Chapter 20. Planning Accelerated Life Tests. William Q. Meeker and Luis A. Escobar Iowa State University and Louisiana State University

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Chapter 20 Planning Accelerated Life Tests William Q. Meeker and Luis A. Escobar Iowa State University and Louisiana State University Copyright 1998-2008 W. Q. Meeker and L. A. Escobar. Based on the authors text Statistical Methods for Reliability Data, John Wiley & Sons Inc. 1998. January 13, 2014 3h 42min 20-1

Planning Accelerated Life Tests Chapter 20 Objectives Outline reasons and practical issues in planning ALTs. Describe criteria for ALT planning. Illustrate how to evaluate the properties of ALTs. Describe methods of constructing and choosing among ALT plans One-variable plans. Two-variable plans. Present guidelines for developing practical ALT plans with good statistical properties. 20-2

Possible Reasons for Conducting an Accelerated Test Accelerated tests (ATs) are used for different purposes. These include: ATs designed to identify failure modes and other weaknesses in product design. ATs for improving reliability ATs to assess the durability of materials and components. ATs to monitor and audit a production process to identify changes in design or process that might have a seriously negative effect on product reliability. 20-3

Motivation/Example Reliability Assessment of an Adhesive Bond Need: Estimate of the B10 of failure-time distribution at 50 C (expect 10 years). Constraints 300 test units. 6 months for testing. 50 C test expected to yield little relevant data. 20-4

Model and Assumptions Failure-time distribution is loglocation-scale [ log(t) µ Pr(T t) = F(t;µ,σ) = Φ σ ] µ = µ(x) = β 0 +β 1 x, where x = 11605 temp C+273.15. σ does not depend on the experimental variables. Units tested simultaneously until censoring time t c. Observations statistically independent. 20-5

Assumed Planning Information for the Adhesive Bond Experiment The objective is finding a test plan to estimate B10 with good precision. Weibull failure-time distribution with same shape parameter at each level of temperature σ and location scale parameter µ(x) = β 0 +β 1 x, where x is C in the Arrhenius scale..1% failing in 6 months at 50 C. 90% failing in 6 months at 120 C. Result: Defines failure probability in 6 months at all levels of temperature. If σ is given also, defines all model parameters. 20-6

Engineers Originally Proposed Test Plan for the Adhesive Bond Temp Allocation Failure Expected C Proportion Number Probability Number Failing π i n i p i E(r i ) 50 0.001 110 1/3 100 0.60 60 130 1/3 100 1.00 100 150 1/3 100 1.00 100 20-7

Adhesive Bond Engineers Originally Proposed Test Plan n = 300, π i = 1/3 at each 110 C, 130 C, 150 C 10 5 10 4 Days 10 3 10 2 10 1 50% 10% 5% 10 0 40 60 80 100 120 140 160 Degrees C 20-8

Critique of Engineers Original Proposed Plan Arrhenius model in doubt at high temperatures (above 120 C). Question ability to extrapolate to 50 C. Data much above the B10 are of limited value. Suggestion for improvement: Test at lower more realistic temperatures (even if only small fraction will fail). Larger allocation to lower temperatures. 20-9

Engineers Modified Traditional ALT Plan with a Maximum Test Temperature of 120 C Temp Allocation Failure Expected C Proportion Number Probability Number Failing π i n i p i E(r i ) 50 0 80 1/3 100.04 4 100 1/3 100.29 29 120 1/3 100.90 90 For this plan and the Weibull-Arrhenius model, Ase[log( t.1 (50))] =.4167. The asymptotic precision factor for a 95% confidence interval of t.1 (50) is R = exp(1.96 Ase) = 2.26. 20-10

Simulation of Engineers Modified Traditional ALT Plan Levels = 80,100,120 Degrees C, n=100,100,100 Censor time=183,183,183, parameters= -16.74,0.7265,0.5999 Days 50000 20000 10000 5000 2000 1000 500 200 100 50 20 10 5 Results based on 300 simulations Lines shown for 50 simulations Precision factors R for quantile estimates at 50 Degrees C R( 0.1 quantile)= 2.288 R( 0.5 quantile)= 2.484 R(Ea)= 1.165 40 50 60 70 80 90 100 120 Degrees C on Arrhenius scale 10% 20-11

