VACUUM & AIRLESS. Select from Kimble vacuum traps, manifolds, Schlenk tubes, adapters, and bubblers for your vacuum and airless glassware needs.

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1 VACUUM & AIRLESS Select from Kimble vacuum traps, manifolds, Schlenk tubes, adapters, and bubblers for your vacuum and airless glassware needs. tions precision glassware solutions precision glassware solutions precision glassware solutions precision glassware solutions precision glassware solutions precision glassware solutions pre glassware solutions precision glassware solutions precision glassware solutions precision glassware solutions precision glassware solutions precision glassware solutions precision glasswa tions precision glassware solutions precision glassware solutions precision glassware solutions precision glassware solutions precision glassware solutions precision glassware solutions pre sion glassware solutions precision glassware solutions precision glassware solutions precision glassware solutions precision glassware solutions precision glassware solutions precision gla solutions precision glassware solutions precision glassware solutions precision glassware solutions precision glassware solutions precision glassware solutions precision glassware solution

2 366 VACUUM & AIRLESS Inlets Airless-ware is a family of ground-jointed glassware designed for the manipulation of air-sensitive compounds on a medium to large scale, using an inert gas to exclude air or moisture vapors. The essential feature of most of the Airless-ware apparatus is a sidearm fitted with a stopcock. Through this sidearm the apparatus is evacuated to eliminate air and an inert gas is introduced. A high vacuum is not necessary because the purge cycle is repeated several times. For example, suppose an initial evacuation of 2 mm pressure; after the second pumping and filling, the pressure of residual air is 2 x 2/760 mm, and after the third cycle it is 2 x (2/760)2 mm, or approximately 0-5 mm of residual air. Due to the frequency with which these purging cycles are performed, it is useful to have a manifold equipped with a series of vacuum valves. Attached to this manifold is a source of purified nitrogen or argon and a source of vacuum. The source of vacuum should be a mechanical vacuum pump. The pump should be protected by a dry ice-cooled or liquid nitrogen-cooled trap. A size 25 vacuum trap would serve this purpose. This trap must have a relatively large volume and be easily removed from the system since considerable quantities of condensables are accumulated at this point. For moderately air sensitive materials, the solvent may be purged with an inert gas stream prior to use. Balloon Type Inlet Adapters This gas balloon type adapter is used for protective storage in jointed vessels. The inert gas tubing may be disconnected, giving the vessel its own portable inert gas source to balance volume changes caused by sample removal Supplied without the balloon Replacement retainer is One arm of the T-bore stopcock is connected to the inert gas source. The arm with a hose connector is connected to a balloon. Vessels connected to this adapter may be flushed and filled with inert gas. The balloon can be expanded with inert gas for storage at the same time or separately. The stopcock bore is then rotated to connect the balloon to the vessel. Fits Tubing ID (inches) / / Inlet Adapters with Septum This gas inlet adapter has a standard taper joint. Sidearm has a 2 mm bore 8200 PTFE stopcock with a port for gas introduction and a rubber-stoppered port on the top tube for syringe retrieval Supplied complete with one 8823 septum stopper borosilicate glass conforming to USP Type I and ASTM E438, Type I, Class A / /40 Description Size 22 Stopcock Plug Retainer, Fits Plug Sizes 6.2/56, 7.35/50, 7/40, 5/35, O-Ring Size 207 Description Size 2 mm Straight Bore Stopcock Plug, PTFE, /25 mm Plug Size Sleeved septum stopper with off-center hole 44 Toll Free: International:

