MV-Series High-Pressure Valves USER GUIDE

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MV-Series High-Pressure Valves USER GUIDE 369 Syringa Ridge Sandpoint, ID 83864 281.782.8312 www.vindum.com support@vindum.com V:1.0 (6-27-17)

This page is intentionally blank. Copyright 2017 Vindum Engineering, Inc. All rights reserved. Reproduction or use of contents in any manner is prohibited without express permission from Vindum Engineering. While every precaution has been taken in the preparation of this manual, the publisher assumes no responsibility for errors or omissions. Neither is any liability assumed for damages resulting from use of the information contained herein. 2

Table of Contents Chapter 1 General Overview... 5 1.1 Configuration... 5 1.2 Main O-Ring Seal Material... 5 1.3 Pressure Rating... 5 1.4 Valve Temperature Rating... 5 1.5 Wetted Parts... 5 Chapter 2 Valve Configurations... 7 Chapter 3 Manifold Options... 9 Chapter 4 Modular Breadboard Plate... 11 4.1 Plate Sizing... 11 4.2 Tube Sizing... 11 Chapter 5 Manual Valve Maintenance... 13 5.1 Manual Valve Parts... 13 5.2 Necessary Tools... 13 5.3 Disassembly... 14 5.4 Inspect the part for damages... 14 5.5 Reassembly... 14 Chapter 6 Troubleshooting... 15 6.1 Fluid Supply Problems... 15 6.1.1 Fluid leaks from the valve bleed port... 15 6.1.2 Fluid leaks across a closed valve... 15 6.1.3 Fluid leaks from high pressure fittings... 16 Appendix 1: MV Valve Parts... 17 Appendix 2: Commercially Available Parts... 19 Appendix 3: O-ring Compatibility Chart... 21 Appendix 4: Quote Request/Order Form... 23 Index... 25 3

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Chapter 1 1. General Overview The Vindum Modular Valve System (MVS) is designed to allow fast, easy construction of high pressure fluid flow systems. The MV system is available in a wide variety of configurations for valves, manifolds, and breadboard style mounting grids. Our manual valves are needle-style valves, and can withstand pressures up to 12,000 psi, and temperatures of up to 350 o (higher temperatures options available), with proper O-ring selection. 1.1 Configurations Each MV can be manufactured with both Autoclave Speedbite ports, or High-Pressure (HiP) AF2 ports. Valves can be manufactured in 2 and 3 way configurations. The manifolds can be manufactured in 2, 3, 4, 5, and 9 way configurations. Both valves and manifolds are available in full stainless steel and Hastelloy core configurations. Hastelloy core parts are resistant to corrosion from many fluids, such as brines. 1.2 Main O-Ring Seal Material The following materials are available for the wetted O-ring. The wetted O-ring material needs to agree with the fluid used. Viton (Standard unless specified) Aflas Buna Teflon UHMW 1.3 Pressure Rating The MV system is rated for pressures up to 12,000 psi. 1.4 Temperature Rating The MV system can withstand temperatures up to 350 o F with proper O-ring selection. Higher temperature options are available on request. 1.5 Wetted Parts There are two options of materials for the valves wetted parts, or the parts of the valve that will come in contact with the fluid: 316 Stainless Steel for inert materials, or Hastelloy C-276 for corrosive materials or brine 5

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Chapter 2 2. Valve Configurations 2.1 Single Handled Valves Valves are available with one inlet and one outlet, two inlets and one outlet, and with one inlet and two outlets. The lower ports should be used for inputs, as using the upper ports for inputs places constant pressure on the O-rings, and will reduce O-ring life. The following table details the various configurations allowed. Inlets Outlets Flow direction 1 2 1 3 Inlets Outlets Flow direction 1 4 1 3,4 1 2,3 2,3 1 1 2,4 2,4 1 1 3,4 3,4 1 Figure 2.1: Valve options and flow directions 7

Chapter 3 3. Manifold Options The following table shows the available configurations of our manifolds. Manifolds are available with both Autoclave Speedbite ports (standard) and HiP AF2 ports (specify). Number of Ports Number of Ports 2, Union 4, Cross 2, Elbow 5 3, Tee 9 SS stands for full stainless steel construction. HC stands for stainless steel body with a Hastelloy Core. Figure 3.1: Manifold options 8