Methods of Evaluating Test Plan Properties Assume inferences needed on a function g(θ) (one-to-one and all the first derivatives with respect to the elements of θ exist, and are continuous). Properties depend on test plan, model and (unknown) parameter values. Need planning values. Asymptotic variance of g( θ) [ g(θ) Avar[g( θ)] = θ ] Σ θ [ g(θ) Simple to compute (with software) and general results. θ ]. Use Monte Carlo simulation. Specific results, provides picture of data, requires much computer time. 20-12

Statistically Optimum Plan for the Adhesive Bond Objective: Estimate B10 at 50 C with minimum variance. Constraint: Maximum testing temperature of 120 C. Inputs: Failure probabilities p U =.001 and p H =.90. 20-13

Contour Plot Showing log 10 {Avar[log( t.1 )]/minavar[log( t.1 )]} as Function of ξ L,π L to Find the Optimum ALT Plan 1.0 0.8 0.6 π L 0.4.1.2 0.2 0.0.5 1 2 0.0 0.2 0.4 0.6 0.8 1.0 ξ L 20-14

Adhesive Bond Weibull Distribution Statistically Optimum Plan Allocations: π Low =.71 at 95 C, π High =.29 at 120 C 10 5 10 4 Days 10 3 10 2 10 1 50% 10% 5% 10 0 40 60 80 100 120 140 160 Degrees C 20-15

Simulation of the Weibull Distribution Statistically Optimum Plan Levels = 95,120 Degrees C, n=212,88 Censor time=183,183, parameters= -16.74,0.7265,0.5999 Days 50000 20000 10000 5000 2000 1000 500 200 100 50 20 10 5 Results based on 300 simulations Lines shown for 50 simulations Precision factors R for quantile estimates at 50 Degrees C R( 0.1 quantile)= 2.103 R( 0.5 quantile)= 2.309 R(Ea)= 1.155 40 50 60 70 80 90 100 120 Degrees C on Arrhenius scale 10% 20-16

Weibull Distribution Statistically Optimum Plan Temp Allocation Failure Expected C Proportion Number Probability Number Failing π i n i p i E(r i ) 50.001 95.71 213.18 38 120.29 87.90 78 For this plan and the Weibull-Arrhenius model, Ase[log( t.1 (50))] =.3794 20-17

Adhesive Bond Lognormal Distribution Statistically Optimum Plan Allocations: π Low =.74 at 78 C, π High =.26 at 120 C 10 5 10 4 Days 10 3 10 2 10 1 10 0 50% 5% 10% 40 60 80 100 120 140 160 Degrees C 20-18

Lognormal Distribution Statistically Optimum Plan Temp Allocation Failure Expected C Proportion Number Probability Number Failing π i n i p i E(r i ) 50.001 78.74 233.13 30 120.26 77.90 69 For this plan and the Lognormal-Arrhenius model, Ase[log( t.1 (50))] =.2002 20-19

Critique of the Statistically Optimum Plan Still too much temperature extrapolation (to 50 C). Only two levels of temperature. Optimum Weibull and lognormal plans quite different 95 C and 120 C for Weibull versus. 78 C and 120 C for lognormal. In general, optimum plans not robust to model departures. 20-20

Want a Plan That Meets practical constraints and is intuitively appealing. Is robust to deviations from assumed inputs. Has reasonably good statistical properties. 20-21

Criteria for Test Planning Subject to constraints in time, sample size and ranges of experimental variables, Minimize Var[log( t p )] under the assumed model. Maximize the determinant of the Fisher information matrix. Minimize Var[log( t p )] under more general or higher-order model(s) (for robustness). Control the expected number of failures at each experimental condition (since a small expected number of failures at critical experimental conditions suggests potential for a failed experiment). 20-22

Types of Accelerated Life Test Plans Optimum plans Maximize statistical precision. Traditional plans Equal spacing and allocation; may be inefficient. Optimized (best) compromise plans require at least 3 levels of the accelerating variable (e.g., 20% constrained at middle) and optimize lower level and allocation. 20-23

General Guidelines for Planning ALTs (Suggested from Optimum Plan Theory) Choose the highest level of the accelerating variable to be as high as possible. Lowest level of the accelerating variable can be optimized. Allocate more units to lower levels of the accelerating variable. Test-plan properties and optimum plans depend on unknown inputs. 20-24

