All-Russia D.I.Mendeleyev Scientific and Research Institute for Metrology (VNIIM)

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1 All-Russia D.I.Mendeleyev Scientific and Research Institute for Metrology (VNIIM) APMP 2015 TCFF Meeting 2 Nov Beijing, China Konstantin Popov k.v.popov@vniim.ru

2 Contents Participating in second round of CCM.FF-K Flow facility for large liquid flow range Flow facility for hydrocarbon liquid New primary standard for static liquid volume

3 Contents Participating in second round of CCM.FF-K Flow facility for large liquid flow range Flow facility for hydrocarbon liquid New primary standard for static liquid volume

4 CCM.FF-K3.2011: Updated time schedule (in progress) China Taiwan July 2013 May 2014 July 2014 France France July 2013 April 2014 August 2014? Netherlands Japan USA Russia August 2013 Dec October 2014? Austria Italy August 2013 Sept March 2015 April 2015

5 CCM.FF-K3.2011: Updated time schedule (in progress) China Taiwan July 2013 May 2014 July 2014 France France July 2013 April 2014 August 2014? Netherlands Japan USA Russia August 2013 Austria Dec October 2014 Italy? Customs clearance problems in Russia? August 2013 Sept March 2015 April 2015

6 CCM.FF-K3.2011: Updated time schedule (in progress) China Taiwan July 2013 May 2014 July 2014 France France July 2013 April 2014 August 2014? Netherlands Japan USA Russia August 2013 Austria Dec October 2014 Italy? 14 comparisons VNIIM (in progress) August 2013 Sept March 2015 April 2015

7 Contents Participating in second round of CCM.FF-K Flow facility for large liquid flow range Flow facility for hydrocarbon liquid New primary standard for static liquid volume

8 Flow meter calibration facility REFERENCE TOWER PSTR04 Water tower 23 m height Capacity ~ 100 m 3 Number of sections 15 Flow range ( ) m 3 /s DN mm Uncertainty ( )% 2200 dm 3 volume tank with active level switches for start/stop Uncertainty % June 2014

9 Flow meter calibration facility REFERENCE TOWER PSTR04 Water tower 22.5 m height Capacity ~ 100 m 3 Number of sections 15 Flow range ( ) m 3 /s DN mm Uncertainty ( )% 2200 dm 3 volume tank with active level switches for start/stop Uncertainty % May 2015

10 Flow meter calibration facility REFERENCE TOWER PSTR04

11 Flow meter calibration facility REFERENCE TOWER PSTR04 Sep 2015

12 Contents Participating in second round of CCM.FF-K Flow facility for large liquid flow range Flow facility for hydrocarbon liquid New primary standard for static liquid volume

13 Flow facility for hydrocarbon liquid In 2015 in Russia constructed new calibration facility for hydrocarbon liquid OilGasMetrology, Russia, Belgorod

14 Flow facility for hydrocarbon liquid Flowrate range ( ) m 3 /h Maximum pressure 1.6 Mpa Temperature of liquid (5 50) o C Viscosity (at 20 o C) Different liquids Kerosine Disel Oil (1) Oil (2)

15 Flow facility for hydrocarbon liquid Weight scale II class OIML 76-1 (1000 kg, 0.005%) Proving tank (1000 dm 3, 0.01 %) Proving tank (20 dm 3, 0.01 %) Density analyser 7835 ( kg/m 3, 0.1 kg/m 3 ) Ball prover ( m 3 /h, 0.03%) Ball prover ( m 3 /h, 0.03%) Piston prover ( m 3 /h, 0.05%)

16 Contents Participating in second round of CCM.FF-K Flow facility for large liquid flow range Flow facility for hydrocarbon liquid New primary standard for static liquid volume

17 State primary special standard of the unit static liquid volume (NEW) Since the end of 2014 VNIIM develops primary standard of the unit static liquid volume: Gravimetrical method of volume calibration Set of standard measuring tanks Set of mass comparators Set of weights E 1 F 1 M 1 Density analyzer Anton Paar Volume range dm 3 Expected uncertainty < 0.01%

18 Traceability chain National standard of mass (kg) VNIIM National standard of temperature (K) VNIIM Weights Gravimetrical method National standard of density (kg/m 3 ) VNIIM Volume tanks dm 3 (U >= 0.006%) Volume method Ball provers, piston-provers, tanks, Water tower with level switches (U = %) Volume flow meters

19 Structure of facility

20 Equipment for weighting Weight 20 kg E 1 comparator 40 kg, STD 0.1 g Set of weights (50 x 20 kg F 1 ) comparator 250 kg, STD 0.55 g comparator 1300 kg, STD 2.6 g

21 Equipment for weighting Weight 20 kg E 1 comparator 40 kg, STD 0.1 g Set of weights (50 x 20 kg F 1 ) comparator 250 kg, STD 0.55 g comparator 1300 kg, STD 2.6 g

22 Equipment for weighting Weight 20 kg E 1 comparator 40 kg, STD 0.1 g Set of weights (50 x 20 kg F 1 ) comparator 250 kg, STD 0.55 g comparator 1300 kg, STD 2.6 g

23 Equipment for weighting Weight 20 kg E 1 comparator 40 kg, STD 0.1 g Set of weights (50 x 20 kg F 1 ) comparator 250 kg, STD 0.55 g comparator 1300 kg, STD 2.6 g

24 Equipment for weighting Weight 20 kg E 1 comparator 40 kg, STD 0.1 g Set of weights (50 x 20 kg F 1 ) comparator 250 kg, STD 0.55 g comparator 1300 kg, STD 2.6 g

25 Equipment for weighting Weight 20 kg E 1 comparator 40 kg, STD 0.1 g Set of weights (50 x 20 kg F 1 ) comparator 250 kg, STD 0.55 g comparator 1300 kg, STD 2.6 g

26 Nearest plans with new facility In 2015 we plane to -start repair of building (for static volume facility) -make prover tank (overflow, 1000 dm 3 ) -recieve weights, mass comparators and some additional equipment In 2016 we plane -construct and check the work of equipment -take a part in comparisons: -bilateral comparison (Pilot lab VSL) with prover tank 1000 dm 3 -COOMET.M.FF-S6 (Comparison of the determination of static volume of reference metallic tanks, Volume of liquid: 1 L, 2 L, 5 L, 10 L, 20 L and 50 L) -APMP.M.FF-K4?? at the end of 2016 we have to end this work and report about our facility to Rosstandart (Russia)

27 Peer-review in 2015

28 Thanks for attention

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