Sample Cylinders and Accessories

Sample Cylinders and Accessories SC and MC Series FITOK Group FITOK GmbH (Headquarter) Sprendlinger Landstr. 115, 6069 Offenbach am Main, Germany Tel.: +49 69 8900 4498 Fax: +49 69 8900 4495 FITOK, Inc. 184 North Promenade Blvd., Suite 7, Stafford, Texas 77477, USA Tel.: +1 281 888 0077 Fax: +1 281 582 51 FITOK Incorporated 1-4F, Block C, Zone E, Yingtailong lndustrial Park, Dalang Street, Longhua District, Shenzhen, 518109, China Tel.: +86 5 280 2 Fax: +86 5 280 2619 FITOK Middle East Oil Equipment Trading LLC 208-209, Makateb Tower, Airport Road, P.O.Box 185412, Deira, Dubai, UAE Tel.: +971 4 2959 85 Fax: +971 4 2959 854 info@fitokgroup.com www.fitokgroup.com FK-IC-GC-02-EN-151120 www.fitokgroup.com

1 Sample Cylinders and Accessories Sample Cylinders SC Series Application Hydrocarbon sampling in refineries Gas sampling in chromatography Condensate sampling in fossil fuel and nuclear power plants Surge accumulators or reaction vessels Snubbers in reactor feed lines Materials Sample Cylinders and Accessories 2 Standard FITOK cylinders are available in 04L and 16L stainless steel in both DOT and non-dot ratings. Monel (Alloy ) cylinders are standard as non-dot. Pressure Ratings DOT cylinders come as standard with psi g, 1800 psig or 0 psig ratings. DOT and Non-DOT cylinders can be furnished with higher pressure ratings. Pressure - Temperature Features Material 16L SS 16L SS, 04L SS 04L SS Alloy 16 SS 04L SS Capacities ranges from ml to 785 ml (1 gal) Cylinder ends come in 1/8, and 1/2 connections DOT Specification DOT-A 0 TC-ASM 44 DOT-E 1800 TC-EM 124 DOT-A 1800 TC-ASM 124 4B Cylinder heads are formed by utilizing spinning process for consistent strength, size and dimensions Special high tolerance thread All models are internally sandblasted to smooth surface imperfections and remove foreign particles Temperature, F ( C) -65 (-5) to 100 (7) 0 (44) Working pressure, psig (bar) 1800 1800 1800 (69.0) (4.4) Single and double ended cylinders in most capacities are available as standard 200 (9) 960 (272) 160 (9.7) 160 (9.7) 1580 (108) 8 (57.8) (4.4) Cylinders may be furnished with valves, relief devices, outage tubes, carrying handles, caps and plugs 00 (148) 570 (245) 120 (84.7) 120 (84.7) 1490 (102) 760 (52.) (4.4) Design (204) (260) 290 (226) 060 (210) 110 (77.8) 10 (72.) 110 (77.8) 10 (72.) 1 (98.5) 700 (48.2) 6 (44.7) (4.4) (4.4) FITOK sample cylinders are designed and manufactured to stringent department of transportation regulations of US government in 49 CFR, Paragraphs 178.6 specification A; seamless steel cylinders and 178.42 Specification E; seamless steel cylinders; and 178. 4B; welded steel cylinders, providing long performance life and maximum safety to users. The cylinders are hot spun from seamless tubing for integrity and corrosion resistance. The process provides a smooth internal flow transition through the neck to minimize pockets which can trap previous samples. DOT Certificate for Sample cylinders are being applied. 600 (15) 2920 (201) 6 (4) 2870 (197) 700 (71) 2810 (19) 7 (98) 27 (189) 800 (426) 2700 (186) (69.0) 980 (67.5) 970 (66.8) 9 (65.4) 90 (64.0) (69.0) 980 (67.5) 970 (66.8) 9 (65.4) 90 (64.0) 1410 (97.1) 620 (42.7) 610 (42.0) 590 (.6) 580 (9.9) 570 (9.2) (4.4) (4.4) (4.4) (4.4) (4.4) 8 (454) 26 (181) 560 (8.5) (4.4) 1. Working temperature limited to 00 F (148 C) maximum with PTFE internal coating. 2. Working pressure and temperature may be limited by individual local government regulations. Testing Every sample cylinder is hydrostatically tested to at least 5/ the pressure rating.