Practical Guidelines for Compromise ALT Plans Use three or four levels of the accelerating variable. Limit high level of the accelerating variable to maximum reasonable condition. Reduce lowest level of the accelerating variable (to minimize extrapolation) subject to seeing some action. Allocate more units to lower levels of the accelerating variable. Use statistically optimum plan as a starting point. Evaluate plans in various meaningful ways. 20-25

Adjusted Compromise Weibull ALT Plan for the Adhesive Bond (20% Constrained Allocation at Middle) Temp Allocation Failure Expected C Proportion Number Probability Number Failing π i n i p i E(r i ) 50.001 78.52 156.03 5 98.20 60.24 14 120.28 84.90 76 For this plan with the Weibull-Arrhenius model, Ase[log( t.1 (50))] =.4375. 20-26

Adhesive Bond Adjusted Compromise Weibull ALT Plan π Low =.52, π Mid =.20, π High =.28 10 5 10 4 Days 10 3 10 2 10 1 50% 10% 5% 10 0 40 60 80 100 120 140 160 Degrees C 20-27

Simulation of the Adhesive Bond Compromise Weibull ALT Plan Levels = 78,98,120 Degrees C, n=155,60,84 Censor time=183,183,183, parameters= -16.74,0.7265,0.5999 Days 50000 20000 10000 5000 2000 1000 500 200 100 50 20 10 5 Results based on 300 simulations Lines shown for 50 simulations Precision factors R for quantile estimates at 50 Degrees C R( 0.1 quantile)= 2.381 R( 0.5 quantile)= 2.645 R(Ea)= 1.177 40 50 60 70 80 90 100 120 Degrees C on Arrhenius scale 10% 20-28

Basic Issue 1: Choose Levels of Accelerating Variables Need to Balance: Extrapolation in the acceleration variable (assumed temperature time relationship). Extrapolation in time (assumed failure-time distribution). Suggested Plan: Middle and high levels of the acceleration variable expect to interpolate in time. Low level of the acceleration variable expect to extrapolate in time. 20-29

Basic Issue 2: Allocation of Test Units Allocate more test units to low rather than high levels of the accelerating variable. Tends to equalize the number of failures at experimental conditions. Testing more units near the use conditions is intuitively appealing. Suggested by statistically optimum plan. Need to constrain a certain percentage of units to the middle level of the accelerating variable. 20-30

Properties of Compromise ALT Plans Relative to Statistically Optimum Plans Increases asymptotic variance of estimator of B10 at 50 C by 33% (if assumptions are correct). However it also, Reduces low test temperature to 78 C (from 95 C). Uses three levels of accelerating variable, instead of two levels. Is more robust to departures from assumptions and uncertain inputs. 20-31

Generalizations and Comments Constraints on test positions (instead of test units): Consider replacement after 100p% failures at each level of accelerating variable. Continue tests at each level of accelerating variable until at least 100p% units have failed. Include some tests at the use conditions. Fine tune with computer evaluation and/or simulation of user-suggested plans. Desire to estimate reliability (instead of a quantile) at use conditions. Need to quantify robustness. 20-32

ALT with Two or More Variables Moderate increases in two accelerating variables may be safer than using a large amount of a single accelerating variable. There may be interest in assessing the effect of nonaccelerating variables. There may be interest in assessing joint effects of two more accelerating variables. 20-33

Choosing Experimental Variable Definition to Minimize Interaction Effects Care should be used in defining experimental variables. Guidance on variable definition and possible transformation of the response and the experimental models should, as much as possible, be taken from mechanistic models. Proper choice can reduce the occurrence or importance of statistical interactions. Models without statistical interactions simplify modeling, interpretation, explanation, and experimental design. Knowledge from mechanistic models is also useful for planning experiments. 20-34

Examples of Choosing Experimental Variable Definition to Minimize Interaction Effects For humidity testing of corrosion mechanism use RH and temperature (not vapor pressure and temperature) For testing dielectrics, use size and volts stress (e.g., mm and volts/mm instead of mm and volts) For light exposure, use aperture and total light energy (not aperture and exposure time) To evaluate the adequacy of large-sample approximations with censored data, use % failing and expected number failing (not % failing and sample size). 20-35

Comparison of Experimental Layout with Volts/mm Versus Size and Volts Versus Size Size (mm) 1.0 1.5 2.0 2.5 3.0 Size (mm) 1.0 1.5 2.0 2.5 3.0 50 100 150 200 100 300 500 Voltage Stress (Volts/mm) Volts 20-36

