BR 27g. Operating, assembly and maintenance instructions for discontinuous sampling valve. 1. Design, operation and dimensions:

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Operating, assembly and maintenance instructions for discontinuous sampling valve BR 27g The equipment may only be dismounted and disasembled by skilled staff, who are familiar with the assembly, start-up, and the operation of this product. Skilled staff in the sense of these repair and assembly instructions are persons who, as a result of their training, knowledge, and experience, also their knowledge of the relevant standards, are able to judge the tasks assigned to them, and are able to reconise possible dangers. 1. Design, operation and dimensions: Design, operation and dimensions, also all further technical details can found in the Data sheet <TB 27g> for sampling valve BR 27g. Fig. 1 - vertical sampling BR 27g in special design with heating case 2. Installation, start-up and maintenance: Guidelines for the installation, start-up and maintenance can be found in the operating instructions: For automatic ball valves Operating instructions <BA 27a-01>, For manually operated ball valves Operating instructions < BA 27a-02 > 0. Introduction: These instructions are intended to support the user in the assembly and repair of sampling valves of the BR 27g. Technical details, as a result of the further development of the valves mentioned in these instructions are subject to modifi - cation. The text and illustrations do not necessarily display the scope of supply, or an eventual order of spare parts. Drawings and graphics are not to scale. Customer related designs, which are not in accordance with our standard offer, are not shown. 1 of 10 Fig. 2 - Sectional view of sampling valve BR 27g => For parts list, see Table 1 on page 2

Fig. 3 - Explosion drawing of the sampling valve BR 27g Item Qty. Description Material Item Qty. Description Material 1 1 Main body 1.4571 8 1 Bonnet with sleeve 1.4571/PTFE-40% glass 2 1 Ball 1.4571 9 1 Running sleeve 1.4571 3 1 Stem 1.4571 15 4 Screw A2-70 4 1 Stuffi ng box 1.4571 16 1 Sampling adapter PTFE 5 1 Bearing bush PTFE mit 25% carbon 19 1 O-ring Viton 6 1 Bearing bush PTFE mit 25% glass 20 4 Screw A2-70 7 1 Sealing seat TFM 21 4 Washer A2 11 1 V-ring packing 1.4305 / PTFE 23 1 Sampling bottle Glass 12 1 O-ring Viton 13 1 Set of spring washers 1.8159 - Deltatone 14 2 Screw A2-70 17 1 Sealing ring PTFE 18 1 Spring washer 1.4310 Table 1 - Parts list 2 of 10