Sample Cylinders and Accessories Sample Cylinders and Accessories 4 Single-Ended Cylinders DOT-4B cylinders are hydrostatically proof tested at psig (69 bar) minimum. Technical Data Dimensions are for reference only and are subject to change. Minimum Wall Thickness Outside Diameter Material Grade/Cylinder Specification Pressure Rating psig (bar) ( ± 10%) P in. Outside Diameter Single-Ended Dimensions, in. (mm) Length Minimum wall thickness Weight Ib (kg) Length 04L SS/ DOT-4B (4.4) 00 2.00 (.8) Double-Ended 4.88 8.62 (219) 1.6 (45) 1.10 (0.) 1.80 (0.82) 2.70 (1.2) Double-Ended Cylinders DOT-A 1800/TC-ASM 124 cylinders are hydrostatically proof tested at 000 psig (206 bar). DOT-E 1800/TC-EM 124 cylinders are hydrostatically proof tested at 0 psig (210 bar). One cylinder of each lot is burst tested. DOT-A 0/TC-ASM 44 cylinders are hydrostatically proof tested at 8 psig (586 bar). Outside Diameter P - Fe Size P - Both Ends Fe Size Cleaning and Packaging Minimum Wall Thickness All FITOK sample cylinders and cylinder valves are cleaned and packaged in accordance with FITOK FC-01 standard cleaning procedures. Cleaning and packaging in accordance with FITOK FC-02 special cleaning procedures, to ensure compliance with product cleanliness requirements stated in ASTM G9 Level C are available as an option for cylinder valves. Length 04L SS/ DOT-E 1800 TC-EM 124 04L SS/ DOT-A 1800 TC-ASM 124 16L SS/ DOT-E 1800 TC-EM 124 16L SS/ DOT-A 0 TC-ASM 44 Alloy 1800 1800 1800 0 (44) 1800 290 00 22 785 (1 gal) 290 00 00 00 1/8 or 1/2 or 1/2 1.25 (1.8) 1.5 (8.1) 2.00 (.8). (88.9) 4.00 (102) 2.00 (.8) 1.90 (48.2) 2.00 (.8).88 (98.6). (95.2) 4.94 (125) 5.25 (1) 8.86 (225) 8.94 (227) 11.4 (290) 1.8 (51) 10.9 (277) 17.2 (47) 26.7 (678) 5.25 (1) 8.86 (225) 8.94 (227) 1.8 (51) 8.00 (20) 14.5 (68) 2.5 (597) 5.25 (1) 8.94 (227) 1.8 (51) 0.07 (1.8) 0.18 (4.6) 0.21 (5.2) 0.24 (6.1) 0.1 (0.14) 0.8 (0.17) 0.62 (0.28) 0.94 (0.4) 1.79 (0.81) 1.80 (0.8) 2.10 (0.95) 2.61 (1.20) 6. (2.90) 14.00 (6.) 21.00 (9.) 0.94 (0.4) 1.79 (0.81) 1.80 (0.8) 2.60 (1.20).00 (1.) 5.60 (2.) 9.10 (4.10) 0.94 (0.4) 1.80 (0.82) 2.90 (1.0) Single-Ended and Double-Ended cylinders with pressure ratings up to 0 psig are available. When testing to ASME specifications is required, contact FITOK for quotation and specify maximum pressure and temperature.

5 Sample Cylinders and Accessories Sample Cylinders and Accessories 6 Transportable Pressure Equipment Directive (TPED) Ordering Information The Transportable Pressure Equipment Directive ( TPED) provides requirements relating to the design, manufacture, and testing of transportable pressure vessels and accessories, including sample cylinders and rupture discs. The intent of the directive is to provide a uniform level of product safety throughout the European Union countries. For information about TPED-compliant products, see the FITOK Products Catalogue Sample Cylinders Compliant with the Transportable Pressure Equipment Directive (TPED). Nominal Burst Pressure at 70 F (20 C) 28 psig ± psig 196 bar ± 10. bar 1900 psig ± 100 psig 10 bar ± 6.8 bar Ordering SS-RDD-7BS-28 SS-RDD-7BS-1900 Remark: rupture disc kits should be used with FITOK rupture disc tees or FITOK needle valves with rupture disc kits. Cylinder Surface PTFE Lined Cylinders The internal cylinder surfaces are available with special PTFE lining providing excellent lubricity and very low permeability. Rupture Disc Tees These compact assemblies are designed for use with various FITOK valves. Tees are fabricated of 16 stainless steel. Each tee consists of a rupture disc kit. Electropolishing Electropolishing can provide a clean internal surface with a high degree of passivation. Sample Cylinder Accessories Overpressure Protection C D Compressed gas cylinders must be equipped with pressure relief devices in accordance with US DOT regulations and CGA Pamphlet S-1.1. The CGA Pamphlet lists devices that can be used with specific gases. It also contains information on other types of pressure relief devices. Be sure to use the correct pressure relief device for the gas being used. B A Proper filling of the cylinder according to DOT specifications, or other local regulations, is critical in preventing overpressurization. Ordering Information and Dimensions Rupture Disc Kits Rupture disc models are supplied with a pre-bulged rupture disc which provides excellent resistance to a broad range of corrosive materials, protecting sample cylinder from over-pressurization by venting the cylinder contents to atmosphere. The rupture disc is welded to a body that is threaded into a valve body or a rupture disc tee and sealed by an elastomer o-ring. The rupture disc can be easily replaced without removing the valve or the tee from the cylinder. Materials of Construction End connections Inlet in. Outlet in. Ordering With 28 psig (196 bar) Rupture Disc SS-TM4-F4-RD28 SS-TM8-F4-RD28 Dimensions, in. (mm) A B C D 2.06 (52.4) 2.6 (66.7) 1.0 (26.2) 1. (8.1) 0.5 (1.5) 0. (19) 1.16 (29.4) 1.42 (6) With 1900 psig (10 bar) Rupture Disc Component Body, inlet ring Rupture disc O-ring Material Grade/ASTM Specification 16 SS/A479 Alloy 600/B168 Fluorocarbon FKM in. in. SS-TM4-F4-RD19 SS-TM8-F4-RD19 2.06 (52.4) 2.6 (66.7) 1.0 (26.2) 1. (8.1) 0.5 (1.5) 0. (19) 1.16 (29.4) 1.42 (6)

