Chemgard Filter Housings

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Contamination Control Solutions Chemgard Filter Housings Installation and use manual

Table of Contents Introduction... 2 Safety... 2 Specifications... 3 PVDF... 3 PP... 3 PFA In-line... 3 Installation... 4 Facility Requirements... 4 Mounting... 4 PVDF... 4 PFA In-line... 5 Filter Changeout Instructions... 6 Ordering Information... 8 Entegris, Inc. Chemgard Filter Housing Manual 1

Introduction Chemgard TM filter housings are designed to meet high-purity standards for process fluids. The smooth surfaces of the Chemgard filter housings work well in environments where low particle contamination is essential, and the durable torsion-free seal and leakproof design ensure reliable operation. Read this manual for instructions on how to install and use Chemgard filter housings, along with product specifications and ordering information. Safety Special considerations and precautions are included in the manual, as described below. Contact Entegris with any questions regarding the safe and proper use of your equipment. DANGER Indicates a hazardous situation that, if not avoided, could result in death or serious injury. Warning: Indicates a potential hazardous situation that, if not avoided, could result in death or serious injury as well as irreparable damage to the equipment. Caution: Indicates a potential hazardous situation that, if not avoided, could result in minor to moderate injury as well as minor to moderate damage to the equipment. WARNING: Only technically qualified personnel should install the housing. WARNING: CHEMICAL HAZARDS DOUBLE-CONTAINMENT is required when used with toxic and hazardous chemicals. All filter housings, filters and other pressurized vessels must be doublecontained to prevent serious personal injury. SAFETY CLOTHING, eye protection and safety apparatus appropriate for the liquids in use must be worn during component changeout and startup. Perform all operations with standard liquid handling procedures in accordance with all local codes for safety and ventilation. 2 Chemgard Filter Housing Manual entegris, Inc.

Specifications Chemgard PVDF Materials: Head and bowl Polyvinylidene fluoride Fluid connections: Cartridge connections: Locking ring O-ring See data sheet PVDF (nonwetted part) 2-345 Viton Code 0, 2-222 o-ring and Chemlock cartridges with key Operating conditions: Maximum static inlet pressure 0.3 MPa (3.0 bar, 43 psi) @ 100 C (212 F) 1.0 MPa (10 bar, 145 psi) @ 25 C (77 F) Maximum operating temperature 100 C (212 F) Chemgard PP Materials: Head and bowl Polypropylene Locking ring PVDF (nonwetted part) O-ring 2-345 Viton Fluid connections: See data sheet Cartridge connections: Code 0, 2-222 o-ring and Chemlock cartridges with key Operating conditions: Maximum static inlet pressure 0.14 MPa (1.4 bar, 20 psi) @ 90 C (194 F) 0.7 MPa (7 bar, 100 psi) @ 25 C (77 F) Maximum operating temperature 90 C (194 F) Chemgard In-line PFA Housings Materials: Head and bowl Teflon fluoropolymer PFA 440 HP or equivalent Locking ring PVDF or GFPP (nonwetted part) O-ring Encapsulated fluoropolymer (E-FKM) Fluid connections: See data sheet Cartridge connections: Code 0, 2-222 o-ring and Chemlock cartridges with key Operating conditions: Maximum static inlet pressure 0.3 MPa (3.0 bar, 43 psi) @ 100 C (212 F) 0.75 MPa (7.5 bar, 110 psi) @ 25 C (77 F) Maximum operating temperature 100 C (212 F) Entegris, Inc. Chemgard Filter Housing Manual 3