3. Assembly of the sampling valve: 3.1 Preparation for assembly Before assembling the sampling valve, clean all parts thoroughly, and lay them on a soft padded surface ( rubber mat etc.) Take into consideration, that parts made of plastic are generally soft and sensitive, in particular the sealing surfaces must be handled with care, and not be damaged. Note: The position and arrangment of the individual parts shown in ( Fig. 3 ) must be observed when assembling the valve. 3.2 Assembly of the sampling valve Position the main body ( 1 ) on a clean surface, with the sealing area of the ball facing upwards, and in a working height, so it is accessible for all assembly work. Place the seating ring ( 17 ) and the spring washer ( 18 ) in the body. The positioning of the spring washer is shown in the explosion drawing (Fig. 3) The bearing bush ( 6 ) is pressed into its intended position, for subsequent locating of the stem. After the sealing element, lower part ( 7 ) has been inserted, the stem ( 3 ) is then inserted into the pre-assembled bearing bush ( 6 ). The ball ( 2 ) with the slot is pressed onto the stem, and with evenly applied pressure, the stem is rotated and pressed until it fi nally sits in the sealing shell. Now, turn the ball 90 so that the sampling bore is facing forward. The sealing element, upper part ( 7 ) is inserted, then turn the ball is, so the sealing element locates cleanly into position. The O-ring ( 12 ) and the running sleeve ( 9 ) are placed onto the sealing element. Apply grease to the cheese-head screws ( 15 ) ( e.g.. Gleitmo grease 805, Fuchs or equivalent ). Then the bonnet together with insert ( 8 ) is mounted, and aligned with the cheese-head screws. Tighten the screws evenly, and in alternating pattern. Now turn the body, and place on the opposite facing fl ange, so that the stuffi ng box area is facing upwards and is easily accessible for further assembly work. Insert the PTFE - V-ring packing ( 11 ) into the body bore, in the following order; PTFE-bottom ring, PTFE-V-ringe and steel-v-ring. For exact positioning and locating of the V-ring packing and spring washers, refer to the explosion drawing (Fig. 3). Apply grease to the countersunk screws ( 14 ). The stuffi ng box ( 4 ), pre-assembled with the bearing sleeve ( 5 ), are mounted and aligned with the countersunk screws. Next, tighten the screws evenly and in alternating pattern. After the leak test of the sampling valve, the fi nal assembly can be carried out. The sampling valve is then turned and the fl ange is placed on a clean surface, and positioned, so that the bonnet with the insert is facing upwards, and accessable for further assembly. Apply grease to the screws ( 20 ). The sampling adapter ( 16 ), together with the O-ring ( 19 ), is attached, and aligned with the screws ( 20 ) and washers ( 21 ). After this, tighten the screws evenly and in alternating pattern. The assembly of the sampling valve is now completed. 4. Trouble shooting: Assistance in the case of malfunctions is provided in the operating instructions <BA 27a-01> for automatic control butterfl y valves, resp. <BA 10a-02> for manually-operated control butterfly valves under section 7. 5. Repairing the ball valve 5.1 Replacing the V-ring packing Should the ball valve leak at the packing, the V-ring packing ( 11 ) must be replaced as follows: - Loosen and remove the countersunk screws ( 14 ). - Take off the stuffi ng box fl ange ( 4 ). - Check the bearing bush ( 5 ) for damage, replace if necessary. - Remove the spring washers ( 13 ). - Remove the retainer ring from the V-ring packing. - Carefully remove the PTFE - V-rings ( 11 ) from the packing chamber of the valve body. - Check the V-rings for damage, if in doubt, replace with new ones. Reassembling the valve - To reassemble the valve, proceed in reverse order to the instructions mentioned above. For any missing descriptions or details, refer to the assembly instructions (Section 3). 3 of 10

5.2 Replacing the sealing rings and ball If the ball valve does not shut-off tightly and leaks, the sealing ring ( 7 ) and the ball ( 2 ) must be removed and checked as follows: Dismantling the sampling adapter - Loosen and remove the screws ( 20 ) together with the washers ( 21 ). - Remove the sampling adapter ( 16 ) and check the O-ring ( 19 ) for damage, and if necessary replace. Dismantling the first sealing ring - Loosen and remove the cheese-head screws ( 15 ). - Carefully remove the bonnet ( 8 ) and running sleeve ( 9 ). - Remove the O-ring ( 12 ) and check for damage, and if necessary replace. - Remove the sealing ring ( 7 ) and check for damage, and if necessary replace. Dismantling the V-ring packing - Loosen and remove the countersunk screws ( 14 ). - Take off the stuffi ng box fl ange ( 4 ). - Remove the bearing sleeve ( 5 ) and spring washers (13). - Remove the retainer ring of the V-ring packing. - Now, carefully remove the PTFE - V-rings of the V-ring packing ( 11 ) from the packing chamber of the body. Dismantling the body - Loosen and remove the cheese-head screws ( 15 ). - Carefully take off the bonnet ( 8 ) and running sleeve ( 9 ). - Remove the O-ring ( 12 ) and the sealing ring ( 7 ). Dismantling the ball - The ball ( 2 ) is now accessable in the body, and can now be carefully removed. Removing the ball - The ball ( 2 ) is now accessible in the body, and can now be carefully removed. - Check the ball for damage, and if necessary replace. Dismantling the second sealing ring - Remove the stem ( 3 ) and bearing bush ( 6 ) from the main body ( 1 ). - Remove the sealing ring ( 7 ) and check for damage, and if necessary replace. Dismantling the stem - Remove the stem ( 3 ) and bearing bush ( 6 ) from the body ( 1 ). - The stem ( 5 ) and the bearing bush ( 7 ) can now be checked for damage, and if necessary be replaced. Reassembling the valve - To reassemble the valve, proceed in reverse order to the instructions mentioned above. For any missing descriptions, or details, refer to the as sembly instructions in ( Section 3 ). Reassembling the valve - To reassemble the valve, proceed in reverse order to the assembly instructions. For any missing descriptions or details, refer to the assembly instructions in ( Section 3 ). 5.3 Dismantling the stem In case of damage, or in the course of replacing the sealing ring, it may be necessary to dismantle the stem ( 3 ) as follows: 6. Operating the sampling valve 6.1 Important general instructions It may be necessary to clean the sampling chamber, and blind hole after a sample has been taken. The operator must decide when this is necessary. It is absolutely important, that when taking a sample, the sampling container (glass bottle etc.) is adapted to the temperature of the media to be taken! Safety precautions must be taken when the media temperature exceeds 60 C as a risk of scalding is possible. When taking samples, the general accident prevention regulations must be complied with at all times! 4 of 10