7 Sample Cylinders and Accessories Sample Cylinders and Accessories 8 Nonrotating-Stem Needle Valve with Rupture Disc Kits To order a carrying handle as separate component, use one of the following ordering numbers. Cylinder OD in. (mm) 2. 0 (.8).5 (88.9) 1.9 (48.2) Cylinder 00~ 00 1.9 (48.2) Ordering S4-SCXX-DN4(8)-XXX-H2 Two hose clamps are included in carrying handle ordering number, SCXX and XXX in ordering number should be acquired from "part number description", namely "working pressure" and "internal volume" respectively. 4.0 (102) 22 785 S4-SCXX-DN4(8)-XXX-H4 Ordering Information and Dimensions Caps and Plugs End connections Inlet Outlet Flow Pattern Valve Ordering Orifice in. (mm) Caps and plugs protect FITOK tube fitting or end connections on valves during cylinder transport. Contact the authorized representative or FITOK for details. With 28 psig (196 bar) Rupture Disc in. in. Straight Angle NDSS-NS4-FNS4-7-SAFE2 NDSS-NS4-FNS4-7-A-SAFE2 NDSS-NS8-FNS4-8-A-SAFE2 0.16 (4.0) 0.22 (5.6) Customer-supplied ring shown Tube Fitting Plug FITOK PIPE PLUG Pipe Cap With 1900 psig (10 bar) Rupture Disc FITOK PIPE PLUG in. in. Straight Angle NDSS-NS4-FNS4-7-SAFE1 NDSS-NS4-FNS4-7-A-SAFE1 NDSS-NS8-FNS4-8-A-SAFE1 0.16 (4.0) 0.22 (5.6) FITOK PIPE PLUG Pipe Plug 1. Dimensions are for reference only and are subject to change. 2. Other FITOK valve are available for use with sample cylinders. Contact your authorized FITOK sales and service representative for details. Carrying Handle This carrying handle provides convenience to carry sample cylinders. The handle is made from 04 stainless steel and is available for use on 00 ml and larger cylinders, as well as 00 ml cylinders rated to 0 psig (44 bar). End Caps In order to enable users to transport pressurized samples in safety, end caps are offered by FITOK protecting valves against damage. Each cap threads onto a neck ring that has been peened to the cylinder neck. End caps are made from carbon steel and are available for use on 22 and 785 ml (1gal) cylinders, which can only be used with FITOK angle-pattern valves. To order, specify the cylinder part number followed by the part number of the accessory. End caps and neck rings on both ends of the cylinder are normal style. Carrying Handle