Installation Facility Requirements Housing should be plumbed with the ability to isolate both upstream and downstream flows as required for filter changeout. NOTE: To ensure proper tightness, use the Chemlock integrated torque wrench (part no. YY4600005) to tighten the housing. For E-FKM o-rings, tighten to 35 N m. For all other o-ring types, set to 18.5 N m. PVDF Mounting Bracket Template NOTE: For mounting bracket (part nos. YY4610190 or YY66BRACK). Mounting plate thickness MUST NOT exceed 0.9 cm (0.35 ). For use with Entegris straps and bolts, (part no. YY3610180). Chemgard PVDF Housing Assembly Wrench clearance 197 mm (7.75 ) Width inlet to outlet 145.3 mm (5.72") Length Chemgard PVDF Mounting Template 145.3 mm (5.72 ) 79.2 mm (3.11 ) 33.3 mm (1.31 ) 38.5 mm (1.52 ) 76.9 mm (3.03 ) Mounting Procedure Mounting template detail for reference only. Not shown to scale PVDF Housing 1. Install the mounting bracket upright or inverted. 2. Install the housing head on the mounting bracket. Use four 3 8-16 1" PVDF mounting screws. 4 Chemgard Filter Housing Manual entegris, Inc.

In-line Housings Minimum Space Requirements All systems must have enough clearance below the bowl to allow for filter changeout. It is best to measure the length of the bowl and add enough room to enable easy changeout. Practice installing the bowl in a dry system to ensure sufficient space. Chemgard In-line Housing Assembly Overall width 146 mm (5.74 ) Length In-line Mounting Bracket Template Ø40.6 mm (1.60 ) 40 mm (1.57 ) Ø55 mm (2.16 ) 40 mm (1.57 ) 30.6 mm (1.21 ) 30.6 mm (1.21 ) 30.6 mm (1.21 ) 30.6 mm (1.21 ) 4 Ø18 mm (0.70 ) Mounting template detail for reference only. Not shown to scale Entegris, Inc. Chemgard Filter Housing Manual 5

Filter Changeout Instructions WARNING: Only technically qualified personnel should install the housing. WARNING: CHEMICAL HAZARD Perform all operations with standard liquid handling procedures in accordance with all local codes for safety and ventilation. You MUST wear appropriate clothing and safety apparatus for the liquids you are using. Wear chemical-resistant garments and eye protection during component changeout and startup. 3. OPTIONAL: If you are using a hydrophobic filter, pre-wet the filter 4. Wet the filter o-ring with a wetting agent compatible with your process, then install the filter into the Chemgard head. CAUTION: Push straight up to avoid damage to the o-ring and seal. DO NOT twist. DOUBLE-CONTAINMENT is required when used with toxic and hazardous chemicals. All filter housings, filters and other pressurized vessels must be double-contained to prevent serious personal injury. 1. Isolate and drain the housing. If necessary, allow the housing to cool to a workable temperature. 2. Use the housing wrench to remove the filter bowl, then remove the filter. Push straight up 5. If necessary, remove the existing o-ring. Slide the o-ring removal edge of the housing wrench tool under the o-ring, then slide the tool around the bowl. CAUTION: Use caution when removing the o-ring. Contacting the o-ring seal areas with the removal tool can damage the sealing surface. 6. Prepare the new housing o-ring for installation in the housing bowl: Kalrez perfluoroelastomer, EPR or Viton fluoroelastomer o-rings: Pre-wet the o-ring with DI water or IPA. 6 Chemgard Filter Housing Manual entegris, Inc.

E-FKM o-ring: Heat the o-ring by immersing in hot water (50 60 C) for 2 minutes, or by placing the o-ring 25 mm (1") below a 250-watt heat lamp for 1 minute. Proceed to the next step while the o-ring is still warm. 9. Slide the housing bowl over the filter and push so that the o-ring engages the housing head. Push the locking ring against the head to engage the threads, then hand-tighten. WARNING: Use the correct o-ring type for your process. If necessary, consult Entegris Technical Service. 7. Place the o-ring over the housing bowl and gently push the o-ring down into the groove. Use your fingers to gently press the o-ring into place. CAUTION: DO NOT twist or roll the o-ring or leaking will occur. Push lock ring to engage threads Press o-ring in place 8. IMPORTANT: If you are using an Entegris 10" filter in a 12" universal housing, you must install a spacer in the housing, prior to installing the cartridge. Drop the spacer into the bottom of the housing, or place the spacer on the end of the filter. (The spacer is NOT required for Guardian TM HPX, ATX; Etchgard TM HPX; Fluorogard CF, ATX; and ProcessGard CN and CR cartridges.) Hand-tighten NOTE: If this is not possible due to ergonomic constraints, the locking ring may be used to seat the o-ring. Place the bowl against the head and tighten the locking ring to hand-tight. Use the Chemgard/Chemlock wrench to tighten the locking ring and seat the o-ring. The head and bowl are self-aligning. Unscrew the locking ring and inspect the seal area to make sure the o-ring is seated in the head. Retighten the locking ring to hand-tight. Continue with step 10 to torque the locking ring to its seal specification. Entegris, Inc. Chemgard Filter Housing Manual 7

