Estimating Low Temperature PG-Grade of Binders in RAP without Extraction

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Estimating Low Temperature PG-Grade of Binders in RAP without Extraction Hussain U. Bahia, Tao Ma, Emil Bautista University of Wisconsin Peter Sebaaly, Elie Hajj University of Nevada-Reno Spring RAP ETG Meeting April 22, 2009 Manchester, NH

Outline Relevance Testing Procedure Analysis Spreadsheet Next steps

Research Needs 2007 Survey - Cecil Jones Modulus of RAP Mixes Fatigue Concerns Final Effective Binder Grade Performance of High RAP Mixes Need to Bump Binder Grade How to Better Control RAP - Fractionating

Concept of Testing Replace extraction and testing with testing RAP mortar Mortar: Voidless mix of selected gradation of RAP with binder Estimate PG of binder in RAP from mortar testing High Temp PG Intermediate Temp PG Low Temp PG Most critical Start with BBR

Challenges / Solutions BBR is not designed for testing mortars Not enough load to cause enough deflection Cannot exceed load cell limits Mold is too narrow for casting mortars Solutions Change mold Done Increase temp of testing and use models Done Re-design BBR allow higher load and measure fracture 70 % done

Mold Modification 1. Wider Sample 12.5 x 10.0 mm 2. Teflon coated 3. Stronger end holders

New Terminology RAP: Reclaimed asphalt pavement Selective RAP (SRAP): RAP passing # 8 sieve retained on single sieve or different sieves combined according to fixed gradation PAV RAP (PRAP): consists of the aggregates extracted from SRAP mixed with PAV binder Binders (B): PAV binder (PB): binder subjected to aged process of RTFO+PAV SRAP binder (SB): aged binder in SRAP; Blended binder (BB): SRAP binder blended with fresh or PAV binder Mortar (M): RAP material mixed with binder PAV mortar (PM): RAP aggregates mixed with PAV binder by weight percentage; SRAP mortar (SM): SRAP mixed with PAV binder by weight percentage;

First Approach: Test Mortars, Correlate to Binder

First Approach: Use Blending Chart to Estimate RAP Binder Grade RAP Binder S(60) New Binder S(60)

Many Problems Correlations vary Highly temperature dependent RAP mortars have very high stiffness hard to control molding Blending charts do not work for all loading times

New Approach Selective RAP to control molding # 30, #50, #100 Use PAV aged binder for blending Can test at same temp as mortar Use more PAV binder to make molding easier New analysis procedure focus on S(60), m(60). It appears to be working based on verification

Select RAP Gradation

Blending Procedures Blending procedure: Binder and was heated at 150 while aggregate and RAP were heated at 180 for 1h before mixing together to get mortar. Different mortar samples were heated for different times ( 1, 2 & 3 hrs) and then left to cool down to the ambient temperature. During the heating process, mortar was stirred every half an hour and Argon gas was used to prevent further aging of binder. All the mortar samples were heated at 150 for 1h and then stirred and poured into beam molds.

Effect of Blending Time (S-ratio) 3 hours 2 hours 1 hours T3: With fines

Effect of Blending Time (m-ratio)

Steps 1,2,3, 4 Test new binder after PAV at 3 temps Two around grade, plus one more temp E.g. for PG xx-22, test at -6 and -12, Plus 0.0C > At 0.0 C, reduce load in BBR if @ -6 C S(60) <60MPa Burn SRAP, estimate %AC, get RAP agg. Mix SRAP with PAV Binder, total 25% AC PRAP, test 2 specimens at 0.0 C Mix SRAP aggregates with 25% PAV aged AC SRAP, test 2 specimens at 0.0 C

1. Estimate Equivalent Limiting Stiffness at Test Temp used for Mortars 1,000 PAV Binder (RTFO + PAV) S60 (MPa 100 10 0 2 4 6 8 10 12 14 0.50 Temperature (C) 0.45 S60 (MPa) Equivalent Limited Stiffness 0.40 0.35 Mortars Test Temp. = 0.0 C (m value) 60 0.30 0.25 PAV Binder (RTFO + PAV) 0 2 4 6 8 10 12 14 Temperature (C) m value Equivalent m value Limit

2. Convert binder to mortar limits ( all at 0.0 C) Stiffness (MP 10,000 1,000 100 10 Stiffness at Testing Temperature 1 10 100 1000 Time (sec.) 0.9 PAV Binder Limit Stiffness 0.7 0.5 0.3 0.1 m value m value at Testing Temperature 1 10 100 1000 Time (sec.) PAV Binder Mortar Binder Limit m value