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Chapter 4 4. Modular Breadboard Plate 4.1 Plate Sizing Breadboard plates are available at almost any size, by request. 1 or 25mm hole spacing patterns are available. 1 spaced boards require 8-32 screws. 4.2 Tube Sizing If you are using Autoclave Speedbite ports (standard) with Vindum Manual Valves, you have the option of using 1/8 or 1/16 tubing. HiP AF2 ports require 1/8 diameter tubing. In order to properly size tubing on Vindum breadboards, we use 90 o angles when creating bends in the tubing. This allows the tubing length to be calculated with a simple equation. L=X+Y*(n+0.5) Variable Variable name L X n Y Length of tubing in one direction Depth of fitting Number of spaces Spacing size (either 1 or 25 mm. X values HiP AF2 Speedbite.3 (7.62 mm).28 (6.35 mm) Figure 4.1: Tubing Length Chart The length of one direction of the tube is measured from the end of the tube to the center of the perpendicular portion along the direction of the tube. While it is possible to calculate the exact length of the tube required by using the formula in the table, and adding length for the radius of the turn, it is often easier to bend the tube into the appropriate shape with excess tubing, then cut the tubing to length. If you use this approach, make sure you account for the radius of the tubing, as failure to do so will result in tubing that is the incorrect length. Slight bends might be required to adapt to the difference in heights between outputs and inputs. 4.2.1 Tube Routing for 5-way and 9-way Manifolds When using a 5-way or 9-way manifold, it is necessary to route tubing to the top port of the manifold. The easiest way to do this is create three 90 o bends in the tubing. Care should be taken when planning the tube routing to ensure that there is no interference with the other tubes coming from the manifold. See figures 4.2 and 4.3 for details on how high the tube routing needs to be. When creating customized bend lengths, it is recommended that you leave at least 5/8 (16mm) before the bend for Autoclave fittings and 7/ 8 (23mm) 10

for HiP fittings. To fit the tube properly, the tube should enter into the surface of the manifold by X+.2 (5.08 mm). For values of X, see Figure 4.1. It is also necessary to have special routing for the top row of the 9 way manifold fittings. See figure 4.2 for information on 9-way manifold dimensions. Figure 4.2: 9-way manifold dimensions. Figure 4.3: 5-way manifold dimensions 11

Chapter 5 5. Manual Valve Maintenance 5.1 Manual Valve Parts Figure 5.1: Manual Valve Exploded view ITEM NO. PART NUMBER DESCRIPTION QTY. 1 21100 VALVE BODY, SS & HC 1 2 21070 NUT, PACKING 1 3 410302 Teflon Backup Ring 2 4 410301 PEEK Backup Ring 2 5 ASA568A-119 O-RING, 1.130 O.D. X.924 I.D. X.103 W, Viton Fluoroelastomer* 6 21060 HANDLE 1 7 21050 KEEPER, SEAL PACK 1 8 94105A826 10-32 Set Screw, 3/8" long 1 9 92196A265 18-8 Screw 1 10 21120 Valve Stem Assembly 1 *Other materials available on request. Figure 5.2: Manual Valve Parts list 1 12

5.2 Necessary Tools 9/64 Allen wrench 5/32 Allen wrench 1/8 in Allen wrench 1/2 in wrench Non metal tapered rod, such as a small wooden skewer, plastic dental pick or nylon rod approximately 1/8 in diameter. (No Metal) 5.3 Disassembly 1. Close the valve all the way. 2. Shut off pressure to fluid and disconnect valve from plumbing. 3. Use 5/32 Allen wrench to remove the screw on top of the valve. 4. Use the 1/2 in wrench to unscrew the brass keeper. 5. Open the valve all the way. This will remove the stem gently without damaging any of the components. 6. Use 1/8 Allen wrench to loosen the set screw in the handle. Remove the handle. 7. Remove the packing nut. 8. Unscrew the stem assembly from the bottom side of the brass keeper. 9. Using the non-metal tapered rod, remove the backup rings in the valve body. The backup rings are removed in the following order: Teflon, PEEK, O-ring, PEEK, Teflon. 5.4 Inspect the part for damages Wipe the part clean with a paper towel or a clean cloth. Look at the valve stem for scratches or divots. If there are scratches or divots on the valve stem, you may need to polish the stem or purchase a new one. Inspect the inside of the base for buildup or damage. If there is build-up, remove it with solvent and a rag, but do not use anything that might scratch the seat where the stem contacts the valve body, or near the O- rings. At high pressures, even small scratches can cause leaks. 5.5 Reassembly 1. Replace the backup rings and the O-ring. The order to replace them in is Teflon (tan), PEEK (white), O- Ring, PEEK, Teflon. 2. Place the packing nut in the base with the smaller section toward the backup rings. 3. Screw the stem assembly into the brass keeper all the way. This ensures you do not damage the stem in the next step. 4. Screw the brass keeper into the base. Snug it, but do not overtighten, with a wrench. 5. Replace the 18-8 Screw in the top of the base. 6. Replace the handle and tighten the set screw. 13

