SERVOTOUGH Oxy (1900)

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PROCESS ANALYSERS SERVOTOUGH (1900) The SERVOTOUGH offers reliability, flexibility, simplicity of use and installation for applications in the most hazardous and challenging of environments. The worlds leading paramagnetic technology, combined with advanced safety concepts and additional features make this the analyser against which all others should be judged. FEATURES Heated Sample Compartment - eliminates condensation issues for samples with a dewpoint up to 50ºC, significantly simplifying sample system requirements. Servomex Flowcube Technology - Internal Flow Sensor for peace of mind, improved safety, and preventative maintenance. Internal Pressure Compensation - compensates for pressure variations caused by either barometric or vent pressure fluctuations e.g. flare stacks. Hazardous Area Approved for Gases and Dusts Atex Cat 2 IECEx Zone 1 and Zone 21 USA CSA us Div 1, Zone 1 and Zone 21 Autovalidation - reduces the level of hands on maintenance via remote or local validation for the highest levels of confidence, and measurement availability. Low Cost of Ownership - no requirement for measurement reference gases or purge gases for certification or flammable samples. Long calibration intervals and cell life. SIL 2 Hardware Compliance - functional safety manual available. APPLICATIONS Process control. Safety critical oxidation, such as ethylene oxide and propylene oxide purity. Feedstock clean up. Inerting/blanketing. Flare stack analysis.

KEY FEATURES Heated Sample An innovative, fully heated sample compartment removes the requirement for a sample conditioning system on samples with a dew point of up to 50ºC (122ºF ). Responsible for up to 80% of failures in comparable units, sample conditioning failure is a major cause of unplanned downtime. The heated sample compartment design reduces this risk of downtime by limiting the need for coolers, dryers and other conditioning devices. This design improves operational cost as well as initial system and integration costs, making it especially ideal for use where wet gases are to be measured. Servomex Flowcube Technology Servomex s determination to deliver users the most safe, accurate and reliable levels of measurement remains at the forefront of our design philosophy therefore our unique flow sensor technology has been placed after the measurement transducer, enabling accurate flow trending and alarm setting for many applications including safety critical applications. * Internal Pressure Compensation An integrated pressure compensation system that not only compensates for barometric pressure but also for sample vent back pressure variations e.g. from flare stacks, enabling emission compliance targets to be easily met. Low Cost of Ownership Both the flow sensor and pressure compensation system technologies report via the instrument s standard communication options. This permits simplified installation which can reduce the number of discrete devices needed and greatly reduces complex cabling issues. * Not suitable for gas mixtures that contain hydrogen and/or helium at concentrations over 10% of the total mixture. HAZARDOUS AREA APPROVALS ATEX: II 2 GD, Ex ia d IIC T4 Gb (-10 C Ta +50 C)* Ex tb IIIC T90 C Db (-10 C Ta +50 C)* IECEx : Ex ia d IIC T4 Gb (-10 C Ta +50 C)* Ex tb IIIC T90 C Db (-10 C Ta +50 C)* USA CSA us Class I, Division 1, Groups A, B, C, D T4 (-10 C Ta +50 C)* Class II, Division 1, Groups E, F, G (-10 C Ta +50 C)* Class III, (-10 C Ta +50 C)* Class I, Zone 1, Ex ia d IIC T4 (-10 C Ta +50 C)* Class I, Zone 21, Ex td T90 C Class I, Zone 1, AEx ia d IIC T4 (-10 C Ta +50 C)* Class I, Zone 21, Ex td T90 C * (+14 F Ta +122 C) EC DIRECTIVE COMPLIANCE The SERVOTOUGH (1900) complies with the following EC Directives *: Electromagnetic Compatibility Directive 2004/108 EC Atex Directive (94/9/EC) * See certification supplement manual for further information Page 2

