On-Stream Tightness Testing of Vacuum Process Installations

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ECNDT 2006 - Tu.2.6.3 On-Stream Tightness Testing of Vacuum Process Installations André de JONGE, Leak Detection Group, DCI Meettechniek B.V., Kapelle, The Netherlands DCI Meettechniek. -DCI was founded in 1988. -DCI is an independent company specialized in technical services aimed at the processing industry. These services are usually carried out on-site at the client's location. -DCI performs: -(on-stream) leak tightness testing (>25 years) -heat exchanger tube inspections (>15 years) -valve testing (>15 years) -has approximately 35 employees -the shares are (indirectly) owned by RTD and Stork Primary markets Our office is located in the south west of the Netherlands. Our clients are located all over Europe, but often also far beyond this. 1

Power Plants and (Petro)chemical Industry Many sorts of leak tests are carried out in the process industry. Especially for vacuum systems, a number of testing methods are developed on one's own. Using these techniques, it is possible to find air inleakages with the plant in operation. Turbine vacuum system Vacuum destillation columns On-stream leak testing - Air ingress In power plants used, to find air inleakages in turbine- and condenser vacuum systems In (petro)chemical industry to find leakages in evaporators and vacuum columns - Cooling water leakages In power plants used to find water leakages in condensers - Helium Extraction Method Developed for testing heat exchangers in operation 2

Power plants Leak test of turbine vacuum system Air ingress problem analysis Atmospheric air entering the vacuum causes an increase of non-condensing gases in the condenser. This can cause: -a system pressure increase -pump capacity too small -increase of system pressure -an increase of Oxygen level in condensate -a pressure-rise test, which is out of specification -performed at specified generator power -volume of vacuum system Also often a preventive leak test is carried out. -global check before a revision -after a shut down to check the repairs 3

Locating air leakages -Smoke test (chemical smoke source) -problems because of the presence of air currents (drafts, ventilation) -low test sensitivity -Ultrasonic detection -problems because of surrounding (background) noise -low test sensitivity -Halogen test -not allowed any more because of environmental properties -Helium test Helium test Why to use Helium? -Helium is an inert gas mass 4, only 5 ppm present in the atmosphere) -Not harmful, explosive or corrosive -Absolute selective measurement for qualifying and quantifying leaks -Helium does not condensate in the condenser atmosphere -Best performance at maximum power Vacuum schedule, power plant 4

Air ingress localization When carrying out a leak test on a turbine- condenser vacuum system, the partial pressure of helium in the system, is measured during the complete test. At the same time all potential leak locations like rupture disks, shaft seals, flanges etc. are sprayed from the atmospheric side with helium. Should a leak be sprayed over, an air-helium mixture will enter the vacuum system and cause an increase of the partial pressure of helium. The reaction time, i.e. the time between bringing the helium in contact with the leak and the detection of rise of its partial pressure, is to be determined by experiment. Normally this time is approximately 30 seconds. The detection sensitivity, which differs per installation and per operational situation, can be down to 5 mbar.l/s. 5

Air ingress localization Testing of components in insulation All necessary test equipment, mounted in a Van. Air ingress testing -Vacuum pressure depends on: -vapour pressure of the condensate at the prevailing temperature -condition condenser -pressure of non-condensing gases -Air ingress increases the amount of non-condensing gases and so the vacuum pressure rises This vacuum pressure rise will cause an increase of system temperature (reduced efficiency). 6

Air ingress testing -High presence of non-condensing gases: -worse vacuum -more pump capacity necessary -Efficiency lower; higher fuel costs -Air (Oxygen, harmful components) can cause damage of the installation -All these problems lead to extra costs or to income reduction Air ingress testing -Vacuum system of medium size power plant can be tested in 2-3 days -Efficiency increase depends on size leaks -Trend: -problem solving -preventive measurements Example (1) -Power plant in Turkey: vacuum pump output was 65 m 3 /h; after repair found leak, the pump output decreased to 35 m 3 /h; this resulted in a power increase of 2 MW; income difference of $70.000,- per month Example (2) Power plant needs both vacuum pumps at full power, to maintain the vacuum. After repair; possibility to stop one pump; -Direct cost reduction -Reserve pump capacity available if anything deteriorates 7

Found leaks Test equipment 8

Other techniques. Principle of helium leak test of heat exchanger in operation. The mass spectrometer is coupled via the extractor (a kind of semi-permeable membrane) to the secundary (low pressure) side of the heat exchanger. In the primary circuit (high pressure side) Helium is injected. A leak will be manifest, when the helium partial pressure increases in the secundary circuit of the heat exchanger. Benefits of Air Ingress Testing -Reliable method to localize and quantify leakages; also for insulated vacuum systems -Better vacuum results in product quality improvement -Efficiency higher; lower fuel costs -Air (Oxygen, harmful components) can cause damage of the installation Air ingress can lead to extra costs or to income reduction 9