Pfeiffer. Operating, assembly and maintenance instructions for discontinuous sampling valve Series 27i. 1. Design, operation and dimensions

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Operating, assembly and maintenance instructions for discontinuous sampling valve Series 27i This equipment may only be dismounted and disassembled by skilled staff, who are familiar with the assembly, the start-up and the operation of this product. Skilled staff in the sense of these repair and assembly instructions, are persons who, as a result of their training, knowledge, and experience, also their knowledge of the relevant standards are able to judge the tasks assigned to them and are able reconise possible dangers. 1. Design, operation and dimensions Design, operation and dimensions, as well as all further technical details may be found in the Data sheet < TB 27i_EN > for sampling valve series 27i / 27k Fig. 1 - Sampling valve Series 27i 0. Intorduction These instructions are intended to support the user in the assembly and repair of sampling valves of series 27i Technical details, as a result of further development of the valves mentioned in these instructions are subject to modification. The text and illustrations do not necessarily display the scope of supply, or an eventual order of spare parts. Drawings and graphics are not to scale. Customer related designs, which are not in accordance with our standard offer, are not shown. The transfer of these instructions to third parties is only allowed with the written approval of Pfeiffer Chemie- Armaturenbau GmbH. All documents are protected according to the laws of the German Copyright Act. The transmission and/or duplication of documents, even in abstracts, also the exploitation and communication of their content is not permitted, unless expressly granted. Violations are an offence and liable to claims for damages. We reserve all rights for the exercise of industrial property rights. 2. Installation, start-up and maintenance Guidelines for the installation, start-up and maintenance can be found in the respective operating instructions for sampling valves. Fig. 2 - Sectional view of sampling valve series 27i => Parts list, see table 1 on page 2 Page 1 of 8

Sampling valve Series 27i 3. Assembly of the sampling valve 3.1 Preparation for assembly Before assembling sample valve, clean all parts thoroughly, and lay them on a soft padded surface ( rubber mat ect.) Take into consideration, that parts made of plastic are generally soft and sensitive, in particular the sealing surfaces must be handled with care and not be damaged. Attention: To avoid cold corrosion of the screws in the bodies, the manufacturer has used a high performance lubricating grease (e.g.. Gleitmo 805. from. Fuchs). This grease however, may not be applied to valves which are used in an oxygen enviroment. Valves, which must be free of grease, especially for use in oxygen, an appropriate lubrication must be used. Note: The position and arrangement of the individual parts shown in the explosion drawing (Fig. 3) must be observed when assembling the valve. 3.2 Body assembly of the ball valve The assembly begins with the main body ( 1 ). Insert the lined spring washer ( 13 ) into the main body ( 1 ) The assembly position can be taken from the drawing ( Fig. 3 ). Fig. 3 - Explosion drawing of the sampling valve series 27i Pos. Qty. Description Materials 1 1 Main body 1.4571 2 1 Bonnet 1.4571 3 1 Ball 1.4571 4 1 Stem 1.4571 5 1 Stuffing box WN 1.4571 6 1 Bearing bush PTFE with 25% glass 7 1 Bearing bush PTFE with 25% carbon 8 1 Sealing ring set TFM 9 1 Ring PTFE 10 1 Ring PTFE 11 1 Spring washer set 1.8159 - Deltatone coated 12 1 V-ring packing 1.4305 / PTFE 13 1 Spring washer 1.4310 14 4 Screw A2-70 15 4 Screw A2-70 16 1 Insert PTFE 17 1 Retainer ring 1.4310 18 1 Setting screw A2-70 19 1 Drip insert sleeve PTFE 20 1 Sampling bottle Glass Table 1 - Parts list The sealing ring ( 8a ) is pressed onto the spring washer. With a light rotating movement, press the bearing sleeve ( 6 ) onto the stem. ( 4 ) Guide the stem ( 4 ) together with the bearing sleeve ( 6 ) through the intended stem opening in the inside of the main body ( 1 ). The sealing surface of the stem ( 4 ) must not be damaged. It is also necessary to ensure, that the bearing bush ( 6 ) together with the stem ( 4 ) is not slanted when inserting into the opening of the body ( 1 ). The stem ( 4 ) must now be rotated, so that the two flat ends are vertical to the working surface. Now the ball ( 3 ) can be carefully inserted. Place the body sealing rings ( 9 and 10 ) in the turned bore of the body ( 1 ). The bonnet ( 2 ) together with the insert ( 16 ) and the retainer ring ( 17 ) are pre-assembled, and fixed in position with the setting screw ( 18 ). Page 2 of 8