SPECIFICATIONS Gas measured: gen TECHNOLOGY: Paramagnetic HAZARDOUS AREA: ATEX Cat. 2 Gases and dusts: IECEx Zone 1 and Zone 21 USA CSA us Div 1,Zone 1 and Zone 21 PERFORMANCE: Measurement range: 0-21 % O 2 Lower detection limit: < ± 50ppm O 2 Linearity error: No measurable error Repeatability error: 0.02% O 2 Intrinsic error (accuracy): < ±0.05% O 2 (based on ± 95% confidence limits) Response time (T 90 ): <6 seconds at 200ml/min and 1l/min Zero drift per week: <0.05% O 2 /week Span drift per week: <0.05% O 2 /week Temperature Co-efficient zero: <±0.03% O 2 /10 C Sample vent pressure effects: Pressure compensation not : 1% change in sample vent pressure corresponds to a 1% change in reading Pressure compensation : 1% change in sample vent pressure corresponds to a <0.05% change in reading Sample flow variations: A change in flow from 50-250ml/min (12-70l/hr internal bypass option) will cause a zero change of <0.1% O 2 and a span change of <0.5% of reading SIGNAL OUTPUTS: As standard each unit comes with: Analogue outputs: One isolated 4-20mA / 0-20mA Analogue output range: User selectable over the measurement range (minimum range 0-1% O 2 ) Alarms: Two volt free single pole double throw relays (30V dc 1A) Status signals: Four volt free single pole double throw relays (30V dc 1A): instrument fault, maintenance required, service in progress and ma range indication Digital Modbus RTU (RS485) communications: Ethernet (Modbus TCP) OPERATING ENVIRONMENT: Temperature: Operating: -10 C to +50 C (+14 F to +122 F) Storage: -20 C to +60 C (-4 F to +140 F) Relative humidity: 0-95% RH, non-condensing Warm up time: Typically <4 hours (at 20 C ambient (68 F) depending on application and environment) Operating altitude range: - -500 to 2000 metres Ingress protection: IP66 and NEMA 4X FLOW SENSOR: Accuracy: < ± 5% of full scale for 100% N 2 * Minimum detectable change: 1% of full scale Response time (T 63 ): <15 seconds Ambient temperature co-efficient span: <2% of full scale per 10 C Calibration interval: 6 to 12 months * For gases with higher molecular weights than N 2, the accuracy will be < ± 10% of full scale. Page 3

SPECIFICATIONS SAMPLE GAS: The sample gas must be clean, non-corrosive and free from oil and condensates Particulate size: <3 µm Dew point: Unheated sample compartment: a minimum 5 C (9 F) below ambient temperature Heated sample compartment: maximum sample dewpoint 50 C (122 F) Flow rates:* Standard: 50 to 250ml/min (200ml/min recommended) Optional high flow internal bypass: 50 to 70l/hr (60l/hr recommended) Sample connection: 1/4 NPT female, 6mm tube or 1/4 tube Sample wetted Standard measurement option: 304SS, 316SS, borosilicate glass, platinum, materials: platinum/iridium alloy, electroless nickel, Viton Solvent resistant option: 304SS, 316SS, borosilicate glass, platinum, platinum/iridium alloy, electroless nickel, Chemraz 555, PTFE Maximum sample 24kPa absolute (18psi absolute) vent pressure:* Maximum inlet 02.kPa (0.03psi) relative to sample vent pressure pressure:* * The pressure and flow of sample gases must be externally regulated to meet the above requirements For the high flow internal bypass option, the maximum sample vent pressure and maximum sample inlet pressure are limited to: 122.8kPa (17.8psia) and 1.4kPa (0.2psi) relative to sample vent pressure respectively CORROSIVE PURGE GAS: Recommended gas: Instrument grade air Flow rate: 40 to 60ml/min Purge inlet connection: 1/4 NPT female Purge outlet: Through analyser breather, no external connection POWER SUPPLY: 100-120 or 220-240V AC, 50/60Hz, 50 VA The output will change by <1 % FSR for a deviation from the selected supply voltage of up to 15% The output will change by <1 % FSR for a 5% deviation from the selected supply frequency SERVICE & SUPPORT For new installations and replacement of older Servomex and competitor products, we will work with you to develop a bespoke service and support package, ensuring full measurement availability and plant operation within your timescales and budget. SERVOSPARES To ensure the integrity and optimum performance of your Servomex product, we recommend fitting only factory authorised spare parts. This is particularly important for all hazardous area certified products. SERVOSURE Ensure your Servomex analyser is properly commissioned and delivers optimum performance with a maintenance contract, service programme and extended warranty. SERVOTECH Make the most of your Servomex gas analyser by attending a training course at one of our training centres in Europe, USA or Asia or on your own site. SERVOHELP Whether you have a simple question or complex process challenge, our local offices and global support network are here to help you. Page 4