Comparison of Experimental Layout with Volts versus Size and Volts/mm versus Size Size (mm) 1.0 1.5 2.0 2.5 3.0 Size (mm) 1.0 1.5 2.0 2.5 3.0 50 100 200 300 100 200 300 400 Volts Voltage Stress (Volts/mm) 20-37

Insulation ALT From Chapter 6 of Nelson (1990) and Escobar and Meeker (1995) Engineers needed rapid assessment of insulation life at use conditions. 1000/10000 hours available for testing. 170 test units available for testing. Possible experimental variables: VPM (Volts/mm) [accelerating]. THICK (cm) [nonaccelerating]. TEMP ( C) [accelerating]. 20-38

Multiple Variable ALT Model and Assumptions Failure-time distribution [ log(t) µ Pr(T t) = F(t;µ,σ) = Φ σ ]. µ = µ(x) is a function of the accelerating (or other experimental) variables. σ does not depend on the experimental variables. Units tested simultaneously until censoring time t c. Observations statistically independent. 20-39

Models Used in Examples σ constant. µ = β 0 +β 1 log(vpm) µ = β 0 +β 1 log(vpm)+β 2 log(thick) [ 11605 µ = β 0 +β 1 log(vpm)+β 2 temp C+273.15 ] 20-40

Insulation ALT 3 3 VPM THICK Factorial Test Plan Standardized Factor 1-0.2 0.0 0.2 0.4 0.6 0.8 1.0 1.2 0.4 p=3.2x10-6 p=.01 p=.1 p=.5 p=.99 Thickness (cm) 0.35 0.3 0.25 0.2 0.15 p UU =1.8x10-6 p=1-2 -1 0 1 Standardized Factor 2 80 100 120 140 160 180 200 Electrical Stress (volts per mm) 20-41

The ALT Design Problem Design test plan to estimate life at the use conditions of VPM U = 80 volts/mm, THICK U = 0.266 cm, TEMP U = 120 C. Interest centers on a quantile in lower tail of life distribution, t p = exp [ µ(x U )+Φ 1 (p)σ ]. Need to choose levels of the accelerating variable(s) x 1,...,x k and allocations π 1,,π k to those conditions. Equal allocation can be a poor choice. 20-42

Multi-Variable Experimental Region Maximum levels for all variables: VPM H = 200 volts/mm THICK H = 0.355 cm TEMP H = 260 C. Explicit minimum levels for all experimental variables: VPM A = 80volts/mm THICK A = 0.163cm TEMP A = 120 C (also stricter implicit limits for VPM and TEMP). May need to restrict highest combinations of accelerating variables; e.g., constrain by equal failure-probability line (by using a maximum failure probability constraint p or equivalently a standardized censored failure time ζ constraint). 20-43

Insulation ALT VPM THICK Optimum Test Plan Standardized Factor 1-0.2 0.0 0.2 0.4 0.6 0.8 1.0 1.2 Thickness (cm) 0.4 0.35 0.3 0.25 0.2 0.15 p UU =1.8x10-6 p=.33 p=1-2 -1 0 1 Standardized Factor 2 80 100 120 140 160 180 200 Electrical Stress (volts per mm) 20-44

Degenerate and Nondegenerate Test Plans to Estimate t p Degenerate plans: Test all units at x U. Test two (or more) combinations of the experimental variables on a line with slope s passing through x U. Nondegenerate practical plans: Test at three (or more) noncollinear combinations of the experimental variables in the plane. 20-45

Optimum Degenerate Plan: Technical Results When acceleration does not help sufficiently, it is optimum to test all units at the use conditions. Otherwise there is at least one optimum degenerate test plan in the x 1 x 2 plane. Some units tested at highest levels of accelerating variables. Optimum degenerate plan corresponds to a single-variable optimum. 20-46

Splitting Degenerate Plans It is possible to split a degenerate plan into a nondegenerate optimum test plan (maintaining optimum Var[log( t p )]). Use secondary criteria to chose best split plan. Split x i = (x 1i,x 2i ) with allocation π i into x i1 = (x 1i1,x 2i1 ) and x i2 = (x 1i2,x 2i2 ) with allocations π i1 and π i2 (where π i1 +π i2 = π i ) π i1 x i1 +π i2 x i2 = π i x i. Can introduce a p constraint [or a ζ constraint where p = Φ(ζ )]. Can also split compromise plans and maintain Var[log( t p )]. 20-47