6.2 Sampling valve with hand-lever Screw on the sample bottle by hand as tightliy as possible. Turn the hand-lever 180 until the bore is in the media fl ow. Turn back the handlever to allow the sample to fl ow into the bottle. Repeat this procedure until the required amount of media has been collected in the bottle, Unscrew the sample bottle, and if necessary seal bottle with a lid. 6.3 Sampling valve with hand-lever and protective case Open protective case. Screw on the sample bottle by hand as tightliy as possible. Turn hand-lever 180 until the bore is in the media fl ow. Turn back the lever to allow the sample to fl ow into the bottle. Repeat this procedure until the required amount of media has been collected in the bottle. Open the protective case, and remove the sample bottle, and if necessary seal bottle with a lid. 6.4 Sampling valve with hand-lever and protective case with support Open protective case. Pull down the support on the handlever. Place the sample bottle in the PTFEseat of the support. Guide the support upwards. Close the protective case. Turn the hand-lever 180 until the bore is in the media fl ow. Turn back the handlever to allow the media to fl ow into the bottle. Repeat this procedure until the required amount has been collected in the bottle. Open the protective case, guide the support downwards, remove sample bottle, and if necessary seal bottle with a lid. 6.5 Sampling valve with automated 180 rotary actuator and protective case 6.5.1 General automated sampling Open protective case. Screw on sample bottle by hand as tightly as possible. Open the air supply valve at the automation unit. Attention: Before operating, refer to the respective operating instructions for the automated unit, which can be found in Section 7 ( Operating the automated unit ). Close the supply valve at the automation unit. Open the protective case, and if necessary seal bottle with a lid. 6.5.2 automated sampling with back pressure indication Operating this type of sampling is identical to the operating instructions in Section 6.5.1 In addition to the above mentioned version, the following function is included: - The automation switches off automatically and no further sample can be taken when the sample level in the glass reaches the back pressure tube. When attaching the bottle, avoid at all times bending the back pressure tube! 6.5.3 automated sampling with pneumatic barrier Operating this type of sampling is identical to the operating instructions in Section 6.5.1 In addition to the above mentioned version, the following function is included: - The automation switches off automatically and no further sample can be taken, when the protective case is opended during the sampling procedure. 5 of 10