DESCRIPTION Analyser certification: 3 certified versions of the analyser are available Atex IECEx USA CSA us Supply voltage: 2 versions of supply voltage are available 100-120V 220-240V Measurement: Stainless Steel pipework with Viton seals Standard Stainless Steel pipework with Chemraz and PTFE seals allowing enhanced solvent resistance Solvent resistant Sample flow: Standard flow option of 250ml/min 250ml/min An internal by-pass allows inlet flows of up to 1l/min 1l/min Sample heating: The measurement transducer in the is heated to approximately 65ºC (149ºF) for measurement stability. In this configuration sample gases must be supplied to the analyser at a dewpoint of at least 5ºC (9ºF) below that of ambient temperature Sample heating not required The measurement transducer in the and the full sample pipework including the sample inlet and outlet connections are heated to 60ºC (140ºF). This allows the gases up to a dew point of 50ºC (122ºF) to be sampled directly into the analyser Sample heating Internal pressure compensation: The uncorrected gas measurement is directly affected by changes in atmospheric pressure and any sample vent back pressures on the sample outlet. A 1% change in pressure will directly affect the measurement by 1% of reading. This needs to be considered when looking at the measurement performance required Pressure compensation not required The fitting of the internal pressure transducer reduces the effect of pressure changes by a twentieth. A 1% change in pressure will result in a less than 0.05 % change in sample reading Pressure compensation Flowcube internal flow sensor: The measurement of the analyser is highly reliable and has internal diagnostics to ensure correct operation, yet in low flow conditions the measurement accuracy may be affected and this cannot be diagnosed by the instrument without a flow sensor Flow sensor not required Our Flowcube technology offers an internal solid state flow sensor directly to the outlet of the measurement transducer, ensuring that the measurement gas is flowing through the transducer at all times for maximum reliability and safety Flow sensor Flowcube technology offers one high and twolow flow alarms which can be configured to be inactive or to indicate a fault or maintenance required status, via the instrument relay output and the digital communications. Flow level is also reported via the digital communications or the display, so flow trending and maintenance of systems elements can be scheduled. (Note: the flow sensor is currently not suitable for gas mixtures that contain hydrogen and/or helium at concentrations over 10% of the total mixture) Page 5

DESCRIPTION Autovalidation/ calibration: Autovalidation/calibration is not An option card is available that allows the instrument to control validation or calibration gases automatically (volt free single pole double throw relays: 30V dc 1A) This option can also be used for remote calibration of the analyser. Autovalidation using test gases allows the maximum confidence in the measurement to be gained on a regular basis without the expense of using personnel for routine validation. During autovalidation the analyser indicates that it is off line from the process with a service in progress relay contact and if it should detect that the measurement performance is outside preset tolerances it will indicate that maintenance is required through a second relay contact Autovalidation not required Autovalidation Digital communications: This allows for the analyser to be fully maintained and configured remotely. It also allows for a greater level of remote diagnostics to be carried out above that supplied by the standard relay contacts Modbus RTU (RS485) Modbus RTU (RS485) Ethernet (Modbus TCP) Ethernet (Modbus TCP) Sample inlet: Allows the connection of 1/4 NPT male fittings directly to the analyser Allows the connection of 1/4" OD tube directly to the analyser Allows the connection of 6mm OD tube directly to the analyser 1/4 NPT female 1/4 OD compression fitting 6mm OD Compression fitting Enclosure options: IP66 Breather as standard allows the pressure within the enclosure to be the same as the surrounding atmosphere Breather A 1/4 NPT female inert gas (normally instrument air or nitrogen) inlet fitting allows inert gas to be supplied to the analyser to prevent the build up of any corrosive gases within the sample compartment in environments where corrosive gases may be present, this will extend the operational life of the analyser in such environments Corrosive purge Gland/conduit entries: As standard the analyser is supplied with 4 gland entries, 2 x 1/2" NPT female and 2 x 3/4" NPT female Adapters to M20 gland entries supplied Adapters to PG13.5 gland entries supplied NPT Metric M20 PG 13.5 Operators manuals: An Operators manual contains all the information needed to install and safely set up the analyser Service manual: A Service manual (in only) contains technical descriptions, fault diagnosis, parts removal, refitting and test instructions, tool and test equipment lists, and electrical drawings. It is intended for use by Servomex trained service personnel Not required Functional safety manual: International instructions for those planning, designing, installing, commissioning and maintaining Safety Instrumented Systems. Demonstrates analysers hardware compliance to SIL 2 of IEC 61508 Not required Page 6