Place the drip insert bush ( 19 ) and the sealing ring ( 8b ) in the bonnet ( 2 ). The pre-assembled bonnet ( 2 ) is placed onto the body ( 1 ) and carefully pressed together. Rotate the bonnet ( 2 ) so that the connecting bores of both bodies ( 1 und 2 ) are aligned to each other. Apply grease to the screws ( 14 ). Now, screw the body ( 1 ) and the bonnet ( 2 ) together, evenly and in an alternating pattern. 5. Repairing the sampling valve 5.1 Replacing the V-ring packing If leakage is located at the stuffing box, können die PTFErings ( 12 ) may be defect. It is therefore recommended to check the condition of the packing. To dismantle the V-ring packing, proceed in reverse order to the assembly instructions as described in Section 3. As with all other plastic parts, check the sealing rings and the ball for damage, and if necessary replace these parts. 3.3 Final assembly of the sampling valve With a light rotating movement, push the V-ring packing (12 ) over the control shaft ( 4 ) and insert into the packing chamber of the body ( 1 ). Refer to the explosion drawing ( Fig. 3 ) for exact positioning of the V-rings. The spring washers ( 11 ) are placed on the V-packing The positioning of the spring washers can also be taken from the explosion drawing ( Fig. 3 ). The bearing sleeve ( 7 ) is pressed into the stuffing box flange ( 5 ). Following this, place the stuffing box flange ( 5 ) over the control shaft, and onto the body. With the greased screws ( 15 ) align and tighten the screws evenly in alternating pattern. Note: Before testing for leakage tightness, the valve should be operated once or twice, to enable the ball to sit correctly in the sealing rings, therefore ensuring a good sealing function. 5.2 Replacing the sealing ring and the ball If the ball valve does not shut-off tightly and shows signs of leakage, the sealing rings ( 8a und 8b ) and the ball ( 3 ) may be defect. It is therefore recommended to check these parts. To dismantle the sealing rings and the ball, proceed in reverse order to the assembly instructions, as described in Section 3. As with all other plastic parts, check the sealing rings and the ball for damage, and if necessary replace these parts. 5.3 Other repairs We recommend large repairs to be carried out in our works, by our skilled staff at Pfeiffer. The sampling container e.g. the sampling bottle ( 20 ) is screwed onto the sampling valve. Assembly of the sampling valve is now completed 4. Trouble shooting Action to be taken in the event of malfunction is described in the operating instructions for the sampling valve. You can also contact Pfeiffer directly if you require help. Page 3 of 8

Sampling valve Series 27i 6. Operating the sample valve 6.1 Important general instructions Depending on the media being used, it may be necessary to clean the chamber and the through bore after a sample has been taken. The operator must decide if and when this is necessary. It is essential to ensure, that before taking a sample, the sampling container (glass bottle etc.) is first adapted to the temperature of media being taken. Safety precautions need to be taken, when the media temperature exceeds 60 as a risk of scalding is possible. When taking samples, the general accident prevention regulations must be complied with at all times! 6.2 Sampling valve with hand-lever Screw on the sample bottle by hand as tightly as possible. Turn the hand-lever 180 until the bore is in the media flow. Turn back the hand-lever to allow the sample to flow into the bottle. Repeat this procedure until the required amount of media has been collected in the bottle. Unscrew the sample bottle, and if necessary seal bottle with a lid. 6.3 Sampling valve with hand-lever and protective case Open protective case. Screw on the sample bottle by hand as tightly as possible. Turn the hand-lever 180 until the bore is in the media flow. Turn back the lever to allow the sample to flow into the bottle. Repeat this procedure until the required amount of media has been collected in the bottle. Open the protective case, and remove the sample bottle, if necessary seal bottle with a lid. 6.4 Sampling valve with hand-lever and protective case with support Open protective case. Pull down the support on the handlever. Place the sample bottle in the PTFEseat of the support. Guide the support upwards. Close the protective case. Turn the handlever 180 until the bore is in the media flow. Turn back the handlever to allow the media to flow into the bottle. Repeat this procedure until the required amount has been collected in the bottle. Open the protective case, guide the support downwards, remove sample bottle, and if necessary seal bottle with a lid. 6.5 Sampling valve with automatic 180 rotary actuator and protective case 6.5.1 general automated sampling Open protective case. Screw on the sample bottle by hand as tightly as possible. Open the air supply valve of the automation unit. Attention: Before operating, refer to the respective operating instructions for the automation unit, which can be found in Section 7. Close the air supply at the automation unit. Open protective case, remove the sample bottle, if necessary seal bottle with a lid. Close the protective case. 6.5.2 automated sampling with back pressure indication Operating this type of sampling is identical to the operating instructions Section 6.5.1 In addition to the above mentioned version, the following function is included: - The automation switches off automatically and no further sample can be taken when the sample in the glass reaches the back pressure tube. Page 4 of 8