Allowable RAP Binder Temp ( C) 0.00 Time (sec.) 60.0 S (MPa) 497.5 825.5 S (MPa) 497.5 % SRAP 0.0 23.64 Allowable %SRAP - Stiffness 47.52 47.52 Allowable %SRAP - m-value 27.72 27.72 0.1 27.72 Step 4 - SRAP Binder Limit Percentage Use the PAV Mortar limit stiffness and m-value at test temp from step 3 to determine the limit % of SRAP binder. Mortars PAV mortar (Pmortar) m-value 0.383 m-value 0.383 0.310 100 1376.9 0.297 % SRAP 0.0 Limit S 1376.9 1376.9 Blended Mortar (Bmortar) S (MPa) 825.5 Limit m 0.297 0.297 m-value 0.310 % SRAP 0 100 % SRAP 23.64 LIMIT PERCENT OF SRAP BINDER log(s) = A log(%srapbinder)+b A 9.303E-03 m-value = a (%SRAPBinder)+b a -3.09E-03 Stiffness 2.6968 m-value 0.3825 Target binder low temp PG grade: B -16 C %SRAP 27.72 Allowable %SRAPBinder b %SRAP 47.52

Allowable RAP Binnder Temp ( C) 0.00 Smortarat 60 sec. (MP Time (sec.) 1,000497.5 100 60.0 S (MPa) 825.5 S (MPa) 497.5 % SRAP 0.0 23.64 Allowable %SRAP - Stiffness 16.22 16.22 Mortars PAV mortar (Pmortar) m-value 0.383 m-value 0.383 0.310 100 704.3 % SRAP Limit S 704.3 704.3 Limit m 0.387 0.387 % SRAP 10 10 Allowable 30 %SRAP - m-value 50 70 90 Percentage of SRAP Binder (%) -1.60 0.1 Mortar Stiffness Limit Stiffness -1.60 0.387 0.0 S (MPa) 825.5 Step 4 SRAP Binder Limit Percentage Blended Mortar (Bmortar) m-value 0.310 0 100 1.0 0.1 % SRAP (m value) mortarat 60 sec 23.64 LIMIT PERCENT OF SRAP BINDER log(s) = A log(%srapbinder)+b A 9.303E-03 m-value = a (%SRAPBinder)+b a -3.09E-03 Stiffness 2.6968 m-value 0.3825 Target binder low temp PG grade: B -22 C Allowable %SRAP Binder b -1.60 %SRAP 16.22 %SRAP -1.60

Allowable RAP in New Mix Step 5 - Target Binder Grade v.s SRAP Binder Limit Percentage Fresh Asphalt Binder: PG64-22 Calculation of percent RAP allowed in new HMA Target binder low SRAP binder % Limit Percent binder in new mix 5.0 temp PG grade ( C) Stiffness m-value Minimum* Percent binder in RAP 5.91-10.0 68.9 57.0 57.0 48.3-16.0 47.5 27.7 27.7 23.5-22.0 16.2-1.6-1.6-1.4 SRAP Binder % Limit 80 70 60 50 40 30 20 10 0 10 S value limit M value limit 22 16 10 4 2 Target Binder Low PG Grade ( ) 1. Enter % AC in new mix 2. Select Target PG Grade 3. Determine max allowable RAP

Validation with artificial RAP Time (s) 2PAV Fresh Blended with 51.2% of fresh Calculated Calculated Tested Differ (%) Blended with 74.9% of fresh Tested Differ (%) 8 55.6 10.9 24.2 23.6-2.2 16.4 16.1-1.9 15 44.0 6.9 17.1 17.2 0.4 11.0 11.2 1.2 30 33.3 4.2 11.5 11.8 2.5 7.0 7.2 2.4 60 25.1 2.4 7.6 7.9 3.7 4.4 4.6 4.5 120 18.6 1.4 4.9 5.2 5.3 2.6 2.8 4.4 240 13.6 0.8 3.1 3.4 7.0 1.6 1.6 4.2

Unknowns more work Effect of aging of binder RAP is not considered in this procedure Will attempt aging mortars in PAV Temperature dependency is assumed to be same for blended and new binder Can test mortar at 2 temps to verify Effect of RAP size blend Work is underway to try several sizes

Effect on other PG properties High temp grade Work started on # 100 - #200 RAP in DSR Using parallel plate ( 25-mm) Intermediate temp DSR with new geometry will be tried BBR at longer times Fracture at low temp Device is underdevelopment (New BBR).

Summary An initial procedure has been developed Results appear reasonable A few issues to be checked PAV aging of mortars Temp dependency Future work High and Intermediate Temp testing Fracture

The blending concept New binder is a PG 70-16 (TG PG70-20) X X

Effect of blending time compared to PAV aging

Example of the problem RAP Binder S(60)