OXY PACKS We have developed Packs A to E covering all the main applications to enable a quick turnaround from specification to delivery. A. Entry Pack: Suitable for general oxygen applications B. Hot Pack: Entry pack, plus fully heated sample cell for higher dewpoint samples C. Autoval Pack: Hot pack, plus autovalidation and autocalibration functions for highest levels of confidence and lowest levels of field support D. Pressure and Hot pack, plus internal pressure compensation and internal flow sensor for peace of Flow Pack mind and optimum measurement performance E. Complete Pack: The optimum package for all your measurement needs F. User Configured: All configurations not covered above QUOTATION FORM Analyser Certification Supply Voltage Measurement Sample Flow Sample Heating Internal Pressure Compensation Internal Flow Sensor Autovalidation Digital Communications Sample Inlet Enclosure Options Gland Entries Operators Manual Service Manual Functional Safety Manual Purchase Order No. Contact details: Delivery date: ------------------------------ ------------------ ------------------------------ ------------------------------ Fax back to Business Centre ------------------------------ (refer to fax numbers on page 8) A B C D E F ATEX IECEx USA CSA us 100-120V 220-240V Standard Solvent resistant 250ml/min 1l/min Sample heating not required Sample heating Pressure compensation not required Pressure compensation Flow sensor not required Flow sensor Autovalidation not required Autovalidation Modbus RTU (RS485) Modbus TCP (Ethernet) 1/4 NPT (F) 1/4 OD compression fitting 6mm OD compression fitting Breather Corrosive purge NPT Metric M20 PG 13.5 French German Not required Not required Tick the required box for each option Page 7

DIMENSIONS Dimensions shown in millimetres Weight: 26kg nominal BUSINESS CENTRES EUROPE (Europe and Africa) Tel: +31 (0)79 330 1581 Fax: +31 (0)79 342 0819 Toll Free : 00800 7378 6639 USA & CANADA Tel: +1 281 295 5800 Fax: +1 281 295 5899 Toll Free: 1 800 862 0200 LATIN AMERICA/MEXICO Tel: +55 11 5188 8166 Fax: +55 11 5188 8169 ASIA PACIFIC Tel: +86 (0)21 6489 7570 Fax: +86 (0)21 6442 6498 INDIA AND MIDDLE EAST Tel: +91 22 67100359/60 Fax: +91 22 66778896 TECHNICAL CENTRE Servomex Group Limited Crowborough East Sussex, UK TN6 3FB Tel: +44 (0)1892 652181 Fax: +44 (0)1892 662253 SYSTEMS ENGINEERING CENTRES Crowborough, UK Tel: +44 (0)1892 652181 Houston, USA Tel: +1 281 295 5800 Shanghai, China Tel: +86 (0)21 6489 7570 Mumbai, India Tel: +91 22 67100359/60 www.servomex.com www.hummingbirdsensing.com Servomex has a policy of constant product improvement and reserves the right to change specifications without notice. Servomex Group Limited. 2010. A Spectris company. All rights reserved. PB1910 Rev.3 05/10 E