Maintenance and general care of secondary standard and field instruments This is without doubt the most important lecture that you will be given during this course. That rather rash statement is based on the fact that you may be the best physicist in the world but if the equipment you are using does not work correctly then any measurements that you make will be worthless. In these sessions we will cover the following areas: Session A General care of equipment This will cover issues concerning how instruments should be stored and maintained, cleaning of instruments and general physical (external) checks. The session will introduce the different instrument types that will be used in the practical sessions, covering any specific points associated with individual items, giving an opportunity for students to familiarise themselves with the operation of any items new to them. Checking equipment is operating properly for in-beam measurements Here we will cover checks for both radiation and non-radiation induced leaks, checks for contamination and degradation of component parts such as radiographing of chambers to reveal possible internal damage and the identification of problems through long-term observation of an instrument s performance. Session B* *This will be carried out as part of the HDR Brachytherapy practical session Setting up and carrying out a check source measurement Here you will have the opportunity to carry out examinations and check source measurements of all the instruments available. This will allow you to check that the instrument is in a fit condition for use and to demonstrate the correct set up and operation of the instrument. We will also discuss factors affecting the time required for instruments to settle (thermal, electrical etc); calibration and specification requirements of associated equipment such as barometers and thermometers; familiarisation with calibration certificates associated with the instruments to be used; discussion of levels of uncertainties and agreement between measurement readings. Session A 1 General care of equipment All the instruments used at NPL whether secondary or tertiary standards are expensive to buy and by the time they have been calibrated a lot of very precious time has been invested in them. Despite this when we visit hospitals and laboratories it is not uncommon to see an instrument stored under a desk where it gets kicked or knocked every time someone sits down, or tucked in the corner acting as a door stop. Instruments should have a designated storeroom Maintenance & general care of secondary standard & field instruments Page 1 of 10
or cupboard, preferably lockable, where they can be kept (try not to use the cupboard that has the central heating pipes running through it)! When you have found a cosy and safe place for your instrument remember to look after it. As time goes by, much like us, bits age and drop off! So to keep your equipment healthy, here is a simple checklist to follow. This is not intended as a definitive list and will depend on the instrument type. 1.1 Instrument Check List 1.1.1 Chamber Visual Inspection: a) Make sure that the chamber is properly stored. b) Regularly carry out a physical check of the chamber construction (e.g. check that the cap, outer casings and retaining nuts are not loose, that the pins in the outer stem of a 2561 have not fallen out etc). c) Check for signs of any contamination (e.g. talcum powder, hand cream). d) Keep cables / connectors / dust caps clean and free from damage and replace any missing components. e) Look after the chamber case. Keep it clean and secure (some cases become self-opening!). f) Get to know your chamber. Is there anything that doesn t look right? Operational: g) Always give the chamber a pre-irradiation dose before each use. h) Check for signs of any leaks (natural, radiation induced). i) Carry out regular check source measurements. j) Keep a history of the chamber response to allow you to check its long term stability. k) Carry out regular radiographs of your chamber. These can reveal problems even in brand new chambers. 1.1.2 Electrometer Visual Inspection: a) Make sure that the electrometer is properly stored. b) Check the desiccator regularly and dry it out if suspect. c) Keep cables / connectors / dust caps clean and free from damage and replace any missing components. d) For battery operated instruments, check that the batteries are in good condition and do not need replacing (before leaking occurs inside the instrument!) e) Ensure that the cases and their lids and handles are secure (and there is nothing rattling around inside the case). Operational: f) Check that the charge and/or current calibration are correct. g) Always carry out a self-check on the instrument if available (e.g. Dosemaster). h) Always ensure that the HT supply to the chamber is the correct value. i) Check regularly for any leakages and drifts. Maintenance & general care of secondary standard & field instruments Page 2 of 10
1.1.3 Check source a) Make sure that the source is properly stored. b) Regularly carry out a physical examination of the source (e.g. has it been dropped). c) Check that all parts are present (such as tamper-proof disc on base of source / source feet / source plugs etc) and replace any missing components. d) Keep the storage and transport case in good condition and make sure it conforms to current transport regulations. e) Regularly carry out radioactive leak tests. All the instruments covered on this course have the same basic function of measuring the ionisation produced in the ion chamber volume resulting from the incident radiation beam. This can be determined by measuring the collected charge as with the PTW Unidos or Wellhofer Dose 1 electrometers, or by measuring the current as with the NE 2670. However there may be subtle variations between types, even between instruments of the same type, and user interfaces between manufacturers can be very different. It is therefore advisable to familiarise yourself with the fundamental mode of operation of your own specific equipment. 1.2 Instrument types Instruments that will be used on the course will include some of the following: 1.2.1 Ionisation chamber types 2561/2611 type NE 2571 NE 2502 Wellhofer Farmer type both standard and waterproof Very low energy thin window chambers; NACP, Roos and Markus parallel plate electron chambers 1.2.2 Electrometer types NE 2560 NE 2570 NE 2670 NE Dosemaster PTW Unidos Standard Imaging Supermax Wellhofer Dose 1 1.2.3 Radioactive Check Source types NE 2562 NE 2606 NE 2503 PTW 8921 Maintenance & general care of secondary standard & field instruments Page 3 of 10