Chapter 6 6. Troubleshooting 6.1 Fluid Supply Problems If the valve leaks, any one of the following can occur: It can leak to the outside, in which case the fluid will come out the bleed port located above one of the high pressure fittings. The needle will let fluid pass by it. Fluid can leak from one of the high-pressure fittings. 6.1.1 Fluid Leaks from the Valve Bleed Port If fluid is leaking from the bleed port, fluid is bypassing the O-ring seal. To solve this problem, follow the following steps. 1. Inspect the O-Ring. Make sure it is free from damage and wear. Inspect the O-Ring for contaminants. If there is damage, wear, or contaminates, replace the O-ring. Inspect the back-up rings for damage or contaminants. If the back-up rings are damaged or contaminated, they may be damaging the O-ring. If the backup rings are damaged, replace them. If they are contaminated, you can attempt to remove the contaminate with a cloth and solvent, but if this is unsuccessful, you will have to replace the back-up rings. If the O-ring is damaged, check which direction the pressure is coming from. We recommend using the lower valve port(s) for the high pressure inlet. Using the upper ports will put constant pressure on the O-ring and reduce O-ring life. 2. Inspect the surface of the needle where it contacts the O-ring and back-up rings for scratches. If a scratch is present, fluid will leak through that scratch. The needle will need to be polished with 2000 grit polishing paper, or the stem assembly will need to be replaced. 3. Inspect the valve base where the O-ring and backup rings contact the base for scratches. If the valve base is scratched, the valve base will need to be replaced. You can attempt to polish it with 2000 grit polishing paper, but due to the tight geometry of the valve base, you will most likely be unsuccessful. 6.1.2 Fluid Leaks across a closed valve If fluid is flowing through the valve when it should be closed, it indicates the fluid is bypassing the valve needle. Check the valve stem, needle, and base for contaminates that may be jamming the valve open. If contaminates are present, remove them with solvent, rags, or soft, non-metal tools to avoid scratching any of the valve surfaces. Remove the stem assembly and check the valve needle for scratches or indentations. If the needle is scratched or indented, you will need to polish the surface of the valve needle with 2000 grit polishing paper. This is easiest if done on a lathe. If the scratches or indentations cannot be removed, you will need 14

to replace the valve stem. Check the sloped portion of the valve base below the valve stem. If the surface is scratched or indented, you will need to replace the valve base. You can attempt to polish the scratches out with 200 grit polishing paper, but you are unlikely to succeed due to the tight geometries of the valve base. 6.1.3 Fluid leaks from the high pressure fittings If fluid is leaking from one of the high pressure fittings, it indicates the fitting might not be installed correctly. Ensure the fitting is tightened onto the valve properly. For liquids, finger-tight is tight enough. For gasses, tighten about 3/8 of a turn with a wrench. If a sufficiently tight fitting is still leaking, the fitting may be damaged. Inspect the fitting sleeve for damage or contamination. Clean any contamination and check for leaks. If the sleeve is damaged, you will have to replace it. This requires replacing the tube as well. However, you should be able to salvage the fitting glands. Check the fitting gland for damage. If the threads are not gripping properly, you will have to replace the gland. Replacing the gland requires you to replace both the sleeve and the tube as well, because in most cases you can t remove the gland without destroying the tube the sleeve is on. Check the port for damage or contamination. Clean any contamination with a soft cloth, solvent, and soft, non-metal tools. If the port is damaged, you will have to replace the valve body or manifold. Figure 6.1: Autoclave Speedbite pressure fitting 15

APPENDIX 1 MV valve parts Description BOM Number* Quantity Part Number Notes Valve Body* 1 1 21100 Available in Stainless Steel or Hatelloy Core Packing Nut 2 1 21070 Teflon Backup Ring 3 2 410302 PEEK Backup Ring 4 2 410301 O-Ring 5 1 2-008 Wetted O-ring, available in several materials Handle 6 1 21060 Seal Pack Keeper 7 1 21050 10-32 X 3/8 Set 8 1 94105A826 Screw 18-8 X 1/4 Socket 9 1 92196A265 Head Cap Screw Valve Stem Assembly 10 1 21120 * BOM number refers to the labels on Figure 4: manual valve parts, page 8 16

