Reacrs are designed for use up 60 F ( C) at the working pressures indicated.standard material for the body, cover and gasket is Type 6 stainless steel. Standard O-rings may be used in place of the metal gasket when temperatures permit. Standard connections include two high pressure (coned and threaded) tubing connections for/ tubing (HF) located in the cover.contact facry if other connections and/or locations are preferred. Other items available include: Heating mantle.removable quartz fabric cylinder column type.0 volt, single phase. Bolted closure reacrs are supplied with mounting bolt holes on the botm surface. Thermowell for use with/ thermocouple Safety head located in side flange with rupture disc (see Page.7). PRESSURE CONNECTION (). SOCKET CAP SCREW. COVER. GASKET. MAIN SEAL 6. BODY 7. THERMOCOUPLE WELL* 8. SAFETY HEAD* Bolted Closure Reacrs Catalog No. Capacity Working BC- 00 ml 60 " BC- liter 60 " Approx. Approx. Weight Torque (ft-lb) Depth (pounds) per Bolt liter 60 / " BC- gallon, " 97 0 BC- gallon 60 " gallon, BC- BC Temperature Rating F Diameter * SUPPLIED AS EXTRA WHEN SPECIFIED R /99

8 Clover Leaf Reacrs The Clover Leaf Closure Reacrs provide maximum ease for quick opening or closing of the cover.the cover is simply inserted in the body and then rotated one-eighth of a turn.a safety locking pin is provided insure that the cover is properly positioned and locked. Standard material of construction for these reacrs is heat treated 0 alloy steel.standard connections include two high pressure (coned and threaded)/ tubing connections (HF). Mounting holes are provided in the p and botm of the body for securing or lifting.. LOCK PIN. COVER. O-RING. BODY Clover Leaf Closure Reacrs Catalog No. Diameter Outside Diameter Depth Working Temperature Rating F Capacity CL- CL- CL- " 6 " 0,000 0,000 ml,000 ml,00 ml Alloy Steel CL-8 CL-9 9 0,000 0,80 ml,700 ml Alloy Steel R /97 0.7

9 Series R Reacrs O-Ring Closure The Series R O-ring Closure Reacrs are easily assembled and disassembled with minimal rque required for complete engagement. of construction for standard models is Type 0 alloy steel (or equivalent) properly heat treated for use at elevated pressures.(some models can be provided in stainless steel construction at reduced pressures consult facry). Sealing is accomplished by a highly reliable combination of O-ring and separate metal back-up ring.the wedge shaped back-up ring is designed expand and contract as pressure increases or decreases.consequently, the O-ring is continuously confined with no clearance for extrusion.minimal initial rque is required effect a positive seal. Temperature on these vessels must be restricted 0 F maximum, due the BUNA-N (nitrile) O-ring. (continued on page 0.9) O-Ring Closure Reacrs (one piece cover) Rating / 0,000 0,000 " 0" " R-0-0 R--0 R-6-0 R-0-0 R--0 R-6-0 R-0-60 R--60 R-6-60 R-0-00 R--00 R-6-00 R--0 R ,000 00,000 6 / 0,000 R-6-0 R-0-0 / 0,000 R.-6-0 R.-0-0 R.--0 R.-6-0 / 0,000 / 0, ,000 00, ,000 / 0,000 0,000 " R-6-0 / 6. COVER. BODY. VENT HOLE. BACK UP RING. "O" RING 6. PRESSURE CONNECTION 0 R-6-0 Alloy Steel R-6-60 or equivalent R-6-00 Depth 6 0, ,000 " 00,000 R Alloy R.-6-0 Steel R or equivalent R " R.-0-0 R.--0 R.-6-0 R.-0-0 R.--0 R.-6-0 R R.--60 R R R.--00 R R.-6-0 R.-0-0 R.--0 R.-6-0 R R-6-0 Alloy Steel R-6-0 or equivalent R-6-60 R-6-00 R-0-0 R--0 R-6-0 R-0-0 R--0 R-0-0 R--0 R-6-0 R-0-0 R--0 R-0-0 R--0 R-6-0 R-0-0 R--0 R-0-60 R--60 R-6-60 R-0-60 R--60 R-0-00 R--00 R-6-00 R-0-00 R R 8/0