6. 6 Sampling valve with automated 180 rotary actuator and protective case with support 6.6.1 General automated sampling Open protective case. Pull down the support on the handlever. Place the sample bottle in the PTFE - seat of the support. Guide the support upwards. Open the air supply valve at the automation unit. Attention: Before operating, refer to the respective operating instructions for the automation unit, which can be found in Section 7 ( Operating the automation unit ). Close the air supply valve at the automation unit. Open protective case, guide the support downwards, remove sample bottle and if necessary seal bottle with a lid. 6.6.2 automated sampling with back pressure indication Operating this type of sampling is identical to the operating instructions in Section 6.6.1 In addition to the above mentioned version, the following function is included: - The automation switches off automatically and no further sample can be taken when the sample level in the glass reaches the back pressure tube. When attaching the bottle, avoid at all times bending the tube! 6.6.3 automated sampling with pneumatic barrier Operation for this type of sampling is identical to the operating instructions described in Section 6.6.1 In addition to the above mentioned version, the following function is included: - The automation switches off automatically and no further sample can be taken, when the protective case is opended during the sampling procedure. 7. Operation of automation units 7.1 Automation with ON/OFF - Switch Note: The pulse timing of actuation as well as the timing for fi lling the actuator with air, or venting it, are pre-set timings, which were set before leaving our factory. Any alterations to these settings may only be made after fi rst consulting Pfeiffer Chemie-Armaturenbau GmbH! Press the start button. A complete actuating cycle taking a sample is performed. Repeat this procedure until the required amount of media has been collected in the bottle. 7.2 Automation with counter Note: The pulse timing and intervals between actuation cycles and the timing for fi lling the actuator with air, or venting it, are pre-set timings, which were set before leaving our factory. Any alterations to these settings may only be made after fi rst consulting Pfeiffer Chemie-Armaturenbau GmbH! Set the number of actuating cycles at the counter. Attention: The selected number of actuating cycles to take samples must correspond to the volume of the sample bottle. Press the start button. The pre-selected number of actuating cycles to take samples, are performed. The sampling fi nishes automatically after the selected number of actuating cycles have been completed. Attention! In the event of an operation fault, press the emergency button immediately! 6 of 10

7.3 Automation with counter and timer switch Note: The pulse timing of actuation and the timing for fi lling the actuator with air or venting it, are pre-set timings, which were set before leaving our factory. Any alterations to these settings may only be made after fi rst consulting Pfeiffer Chemie-Armaturenbau GmbH! The required interval between each actuation cycle can be set at the timer switch Determine which timming you require. The required cycle time can be set by turning the outer ring. A pointer indicates the cycle time. Set the number of actuatioin cycles at the counter. Attention: The selected number of actuating cycles must correspond to the volume of the sample bottle. Press the start button. The pre-selected number of actuating cycles to take samples, together with the pre-selected intervals fi nishes automatically after the selected number of actuating cycles have been completed. Attention! In the event of an operation fault, press the emergency button immediately. Fig. 4 - Samsomatic - Time switch 3970 Select time range The switch-over range is selected with the rotary knob located in the middle of the timer, by setting the dial arrow to the required range. Selection s x10s m x10m h x10h Time range 0,3 to 6 seconds 3 to 60 seconds 0,3 to 6 minutes 3 to 60 minutes 0,3 to 6 hours 3 to 60 hours Table 2 - Time range 7 of 10

8. Circuit diagram Circuit diagram for the automatioin unit. Should you have any queries, please contact Pfeiffer Chemie-Armaturenbau GmbH Fig. 5 - Circuit diagram 8 of 10

9. Customer inquiries Details as per the check list for repairs and inquiries. Check list for repairs and inquiries for sampling valve Series 27g General Commission number: ( embossed on the type plate) Customer: Telephone: Fax: Media Media: Temperature: C op. pressure: bar Viscosity: like water like honey like oil others: Characteristic: toxic caustic corrosiveness abrasiv foaming others: Valve Nominal size: DN 25 DN 50 sampling volume 1 to 25ml Option Body: haste alloy C4 Titanium others: Ball Zirkonium oxid Titanium 0,2% Pd others: Add-on Components others: Sampling connection spring washer nickel plated O-ring Viton / FEP lined heating case Duran GL45 fl ange connection bajonet connection others: Duran GL32 others: Attachment: protection case others: Accessories Protection case Standard 1 venting others: Support (not for bajonet locking) Automation: with counter ON / OFF time switch Actuator: multi turn actuator (DAP 60-180 ) hand lever Actuator Manufacturer: Type: Sampling: container others: sample bottle DIN 4796 GL45 Duran clear glass will be supplied by customer others: Table 3 - Check list 9 of 10

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