3 Inlets / AIRLESS-WARE VACUUM & AIRLESS 367 Inlet Adapters Supplied with the patented pressure/vacuum retainer Used with sleeved stopper series has a 8000 glass plug and an inner standard taper joint 2330 series has a PTFE plug and an outer standard taper joint Plug Material /20 inner Glass /40 inner Glass /20 outer PTFE /22 outer PTFE /40 outer PTFE AIRLESS-WARE Pressure Release Valve Designed for applications that require evacuated apparatus to be filled with an inert gas to one atmosphere. Uses include the introduction of an inert gas into a vacuum desiccator or nitrogen into Airless-ware apparatus A pressure release valve should be placed between the nitrogen source and nitrogen manifold on all Airless-ware manifold installations Operation: Three ml of paraffin or silicone oil is added to the bubbler. One arm is connected to the low-pressure gas source, the other to the manifold or Airless-ware equipment. The check valve prevents oil or air from surging into the apparatus. Height Fits Tubing ID (inches) Description Size 2 mm Straight Bore Stopcock Plug, PTFE, /25 mm Plug Size Size 2 Stopcock Plug Retainer Sleeved septum stopper with off-center hole 44 AIRLESS-WARE Transfer Adapters Used to transfer fluids between two flasks or as a onepiece distillation unit. A variety of flasks or adapters may be connected to this unit to use at reduced pressure or under an inert atmosphere All joints are the same size x /40 55 x 270 AIRLESS-WARE Filling Adapters Designed for use with a solvent repurifier to facilitate product removal from the storage area. This adapter will provide clearance from the boiling flask and attaches to a 2320 solvent storage flask Hose connection allows access to vacuum source or inert gas / AIRLESS-WARE Vacuum Valve Adapters Vacuum valve adapter for closing joints on AIRLESS-WARE vessels while allowing reconnection to funnels or other components, with minimum exposure to air or water vapor. Kimble PTFE vacuum valve minimizes contamination and maintains vacuum in the micron region Tip seal of valve is directed toward a normal storage vessel Plug is x /20 30 x /40 90 x 60 Description Size 4 Valve Plug AIRLESS-WARE Connecting Adapter with Glass Plug Converts standard flasks, funnels or other components to airless applications. Stopcock has patented pressure/vacuum retainer borosilicate glass conforming to USP Type I and ASTM E438, Type I, Class A x /20 5 x /40 55 x 80 kimblechase.com

4 368 VACUUM & AIRLESS AIRLESS-WARE AIRLESS-WARE Connecting Adapters This adapter has a three-arm design for the assembly of three vessels. outer joint at the top; bottom joints are inner joints With hooks x /20 60 x 90 Airless Gas Bubbler with HI-VAC Valve This bubbler is designed with an integral valve for controlling gas flow in reactions or to provide an inert atmosphere when either nitrogen or argon is used. The inner tube is positioned to within 5 mm of the tube bottom, requiring a minimal amount of mineral oil Valve plug is Body OD x Overall Width x 80 AIRLESS-WARE Solvent Transfer Manifold This manifold is designed for the purification and transfer of solvents under airless conditions. The manifold allows the vacuum transfer of solvent at room temperature from a boiling flask with a vacuum valve directly into an evacuated solvent storage flask Solvent is then cooled to a low temperature with liquid nitrogen or dry ice/acetone Manifold incorporates a HI-VAC valve with an plug and 3/8 ground connection /40 Airless Gas Bubbler This bubbler is for use with mineral oil to observe gaseous addition to reactions. It also may be used to vent a reaction mixture to the atmosphere. Tubing connections are 8 mm OD May be used with or to join multiple bubblers if necessary Body OD x Overall Width x 80 Airless Gas Bubbler with Ground Joint This gas bubbler is designed to be used with mineral oil or a similar liquid to monitor gas flow to organic reactions. The unit has a 24/40 ground joint and can be used with single or multi-necked flasks having a similar opening. Approximately 0 ml of oil is required to seal the lower inner tube. The rate of gas flow can then be observed Tubing connection is 8 mm OD Body OD x Overall Width x 70 Jacketed Dewar Flasks Specially constructed Dewar flask is fully jacketed with aluminum for excellent insulation of contents. Viewing ports allow visual inspection of the contents through the strip-silvered glass borosilicate glass conforming to USP Type I and ASTM E438, Type I, Class A ID Depth AIRLESS-WARE Reaction Flasks The modified Kjeldahl shape of this flask facilitates heating, stirring and solvent stripping without impairing ease of liquid and solid transfer. Improved version of classic Schlenk tube Bottom of the flask is shaped to fit spherical heating mantles Supplied with a glass plug and the patented pressure/ vacuum retainer Capacity (ml) Standard Taper / / / / / / / /40 Description Size 2 mm Straight Bore Stopcock Glass Plug, solid, plug size 2/30 mm Size 2 Stopcock Plug Retainer Toll Free: International:

5 AIRLESS-WARE / Manifolds VACUUM & AIRLESS 369 AIRLESS-WARE Straus Flask This round bottom flask was developed for solvent storage as required by many inorganic reactions. Dry, deoxygenated and grease-free solvents are maintained in this state for relatively long periods of time Solvent integrity is provided by the Kimble HI-VAC valve, which provides access to the flask contents Quantities of solvent are withdrawn from the flask using either a cannula or a syringe with a proper length needle Valve is 0-4 mm and has an plug Capacity (ml) x Overall Width x x 35 AIRLESS-WARE Vacuum Schlenk Tube with O-Ring Sidearm This modified version of the Schlenk tube is suitable for connection to or vacuum manifolds. Size 5 standard socket joint at the sidearm The 25 and 50 ml tubes have 0-4 mm valves with plugs The 00 and 350 ml tubes have 0-8 mm valves with plugs All sizes have #6 o-ring Capacity (ml) Body OD AIRLESS-WARE Vacuum Schlenk Tube This Schlenk tube is suitable for use with or manifolds. Tube has a HI-VAC valve to control gas flow to the reaction tube Tubes are constructed of medium wall borosilicate glass and perform well under both thermal and pressure-type reactions The 25 and 50 ml tubes have 0-4 mm valves with plugs The 00 and 350 ml tubes have 0-8 mm valves with plugs Capacity (ml) Stem, Body OD , , , , , 5 Description Size 4 Valve Plug Size 8 Valve Plug Description Size 4 Valve Plug Size 8 Valve Plug Vacuum/Gas Manifold with Metering Valves This all-glass manifold is for connecting inert gas and vacuum sources to sidearm stopcocks. Fine control of vacuum and inert gases provided by metering groove cut into plug of each stopcock Distance between stopcocks is 65 mm for the 3-position size and 00 mm for the 5-position size Supplied with patented pressure/vacuum retainers of Places Description Size 2 Stopcock Plug Retainer Size 2 Double Oblique Stopcock Glass Plug, plug size 4.5/50 mm kimblechase.com

6 370 VACUUM & AIRLESS Manifolds Vacuum/Gas Manifold with PTFE Valves This manifold is for connecting inert gas and vacuum sources. 4 mm PTFE vacuum valves provide grease-free fine control Sample contacts only PTFE and borosilicate glass Beams are /2 (2.7 mm) OD, with upper-left and lower-right ends open Ports have 9 mm OD openings Distance between valves is 00 mm series has tip o-rings; 2640 series does not Plugs for 2640 series are Plugs for series are of Places Description Size 4 Valve Plug, PTFE Size 4 PTFE Valve Plug Double Vacuum/Gas Manifold with PTFE Valves at 45 Angle This manifold is for connecting inert gas and vacuum sources. Double vacuum gas manifold with PTFE valves at 45 angle. Supplied with 4 mm PTFE vacuum valves for grease-free operation Fabricated from larger 3/4 medium wall tubing Upper left and lower right beams are open Ports are spaced 00 mm apart and have serrated hose connections Rod braces are located between each bank for added strength Valves are sealed at a 45 angle to allow easier manipulation of Places Double Vacuum/Gas Manifold with Vacuum Chambers An all-glass manifold for connecting inert gas and vacuum sources. Double vacuum gas manifold with vacuum chambers. Fabricated from ½ medium wall tubing Stopcocks are 4 mm bore glass with lower vacuum chamber and are spaced 85 mm apart Top right connection is for inert gas and lower left connection is for vacuum of Places Single Vacuum Manifold with HI-VAC Valves This single manifold is designed for grease-free operation. Incorporates reliable Kimble HI-VAC valves, with size 5 o-ring connectors and size 6 FKM o-rings pinch clamp fits size 5 o-ring connectors Forward-facing valves allow good access Compact enough for ease of assembly within a fume hood, thereby protecting the researcher from noxious chemicals Designed for use with 2320 adapters Can easily be disassembled for cleaning if necessary Replacement plug is with a size 0 FKM o-ring Ports are spaced 75 mm apart of Places Overall Length Double Vacuum/Gas Manifold with HI-VAC Valves This manifold is designed for grease-free operation. Double vacuum gas manifold with HI-VAC valves. Incorporates reliable Kimble HI-VAC valves, with size 5 o-ring connectors and size 6 FKM o-rings pinch clamp fits size 5 o-ring connectors Designed for use with 2320 adapters - Forward-facing valves allow good access Compact enough for ease of assembly within a fume hood, thereby protecting the researcher from noxious chemicals Unit is modular in concept, allowing experiments to be done with maximum flexibility Unions and flexible stainless steel tubing are also available to maximize the utility of this manifold Can easily be disassembled for cleaning if necessary Replacement plug is with two size 0 FKM o-rings and one size 0 FKM tip o-ring Ports are spaced 00 mm apart Ref: Andrea Wayda, AT&T Bell Laboratories of Places Toll Free: International:

7 Manifolds / Tubes / Connectors VACUUM & AIRLESS 37 Threaded Microscale Vacuum Manifold This 6-place manifold is designed for concentration of multiple samples using an inert atmosphere or vacuum. It is also useful for molecular distillation. Unused ports are easily closed off with caps GPI Thread Size Accessories Description PTFE Hose Connector, to / to Threaded Connecting Adapter to Threaded Connecting Adapter Vacuum Schlenk Tube Modified version of the Schlenk tube, with a size 5 standard socket joint at the sidearm, suitable for connection to or vacuum manifolds. The 25 and 50 ml tubes have 0-4 mm valves with plugs The 00 and 350 ml tubes have 0-8 mm valves with plugs All sizes have #6 o-ring Capacity (ml) Body OD Description Size 4 Valve Plug Size 8 Valve Plug AIRLESS-WARE Pressure Release Valve Designed for applications that require evacuated apparatus to be filled with an inert gas to one atmosphere. Uses include the introduction of an inert gas into a vacuum desiccator or nitrogen into Airless-ware apparatus A pressure release valve should be placed between the nitrogen source and nitrogen manifold on all Airless-ware manifold installations Operation: Three ml of paraffin or silicone oil is added to the bubbler. One arm is connected to the low-pressure gas source, the other to the manifold or Airless-ware equipment. The check valve prevents oil or air from surging into the apparatus. Height Fits Tubing ID (inches) Vacuum Connectors with HI-VAC Valves 90 degree vacuum connectors with HI-VAC valves. This adapter is for use with size 5 o-ring glassware and and HI-VAC manifolds. HI-VAC valve has a right angle Two size 5 o-ring connectors (5 mm ID) Size 6 FKM o-rings PTFE plug is borosilicate glass conforming to USP Type I and ASTM E438, Type I, Class A Bore Range x Overall Width x x Vacuum Connectors with HI-VAC Valves Vacuum connectors with HI-VAC valves. 80 degree. This adapter is for use with size 5 o-ring glassware and and HI-VAC manifolds. HI-VAC valve has 80 connections Two size 5 o-ring connectors (5 mm ID) Size 6 FKM o-rings PTFE plug is Bore Range x Overall Width x 00 O-Ring Vacuum Connector with Hose Connection Size 5 o-ring connector (5 mm ID) for use with and HI-VAC manifolds and adapters. For applications utilizing tubing Fits flexible tubing with 3/8 ID Supplied with one size 6 FKM o-ring borosilicate glass conforming to USP Type I and ASTM E438, Type I, Class A Fits Flexible Tubing ID (in) kimblechase.com