10 Included with each vessel is a Tony Bar for removal of the cover nut and necessary eye bolt holes for lifting of the body and components.outer surfaces are blackened prevent rusting. Vent holes are provided prevent pressure build up behind the closure in the event of a worn or damaged seal. Connections include a p and botm high pressure coned and threaded / (HF) tubing connection.other sizes or locations for connections can easily be provided when preferred. Consult facry. Closures are designed in one-piece (cover) for vessels up " and two-piece (cover and main nut) for vessels larger than " Rating (two piece cover) Depth 0" " 0" 0,000 R-6-0 R-0-0 R--0 R-6-0 R-0-0 R--0 7" 0,000 R-6-0 R-0-0 R--0 R-6-0 R-0-0 R ,000 R-6-0 R-0-0 R--0 R-6-0 R-0-0 R--0 60,000 R-6-60 R-0-60 R--60 R-6-60 R-0-60 R ,000 R-6-00 R-0-00 R--00 R-6-00 R-0-00 R--00 0,000 R-6-0 R-0-0 R--0 R-6-0 R-0-0 R--0 9/ 0,000 R-6-0 R-0-0 R--0 R-6-0 R-0-0 R--0 " 0,000 R-6-0 R-0-0 R--0 R-6-0 R-0-0 R--0 " 0,000 R-6-0 R-0-0 R--0 R-6-0 R-0-0 R--0 60,000 R-6-60 R-0-60 R--60 R-6-60 R R ,000 R-6-0 R-0-0 R--0 R-6-0 R-0-0 R--0 / / 0,000 R-6-0 R-0-0 R--0 R-6-0 R-0-0 R--0 R-6-0 R-0-0 R--0 R-6-0 R-0-0 R--0 / 9 0,000 0,000 R-6-0 R6-6-0 R-0-0 R6-0-0 R--0 R6--0 R-6-0 R6-6-0 R-0-0 R6-0-0 R--0 R6--0 0,000 R6-6-0 R6-0-0 R6--0 R6-6-0 R6-0-0 R6--0 / 0,000 R6-6-0 R6-0-0 R6--0 R6-6-0 R6-0-0 R6--0 0,000 R6-6-0 R6-0-0 R6--0 R6-6-0 R6-0-0 R6--0 0/ 0,000 R7-6-0 R7-0-0 R7--0 R7-6-0 R7-0-0 " 0,000 R7-6-0 R7-0-0 R7--0 R7-6-0 R7-0-0 / 0,000 R7-6-0 R7-0-0 R7--0 R7-6-0 R ,000 R8-6-0 R8-0-0 R8--0 R8-6-0 R8-0-0 / 0,000 R8-6-0 R8-0-0 R8--0 R8-6-0 R8-0-0 " 0,000 R9-6-0 R9-0-0 R9--0 R9-6-0 R " / 0,000 R0-6-0 R0-0-0 R0--0 R0-6-0 R0-0-0 " 7" 0,000 0 Alloy Steel or equivalent. PRESSURE CONNECTION. MAIN UNIT NUT. BODY. VENT HOLE. COVER 6. BACK UP RING 7. "O" RING O-Ring Closure Reacrs 6 7 SEALING DETAIL R /99 0.9