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APPENDIX 2 Commercially Available Parts FLUID FITTINGS Description Manufacturer Part Number Notes Fitting Sleeve* 1/16 XX is material type: in tubing Autoclave SSL10 XX SS for Stainless 316 Fitting Sleeve* 1/8 in tubing Autoclave SSL20 XX Fitting Nut 1/16 in tubing gland Autoclave SMN10 Fitting Nut 1/8 in tubing gland Autoclave SMN20 HC for Hastelloy C-276 XX is material type: SS for Stainless 316 HC for Hastelloy C-276 Only available in SS, as it is not a wetted part Only available in SS, as it is not a wetted part Fitting Nut 1/8 in tubing gland Fitting Sleeve* 1/8 in tubing HiP 15-2AM2 Only available in SS, as it is not a wetted part HiP 15-2A2 XX XX is material type: SS for Stainless 316 1/16 inch Tubing Vindum or Any Supplier 1/8 inch Tubing Vindum or Any Supplier SS-316.062 OD x.010 wall Hastelloy C-276.125 OD x.035 wall SS-316 Hastelloy C-276 The wetted material for the valves is listed on the warranty card. Description Manufacturer Part Number Notes 10-32 X 3/8 Set Mcmaster Carr 94105A826 Screw Any Supplier 18-8 X 1/4 Socket Mcmaster Carr 92196A265 Head Cap Screw Any Supplier 8-32 X 3/8 Socket Head Cap Screw Mcmaster Carr Any Supplier 91251A192 For use with modular breadboard Fasteners 18

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APPENDIX 3 O-ring Compatibility Chart (taken from Parker O-Ring Handbook ) P = Poor F = Fair G = Good E = Excellent Butyl Abrasion Resistance Acid Resistance Chemical Resistance Cold Resistance Dynamic Properties Electrical Properties Flame Resistance Heat Resistance Impermeability Oil Resistance Ozone Resistance Set Resistance Tear Resistance Tensile Strength Water / Steam Resist Weather Resistance (-75-250F) FG G E G F G P G E P GE FG G G G GE Chlorinated Polyethylene Chloro-sulfonated Polyethylene G F FG FP G G GE G FG E F FG G F E G G E FG F F G G G F E F G F F E Ethylene Propylene GE G E GE GE G P E G P E GE GE GE E E Flourocarbon (Viton) (-515-400F) G E E FP GE F E E G E E GE F GE FG E Flourosilicone (-100 350F) P FG E GE P E G E P G E GE P F F E Neoprene (-45 250F) G FG FG FG F F G G G FG GE F FG G F E Nitrile or Buna N (-30 250F) G F FG G GE F P G G E P GE FG GE FG F Polyacrylate (-5 to 350F) G P P P F F P E E E E F FG F P E Polyurethane (-40 180F) E P F G E FG P F G G E F GE E P E SBR or Buna S (-70 400F) G F FG G G G P FG F P P G FG GE FG F Silicone (-70 400F) P FG GE E P E F E P PG E GE P P F E Teflon Encapsulated G E E G G G G G (-70 400F) 20

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APPENDIX 4 Quote Request/Order Form For MV Series High Pressure Valves Required Valve Type and Configuration Information. MV Valve MV Manifold Select Wetted Material 316 Stainless Steel Hastelloy C-276 Port configuration Autoclave Speedbite HiP AF2 Inputs (NA for manifolds) Outputs (NA for manifolds) Shape (Tee, union, elbow, or cross) Expected Fluid Types Water, brine, oil, solvents, etc. Expected Operating Temperature Less than 32ºF (0ºC) If less than 32ºF, how low? Between 60ºF and 320ºF (16º to 160º C)? Greater than 320ºF (160ºC) If greater than 320ºF, how high? 22

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INDEX A Autoclave 5,9,11,16,19 B Breadboard 5,11 Sizing 11 F Fittings 11,15,19 H Hip AF2 Port 5,9,11,19 L Leak 14-16 M Maintenance 13 Manifold 5,9,16 N Needle 5,15 O Order form 23 O-ring 5,7,13,13,15,17,21 P Ports 5-11,15,16 Pressure rating 5 Q S Seal Material 5, 21 Speedbite 5,9,11,16 Stem 13-17 T Temperature rating 5 Tools 14-16 Tube Sizing 11 Diameter 11 Length 11 V Valve Options 7 Flow Diagrams 7 Disassembly 14 Reassembly 14 Maintenance 13-16 Parts 13 W Wetted Parts 5,19 Quote 23 R Request form 23 24