Insulation ALT VPM THICK Optimum Test Plan with p /ζ constraint Standardized Factor 1-0.2 0.0 0.2 0.4 0.6 0.8 1.0 1.2 0.4 p=.28 p=1 Thickness (cm) 0.35 0.3 0.25 0.2 0.15 p UU =1.8x10-6 -2-1 0 1 Standardized Factor 2 80 100 120 140 160 180 200 Electrical Stress (volts per mm) 20-48

Insulation ALT VPM THICK 20% Compromise Test Plan with p /ζ constraint Standardized Factor 1 0.0 0.5 1.0 0.4 p=.33 p=.99 Thickness (cm) 0.35 0.3 0.25 0.2 0.15 p UU =1.8x10-6 p=1-2 -1 0 1 Standardized Factor 2 80 100 120 140 160 180 200 220 Electrical Stress (volts per mm) 20-49

Comparison of Test Plans and Properties for the VPM THICK ALT No Interaction Model Interaction Model Plan V[log( t p )] F V[log( t p )] F 3 3 144 2.4 10 3 145 1.2 10 5 Factorial from Nelson (1990) Optimum degenerate 80.1 0.0 0.0 No ζ Optimum split 80.1 7.3 10 4 0.0 No ζ Optimum degenerate 131 0.0 0.0 ζ = 2.5454 Optimum split 131 1.6 10 3 138 1.7 10 5 ζ = 2.5454 20% Compromise degenerate 96.1 0.0 9710 0.0 ζ = 4.04 20% Compromise split 96.1 7.0 10 3 102 1.2 10 4 ζ = 4.04 20-50

Insulation ALT VPM TEMP 3 3 Factorial Test Plan Standardized Factor 1-0.2 0.0 0.2 0.4 0.6 0.8 1.0 1.2 Temperature (degrees C) 260 240 220 200 180 160 140 120 p=.00016 p UU =1.8x10-6 p=.01 p=.1 p=.5 p=.99 p=1-0.2 0.0 0.2 0.4 0.6 0.8 1.0 1.2 Standardized Factor 2 80 100 120 140 160 180 200 Electrical Stress (volts per mm) 20-51

Insulation ALT VPM TEMP Optimum Test Plan Standardized Factor 1-0.2 0.0 0.2 0.4 0.6 0.8 1.0 1.2 Temperature (degrees C) 260 240 220 200 180 160 140 120 p UU =1.8x10-06 p=.39 p=1-0.2 0.0 0.2 0.4 0.6 0.8 1.0 1.2 Standardized Factor 2 80 100 120 140 160 180 200 Electrical Stress (volts per mm) 20-52

Insulation ALT VPM TEMP 20% Compromise Test Plan with p /ζ constraint Standardized Factor 1-0.2 0.0 0.2 0.4 0.6 0.8 1.0 1.2 Temperature (degrees C) 260 240 220 200 180 160 140 120 p UU =1.8x10-06 p=.36 p=1 p=1-0.2 0.0 0.2 0.4 0.6 0.8 1.0 1.2 Standardized Factor 2 80 100 120 140 160 180 200 Electrical Stress (volts per mm) 20-53

Comparison of Test Plan Properties for the VPM TEMP ALT No Interaction Model Interaction Model Plan V[log( t p )] F V[log( t p )] F 3 3 77.3 1.7 10 3 349 2.7 10 6 Factorial Adapted from Nelson (1990) Optimum degenerate 50.5 0.0 0.0 No ζ Optimum split 50.5 1.3 10 3 0.0 No ζ 20% Compromise degenerate 54.7 0.0 1613 0.0 No ζ 20% Compromise split 54.7 2.0 10 3 430 3.0 10 6 No ζ 20% Compromise degenerate 77.7 0.0 5768 0.0 ζ = 5.0 20% Compromise split 77.7 1.2 10 3 324 1.7 10 6 ζ = 5.0 20-54

Extensions of Results to Other Problems With one accelerating and several other regular experimental variables, replicate single-variable ALT at each combination of the regular experimental variables. Can use a fractional factorial for the regular experimental variables. If the approximate effect of a regular experimental variable is known, can tilt factorial to improve precision. With two or more accelerating variables, our results show how to tilt the traditional factorial plans to restrict extrapolation and maintain statistical efficiency. 20-55