8 372 VACUUM & AIRLESS Connectors / O-Rings / Pumps / Traps O-Ring Vacuum Connector with Joint Size 5 o-ring connector (5 mm ID) for use with HI-VAC manifolds. For applications utilizing standard taper glassware Supplied with one size 6 FKM o-ring borosilicate glass conforming to USP Type I and ASTM E438, Type I, Class A : Inner / /40 90 O-Ring Vacuum Connector with Stem Size 5 o-ring connector (5 mm ID) for use with and HI-VAC manifolds and adapters. For applications utilizing tubing Supplied with one size 6 FKM o-ring Stem OD for Tubing O-Ring Glass Connector Cap Size 5 o-ring connector (5 mm ID) to seal flasks or for use with HI-VAC manifold. Supplied with one size 6 FKM o-ring Manufactured from 33 expansion, low extractable borosilicate glass conforming to USP Type I and ASTM E438, Type I, Class A Approx. ID ULTRA-WARE Vacuum/Pressure Pump The GAST diaphragm pump offers a quiet, reliable vacuum/pressure source in a compact, light-weight design. Protected internal surfaces provide high resistance to corrosion and solvent attack. 3/8 hose barbs on both inlet and outlet /8 HP, 5V, 60Hz, 4.2A 7-5/8 long X 5-/8 wide X high 4.4 lbs. / 6.5 kg Ultimate Vacuum (inches Hg) Max Pressure (psi) One-Piece Vacuum Traps with 80 Connections Protects the mechanical pump from attack by corrosive vapors which can be condensed by using liquid nitrogen or dry ice/slurry mixtures. Connections are 80 apart for easy installation into a variety of vacuum systems Body OD x Overall Width x x x 30 Two-Piece Vacuum Traps with 80 Connections This trap protects the mechanical pump from attack by corrosive vapors which can be condensed by using liquid nitrogen or dry ice/ slurry mixtures. Outlets are 80 apart for easy installation into a variety of vacuum systems. Two-piece construction allows removal of condensate Connectors of series are barbed and fit /2 ID flexible tubing Connectors of series are plain Description /42 Vacuum Trap Tube; Capacity 00 ml; OD 35 mm; Length 230 mm /45 Vacuum Trap Tube; Capacity 200 ml; OD 40 mm; Length 260 mm /50 Vacuum Trap Tube; Capacity 800 ml; OD 60 mm; Length 405 mm /50 Vacuum Trap Tube; Capacity 350 ml; OD 50 mm; Length 295 mm /50 Vacuum Trap Tube; Capacity 300 ml; OD 45 mm; Length 340 mm /50 Vacuum Trap Tube; Capacity 500 ml; OD 55 mm; Length 325mm /50 Inner Vacuum Trap /50 Inner Vacuum Trap /42 Inner Vacuum Trap /50 Inner Vacuum Trap Toll Free: International:

9 Traps VACUUM & AIRLESS 373 Two-Piece Vacuum Traps This unit is positioned between the pump and manifold and is used with a Dewar flask containing liquid nitrogen or other coolant. Two-piece construction allows easy removal of condensed material which may damage the pump Inlet and outlet are # 5 o-ring connectors, which use size 6 o-rings (not supplied) for connection to other components in the vacuum system Size 5 o-ring connector uses a pinch clamp Main connector is size 50 and is supplied with a size 229 FKM o-ring Size 75 pinch clamp supplied with the unit to connect the two pieces of the trap together Description Dewar Flask, Aluminum Jacketed, 95 mm ID x 300 mm depth Size 28 Pinch Clamp, Fits O-Ring Conn. Size 2-5, screw lock provided Description Vacuum Trap Tube Accessories Large-Volume Two-Piece Vacuum Traps This trap is designed for large volume solvent removal by vacuum. O-ring joint provides a vacuum-tight, grease-free seal and permits the trap body to be easily disconnected from the stopper for cleaning Connections accept standard flexible /2 hose borosilicate glass conforming to USP Type I and ASTM E438, Type I, Class A Vacuum Gauge Trap For direct connection to vacuum gauges and to trap particulates which would contaminate these instruments when they are vented to the atmosphere. Comes packed with glass wool Manufactured from 33 expansion, low extractable borosilicate glass conforming to USP Type I and ASTM E438, Type I, Class A Capacity (ml) Fits Tubing ID (inches) x Overall Width OD, Length , x 30 Description Size 65 Pinch Clamp, Fits O-Ring Conn. Size 40, screw lock provided Large Volume Vacuum Trap This trap is designed for large volume solvent removal by vacuum. Connections accept standard flexible /2 hose borosilicate glass conforming to USP Type I and ASTM E438, Type I, Class A Capacity (ml) x x x 30 Description /35 Inner Vacuum Trap, 500 and 000 ml Capacities /35 Large Volume Vacuum Trap, 500 ml Flask /35 Large Volume Vacuum Trap, 000 ml Flask kimblechase.com

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