When attaching the bottle, avoid at all times bending the back pressure tube! 6.5.3 automatic sampling with pneumatic barrier Operating this type of sampling is identical to the operating instructions in Section 6.5.1 In addition to the above mentioned version, the following function is included: - The automation switches off automatically and no further sample can be taken if the protective case is opened during the sampling procedure. 6. 6 Sampling valve with automated 180 rotary actuator and protective case with support 6.6.1 general automatic sampling Open protective case. Pull down the support on the handlever. Place the sample bottle in the PTFEseat. Guide the support upwards. Open the air supply valve at automation unit. Attention: Before operating, refer to the respective operating instructions, which can be found in Section 7 (Operating the automation units) Close the air supply valve at the automation unit. Open the protective case, guide the support downwards, remove sample bottle, and if necessary seal the bottle with a lid. Close the protective case. 6.6.2 automatic sampling with back pressure indication Operating this type of sampling is identical to the operating instructions in Section 6.6.1 In addition to the above mentioned version, the following function is included: - The automation switches off automatically and no further sample can be taken, when the sample level in the bottle reaches the back pressure tube! When attaching the bottle, avoid at all times bending the back pressure tube! 6.6.3 automated sampling with pneumatic barrier Operating this type of sampling is identical to the operating instructions in Section 6.6.1 In addition to the above mentioned version, the following function is included: - The automation switches off automatically and no further sample can be taken when the protective case is opened during sampling procedure. 7. Operating the automation units 7.1 Automation with ON / OUT - Switch Note: The timing for filling the actuator with air venting, are preset timings, which were set before leaving our factory. Any alterations to these settings may only be made after first consulting Pfeiffer Chemie- Armaturenbau GmbH! Press the start button. A complete sampling cycle operation is carried out. Continue pressing the button until the required amount of media has been collected in the bottle. 7.2 Automation with counter Note: The pulse and interval times between actuation cycles, and the timming for filling with air and venting the actuator, are pre-set timings, which were set before leaving our factory. Any alterations to these settings may only be made after first consulting Pfeiffer Chemie- Armaturenbau GmbH! Select the number of actuating cycles at the counter. Attention: The selected number of actuating cycles must correspond to the volume of the sample bottle. Press the start button. The pre-selected number of actuating cycles to take samples are performed. The sampling finishes automatically after the selected numbe of actuating cycles has been completed. Page 5 of 8

Sampling valve Series 27i Attention! In the case of an opertion fault, press the emergency button immediately. 7.3 Automation with counter and timer switch Note: The pulse and interval times between actuation cycles, and the timing for filling the actuator with air, or venting, are pre-set timings, which were set before leaving our works. Any alterations to these settings may only be made after first consulting Pfeiffer Chemie- Armaturenbau GmbH! The required interval between each actuation cycle, can be set at the timer switch. Press the start button. The pre-selected number of actuating cycles to take samples, together with the pre-selected intervals are performed. The sampling finishes automatically after the selected number of actuating cycles have been completed. Attention! In case of an operation fault, press the emergency button immediately. Fig. 4 - Samsomatic - Time switch 3970 Select time range The switch-over range is located with the rotary knob located in the middle of the timer. With the dial arrow the required range can be set. Table 2 - Time range Determine which timing you require. The required cycle time can be set by turning the outer ring. A pointer indicates the cycle time. Set the number of actuation cycles at the counter. Attention: The selected number of actuating cycles must correspond to the volume of the sample bottle. Page 6 of 8

8. Circuit diagram Circuit diagram for the automation unit. Should you have any questions, please contact Pfeiffer Chemie-Armaturen GmbH Fig. 5 - Circuit diagram Page 7 of 8

9. Customer inquiries Details as per check list for repairs and inquiries. Table 3 - Check list Pfeiffer Edition July 2004 For your special requirements, please contact our technical sales department. Hooghe Weg 41 47906 Kempen Telefon: 02152 / 2005-0 Telefax: 02152 / 1580 E-Mail: vertrieb@pfeiffer-armaturen.com Internet: www.pfeiffer-armaturen.com Specifications are subject to change without notice Page 8 of 8 Operation and assembly EB 27i_DE PDF=758