11 Tubular Series Reacrs The Tubular Series Reacrs are double ended pressure vessels made from commercial quality cold drawn Type 0 stainless steel seamless tubing.outside (non-wetted) caps are alloy steel.these are both economical and versatile vessels proven in demand for many applications. Finishes are commercial cold drawn finishes, with honed internal finishes. Standard sizes are shown in the chart on page 0., but special lengths and modifications are easily supplied on request.one pressure connection for/ high pressure coned and threaded tubing at each end is standard.additional end connections are possible on the larger size models.also, side connections and end cover thermowells can be supplied when required.consult facry for special requirements. O-Ring Closures are standard when temperatures do not exceed 0 F.This is an easily assembled closure requiring minimal rque for positive sealing.the standard O-ring material used is BUNA-N (nitrile) with various other O-ring materials available on request. Confined Gasket Closures are available for temperatures up 800 F.A % reduction in the listed working pressure is required at this elevated temperature level.these closures utilize a metal gasket (0 stainless steel) which can be rqued down for positive sealing.torque requirements on the thrust bolts will range from 60 0 foot pounds depending on size, pressure, temperature and media being pressurized.these confined gasket closures are available for all models except the TOC and TOC series.when ordering, simply specify catalog number and add suffix (W/Gasket). Pisn Separars can be supplied with the O-ring closure vessels for use as compression cylinders.these are ideal for separating a liquid from a gas and other similar applications.the tubing body is supplied with a honed inside diameter surface accommodate the pisn.when ordering, simply specify catalog number and add suffix (W/Pisn). 0.0 R /97

12 Tubular Series Reacrs Rating " TOC-0 TOC-0 TOC-60 TOC-7 0,000 TOC-0 TOC-0 TOC-60 TOC-7 TOC-0 TOC-0 TOC-60 TOC-7 0"IL 60"IL 7"IL / " 6,000 " " 0,000 TOC7-0 TOC7-0 TOC7-60 TOC7-7 /,000 TOC9-0 TOC9-0 TOC9-60 TOC9-7 7,000 / ",000 " " /,000 TOC-0 TOC-0 TOC-60 TOC-7 Body 0 S.S. TOC-0 TOC-0 TOC-60 TOC-7 TOC-0 TOC-0 TOC-60 TOC-7 Covers TOC7-0 TOC7-0 TOC7-60 TOC7-7,00 TOC9-0 TOC9-0 TOC9-60 TOC9-7 /,00 TOC-0 TOC-0 TOC-60 TOC-7 ",000 TOC-0 TOC-0 TOC-60 TOC-7,000 TOC-0 TOC-0 TOC-60 TOC-7 " TOC7-0 TOC7-0 TOC7-60 TOC7-7,000 TOC9-0 TOC9-0 TOC9-60 TOC9-7 TOC-0 TOC-0 TOC-60 TOC-7 0"IL Catalog Number (O-Ring Closure) Tubing Size O-RING PISTON GASKET PRESSURE CONNECTION. COVER. CAP. "O" RING. BODY (BOTH ENDS ALIKE) 6. PISTON 7. THRUST RING 8. GASKET 9. WEEP HOLE O-RING PISTON GASKET How To Order Tubular Series Reacrs With O-Ring Closure: Specify catalog number, see ordering table above. Note:Use of Buna-N O-ring limits maximum working temperature 0 F.For higher temperatures 800 F, order gasket closure. With Pisn Separars: With Gasket Closure: Specify catalog number, see ordering tablespecify catalog number, see above and add (W/Pisn) as suffix. ordering table above and add W/Gasket) as suffix. Because of temperature limitations * Gasket closure is not available pisns are not normally ordered in on tubing size vessels. combination with the gasket closure. Example: TOC-0 (W/Gasket). R /0 0.

13 Series MS Micro Reacrs The Micro Reacrs shown are designed for numerous applications including small volume testing of components and miniature scale reaction tests. Standard material of construction is Type 6 stainless steel. Operation at temperatures up 800 F is made possible by the metal metal seal construction.working pressures should be reduced by approximately % at the maximum 800 F temperature level. Connections are for/ high pressure coned and threaded tubing (HF).One connection is provided at each end.other sizes or types of connections can be provided. Thermocouples can easily be installed with the use of thermocouple adapters (refer section 8.0). A B (C) (D) 0. Working (C) (D) Outside Diameter Diameter Catalog No. Capacity MS- MS- MS- MS- MS- ml ml ml ml 6 ml MS- MS- MS- MS- MS- ml 7/ ml 0 ml / ml ml 0,000 MS-6 MS-7 MS-8 MS-9 ml ml 6 ml 8 ml 0, , (A) Depth (B) Overall Length 0" " 7" " " " " 6 6 0" " " 0" 0" 6 9 R /97