10. To ensure proper tightness, use the Chemlock integrated torque wrench (part no. YY4600005) to tighten the housing. For E-FKM o-rings, tighten to 35 N m. For all other o-ring types, set to 18.5 N m. CAUTION: DO NOT exceed torque specifications. 11. IMPORTANT: For E-FKM o-rings: If you have heated an o-ring, allow the housing to cool for 30 minutes, then re-tighten to the proper torque. WARNING: You must allow the o-ring to cool and then re-tighten the housing to prevent leaks. Ordering Information Part Number YY4600005 YY4600006 YY4610190 YY66BRACK YY3610180 YY5500005 YY4510180 YY4510140 YY4622191 12. Leak test the housing: Close the drain. Open the downstream vent. Flow liquid though the inlet at low pressure (<1 L /min) until all the air is removed from the housing. Close the downstream vent. Increase inlet pressure to your system pressure. Flow at system pressure for five minutes as you check all seals for leaks. If the housing leaks: Check the torque setting. If the leak persists, disassemble the housing and replace the bowl o-ring. Check the locking ring torque for tightness if the housing is relieved of system pressure or if the system has been exposed to temperatures of 100 C or more. WARNING: DO NOT tighten or adjust the locking ring while the housing is pressurized or when the temperature exceeds 27 C. Description Chemlock integrated housing wrench Chemlock housing wrench head PVDF L-mounting bracket (for Chemlock and Chemgard PFA housings) L-mounting bracket (can be used for mounting both Chemlock PP and Chemgard PP housings) Mounting bolts and straps PFA plugs, 1 4 NPTM, 4/pk PFA cartridge o-ring adapter 2-222 to 2-118, 2/pk 10 PFA cartridge adapter (for 12 universal Chemgard bowl) 20 PFA cartridge adapter (for 22 universal Chemgard bowl) 20 Chemgard housings are compatible with all 20 cartridge filters and contain a cartridge adapter for use with Entegris cartridges. 12 housings contain a 10 cartridge filter adapter and are compatible with all 10 cartridges. 10 housings accommodate 10 cartridges up to 10.3. 8 Chemgard Filter Housing Manual entegris, Inc.

For More Information Please call your Regional Customer Service Center today to learn what Entegris can do for you. Visit www.entegris.com and select the Customer Service link for the center nearest you. Terms and Conditions of Sale All purchases are subject to Entegris Terms and Conditions of Sale. To view and print this information, visit www.entegris.com and select the Legal Notices link from the footer. Product Warranties For Product Warranties, visit www.entegris.com and select the Legal Notices link from the footer. Entegris, the Entegris Rings Design, Fluorogard, ProcessGard, Chemlock, Chemgard, Guardian and Etchgard are trademarks of Entegris, Inc. Kalrez and Viton are registered trademarks of DuPont Dow Elastomers, L.L.C. Teflon is a registered trademark of E.I. du Pont de Nemours and Company. ENTEGRIS, INC. Corporate Headquarters 129 Concord Road Billerica, MA 01821 USA Customer Service Tel. +1 952 556 4181 Customer Service Fax +1 952 556 8022 In North America 800 394 4083 www.entegris.com 2013 Entegris, Inc. All rights reserved Printed in USA 4411-7325ENT-0213