9 Sample Cylinders and Accessories Sample Cylinders and Accessories 10 Outage Tubes Features Standard materials are 16 stainless steel or alloy tubing Standard size or 1/2 Construction Outage tube is welded to the male inlet end of an adapter. This adapter is threaded into the port of a sample cylinder. Usage Outage tube is used to keep a certain space for gaseous phase, the space is determined by the length of outage tube. % outage = (vapor space/total volume) 100 To obtain an exact outage, each outage tube and cylinder assembly should be calibrated by a suitable method. The table below shows approximate outage tube length for standard sample cylinders: Tube Lengths Tube O.D. " 5/16" 1/2" 5/16" ( ± 10%) 00 22 785 (1 gal) 22 785 (1 gal) 00 00 Applied for double-ended and pressure rating 1800 psig cylinders Code Applied for single-ended and pressure rating psig cylinders Applied for double-ended and pressure rating 0 psig cylinders 87 85 5102 5112 5165 5200 5226 521 5717 51114 8221 8846 8452 5109 5159 5560 5162 5274 549 Minimum Vapor, % 10 20 0 Tube Length, in. Outage Tube Adapter Sampling methods and the use of the outage tube are described in technical publications such as ASTM D1265, Standard Method of Sampling Liquefied Petroleum Gases. 0.87 0.85 1.02 1.12 1.65 2.00 2.26 2.1.0 4.62 2.21.0 4.52 1.09 1.59 2.16 1.62 2.74 4.9 1.11 1.07 1.4 1.45 2.2 2.90.8.06 4.59 6.79 2.96 4.59 6.69 1.4 2.27.0 2.17.84 6.21 1.5 1.28 1.66 1.79 2.99.79 4..81 5.88 8.96.71 5.88 8.86 1.77 2.96 4.45 2.71 4.9 8.04 1.59 1. 1.98 2.1.67 4.69 5.62 4.56 7.17 11.14 4.46 7.17 11.04 2.12.65 5.60.26 6.0 9.86 1.84 1.71 2.1 2.46 4.4 5.59 6.74 5.1 8.46 1.1 5.21 8.46 1.21 2.46 4.4 6.74.81 7.12 11.68 Outage Tube Liquid L - Tube Length Vapor Space Standard tube length is 10" (25.4 ). Tube can be cut to desired length. Part Description 6L - SC18 - DN4 - T - PC - H2 - OT87-00 - F2 Cleaning and Packaging Outage Tube Code Carrying Handle Cap & Plug Cylinder Surface End Connection Working Material Series End Type Pressure FC-01 No No No No Special Treatment 1/8 Female 16L SS SC 5 Psig Single S N2 -ended 6L FC-02 F2 00 00 Outage Tube OD " Length 0.87" PTFE Coating T Female N4 1800 Psig 18 04L SS 4L H2 OT87 Cylinder OD 1.9 " to.5" Tube Fitting Plug TP Double -ended D Cylinder OD 1.9 " and 4 " H4 Pipe Plug PP Electropolishing E 1/2 Female 0 Psig N8 Alloy M PC Pipe Cap EC End Cap For Double -ended Only 290 290 Other outage tube code contained in tube lengths table of the above page. 22 22 785 785 Note: "Part Description" is used for composition rules of FITOK product model, Not suitable for specific product part number selection, not random combinations. If in doubt, please contact FITOK group or authorized agent.

11 Sample Cylinders and Accessories Sample Cylinders and Accessories 12 Miniature Sample Cylinders Features Part Description MC Series 6L - MC - DTS4-10 - F2 Working pressure up to: psig (69.0 bar) Capacity: 10, 25 and Single-ended and double-ended designs End connection: connected to /8" FITOK tube fittings or welded to " or /8" tubing Corrosion-resistant stainless steel construction Full-penetration butt weld construction Dimensions Dimensions, in inches (millimeters), are for reference only and are subject to change. 6L 4L Material Series Type 16L SS 04L SS MC S D Single-ended Double-ended TS4 TB6 FT6 End Connection " (6.4 mm) Fractional Tube Socket Weld /8 " (9.5 mm) Fractional Tube Butt Weld /8 " (9.5 mm) Tube 10 10 25 25 Cleaning and Packaging FC-01 F2 FC-02 0.065 (1.7) Nominal Thickness /8 (9.5) O.D. for Tube Fitting (6.4) I.D. for Tube Socket Weld Connection /8 (9.5) O.D. for Butt Weld Connection Note: "Part Description" is used for composition rules of FITOK product model, Not suitable for specific product part number selection, not random combinations. If in doubt, please contact FITOK company or authorized agents. 1.00 (25.4) A Cylinder Model Tolerance Working Pressure psig (bar) A in. (mm) Average Weight oz (g) Singleended Doubleended 10 25 10 25 ±10% ±5% ±10% ±5% (69.0) 2.19 (55.6).69 (9.7) 6.25 (159) 2. (69.8) 4.25 (108) 6.81 (17) 2.2 (62).2 (91) 5.6 (159) 1.9 (54). (94) 5.1 (145) Testing Each cylinder is tested at 2000 psig (18 bar) with nitrogen. Cautions: 1. Strong impingement should be rooted out for sample cylinder. 2. Sample cylinder should be kept off insolation and baking.. Sample cylinders are strictly prohibited roasting by fire when valve is freezed. 4. When the cylinder is using, the working pressure can not exceed its max working pressure.