2 Checking equipment is operating properly for in-beam measurements 2.1 Natural Leak A natural leak can occur in the instrument in the absence of a radiation field. To test for a natural leak after the instrument has been set up, unearth the electrometer and watch the reading for a period of time similar to that for which a normal reading would be taken. Record the reading at the start and watch what happens to it during the measurement, an earthing kick may sometimes occur immediately after pressing the start button. Record the final reading and repeat a few times to ensure consistency. If the drift is not considered negligible then the actual readings should be corrected. Large leaks or drifts may typically arise from: dirty connectors wet desiccators not giving instruments long enough to settle not giving a pre-irradiation dose to the chamber 2.2 Radiation induced leak A radiation-induced leak is associated solely with the chamber and is identifiable only after the chamber has been exposed to a radiation field. If a radiation induced leak is present, there is usually a continued collection of charge even after the beam has been switched off, at a similar rate to that of the reading, which quickly levels off. Radiation induced leaks vary in their magnitude but provided they are small may be ignored. However, a chamber that exhibits a large leak will usually require repair by the manufacturer. 2.3 Contaminated and corroded chambers The importance of recording the historical performance of a chamber is born out by the effects that may occur through contamination or corrosion and degradation. At the lower energy range this may be particularly noticeable. Each time a chamber is calibrated here at NPL we compare its performance against its response in previous calibrations. NB: please let us know if a chamber has been repaired since its last calibration, it saves our time and your money! A small shift in the calibration curve up or down is not unexpected, however a large shift or rotation of successive calibration curves may indicate a problem. The graph in Figure 1 shows a customers secondary standard NE 2561 chamber that had been calibrated successfully with good agreement on two occasions (Autumn 1976, 1979). On its third visit to NPL a significant change in its response at lower energies was observed with a difference of 1.7% at the 2mm Al HVL, with no significant difference at higher energies (Before repair, 1982). On removal of the graphite cap, traces of a white deposit were found near to the vent hole and inside the cavity. When cleaned and the cap replaced it can be seen that the response of the chamber returned close to that previously observed (After repair, 1982). The contaminant was suspected to be talcum powder, probably from a waterproof latex sheath of a type that is now seldom used. Maintenance & general care of secondary standard & field instruments Page 4 of 10
Again in Figure 2 we see an NE 2561 chamber that has shown good agreement between its first two calibrations with a difference of the order of 20% on its third visit. Interestingly the Strontium 90 check source measurements revealed no problem, showing good agreement between all three visits. Q. Why was no difference observed in the Strontium 90 check source measurements for this chamber? A radiograph of the chamber, and its subsequent dismantling, revealed that the hollow aluminium central collecting electrode, which has a wall thickness of 0.2mm had suffered severe corrosion resulting in a hole. Once the electrode was replaced, the chamber was recalibrated exhibiting a similar response to previously. After discussion with the owner it was concluded that the corrosion was due to the very high humidity in the store where the chamber was kept. 1.150 Relative calibration factor (exposure) 1.100 1.050 1.000 Autumn 1976 Autumn 1979 Before repair, 1982 After repair, 1982 0.950 0.1 1 10 HVL (mm Al) Figure 1 shows the effect of contamination, most likely talcum powder, on a Secondary Standard NE 2561 chamber. Maintenance & general care of secondary standard & field instruments Page 5 of 10
1.30 Relative calibration factor (exposure) 1.25 1.20 1.15 1.10 1.05 1.00 October 1982 October 1985 Before repair, 1989 After repair, 1989 0.95 0.1 1 10 HVL (mm) Figure 2 shows the effect of electrode corrosion due to poor storage conditions, on a Secondary Standard NE 2561 Chamber. 2.4 Radiographs Radiographing a chamber is an extremely useful way to investigate possible problems without having to resort to dismantling the chamber, which would inevitably result in the invalidation of the calibration. Here are a number of radiographs that have been taken of chambers that have exhibited strange behaviour. When commissioning a new chamber it is recommended that radiographs be taken to check that the design is consistent with the manufacturer s drawings and specification. Q. Figures 3 and 4 both show brand new chambers that exhibited poorer than expected performance. Can you see why? The chambers in Figures 5-7 are all NE 2561 secondary standard chambers, one is a routine radiograph and the chamber had no problems. The other two Maintenance & general care of secondary standard & field instruments Page 6 of 10
both gave inconsistent readings in check source measurements and in high and low energy beams. Q: The good chamber is shown in Figure 5, can you identify the problems with the other two chambers? Maintenance & general care of secondary standard & field instruments Page 7 of 10
Figure 3 shows a Farmer type chamber with two obvious problems. Figure 4 shows side-on radiographs of two NACP type chambers from different manufacturers. The lower one is correct the upper chamber is not and has a fault that would seriously affect its performance. Maintenance & general care of secondary standard & field instruments Page 8 of 10
Figure 5 shows an NE 2561 chamber that is operating correctly. Figure 6 shows an NE 2561 chamber with? Maintenance & general care of secondary standard & field instruments Page 9 of 10
Figure 7 shows an NE 2561 chamber with? Maintenance & general care of secondary standard & field instruments Page 10 of 10