CH361/361H Week 5 Lecture Synthesis of. 2,3-Dimethylbutene Isomers. Identify unknown. carboxylic acid

Size: px
Start display at page:

Download "CH361/361H Week 5 Lecture Synthesis of. 2,3-Dimethylbutene Isomers. Identify unknown. carboxylic acid"

Transcription

1 sodium salt of unknown aromatic carboxylic acid + soluble impurities + insoluble impurities total mass:? g insoluble impurities mass:? g dissolve in water, filter aq. sol n of unk. sodium salt + sol. impurities decolorize, filter account for all masses; calculate %recovery 361/361 Week 5 Lecture Synthesis of Identify unknown carboxylic acid 2,3-Dimethylbutene Isomers colored dye(s) mass: ~ 20 mg aq. sol n of unk. sodium salt + sol. impurities conc. l; filter mp, MW, pk a, derivative mp water-soluble imp. crude unk. carboxylic acid mass:? g recrystallize pure unk. carboxylic acid mass:? g melting point ( mp )

2 Experiment II verview: reparation & Equilibration of Isomeric 2,3-Dimethylbutenes cat K eq =? ΔG =? Δ =? ΔS =? 2,3-dimethyl-2-butene 2-ene 2,3-dimethyl-1-butene major activities in experiment II RERT 2 synthesis of 2-ene (major) / mixture by Grignard reaction followed by acid mediated dehydration (E1 elimination) last name starts with M-Z synthesis of by Wittig olefination last name starts with A-L purification and isomer separation by distillation / fractional distillation RERT 3 equilibration of alkene isomers and analysis of alkene isomer distributions by gas chromatography (G) determination of thermodynamic properties (DG, D, DS ) by analyzing temperature dependence of equilibrium constant (K eq )

3 Synthetic Strategy: ow to Make Alkenes from 3-Methylbutanone δ δ+? + 3-methylbutanone "2-ene" "1-ene" 3 3 -centered nucleophile -centered electrophile

4 Grignard Reaction/Dehydration: 1. Formation of Grignard / Addition to Ketone 3 δ+ δ Mg magnesium metal δ δ+ 3 I 3 MgI δ δ+ iodomethane (methyl iodide) diethyl ether (Et 2 ) methylmagnesium iodide (a synthetic equivalent of methyl carbanion) S 3 + p-toluenesulfonic acid aq. l MgI 2-ene major product minor product F. A. Victor Grignard winner of 1912 Nobel rize 2,3-dimethylbutan-2-ol purified by simple distillation magnesium alkoxide

5 Grignard Reaction/Dehydration: 2. Dehydration Reaction (E1 Elimination) tertiary (3 ) carbocation 2 S 3 + p-toluenesulfonic acid 2-ene major product bp. 72 minor product bp. 56 separated by fractional distillation 2,3-dimethylbutan-2-ol purified by simple distillation

6 Experimental Set-Up for Grignard Reaction (IN FUME D) READ SAFETY NTE iodomethane is a cancer suspect agent; ALL WRK IN D! (wear proper E); RB will depense iodomethane into press. equal. funnels for you diethyl ether is highly flammable; Grignard reagents are potentially pyrophoric important that glassware is dried in oven, assembled quickly, and flushed with nitrogen BEFRE finishing on Wed., leave glassware in metal bowl ready to be oven dried before Friday s lab

7 Wittig lefination to Generate Directly Na Br NaMe 2 Et sodium tert-pentoxide MeN NBu BF 4 methyltriphenylphosphonium Georg Wittig bromide winner of 1979 Nobel rize bmim + BF an ionic liquid methylenetriphenylphosphorane a phosphorus ylide 2 h + 3 h 3 2 h 3 triphenylphosphine oxide the oxaphosphetane the betaine (a zwitterion)

8 Wittig lefination to Generate Directly Na Br NaMe 2 Et sodium tert-pentoxide MeN NBu BF 4 methyltriphenylphosphonium bromide bmim + BF an ionic liquid methylenetriphenylphosphorane a phosphorus ylide 2 h + 3 h 3 2 h 3 triphenylphosphine oxide the oxaphosphetane the betaine (a zwitterion)

9 Experimental Set-Up for Wittig lefination (on bench) YUR LAB MANUAL NTAINS LDER REDURE BE SURE T LLET ANDUT TDAY (p ) READ SAFETY NTE use of dust mask is ESSENTIAL to avoid unintended inhaltion of finely powdered sodium tertpentoxide; other E as usual (gloves, lab coat, goggles) important that glassware is dried in oven, assembled quickly, and flushed with nitrogen BEFRE finishing on Wed., leave glassware in metal bowl ready to be oven dried before Friday s lab

More Carbonyl Chemistry

More Carbonyl Chemistry Lecture 15 More arbonyl hemistry Shared Nobel Prize with Sabatier in 1912 student of Philippe Barbier François Auguste Victor Grignard 1871-1935 March 3, 2016 Reaction Theme The most common reaction of

More information

19. The Grignard Reaction

19. The Grignard Reaction 19. The Grignard eaction A. Introduction The Grignard reaction is an extremely valuable reaction in organic chemistry because it allows for the formation of carbon-carbon bonds. The reaction was discovered

More information

CHEM254 #4 The Synthesis of a Tertiary Alcohol Using a Pre-Made Grignard Reagent 1

CHEM254 #4 The Synthesis of a Tertiary Alcohol Using a Pre-Made Grignard Reagent 1 CHEM254 #4 The Synthesis of a Tertiary Alcohol Using a Pre-Made Grignard Reagent 1 Background In this project, we will perform a Grignard reaction using a pre-made Grignard reagent. Grignard reagents can

More information

François Auguste Victor Grignard, was a French chemist who discovered one of the world s first synthetic organometallic reactions.

François Auguste Victor Grignard, was a French chemist who discovered one of the world s first synthetic organometallic reactions. CHEM254 #6 The Synthesis of a Tertiary Alcohol Using a Pre-Made Grignard Reagent 1 Introduction/Background Image: François Auguste Victor Grignard (1871-1935) 1 François Auguste Victor Grignard, was a

More information

Paper No and Title. Paper 9: Organic Chemistry-III (Reaction Mechanism-2) Module no.13: Addition of Grignard reagent

Paper No and Title. Paper 9: Organic Chemistry-III (Reaction Mechanism-2) Module no.13: Addition of Grignard reagent Subject Chemistry Paper No and Title Module No and Title Module Tag 9: Organic Chemistry-III (Reaction Mechanism-2) 13: Addition of Grignard reagent CHE_P9_M13 TABLE OF CONTENTS 1. Learning Outcomes 2.

More information

More Carbonyl Chemistry

More Carbonyl Chemistry Lecture 16 More arbonyl hemistry March 8, 2018 Victor Grignard Georg Wittig Exam II Wed March 21 from 7pm to 9pm In this room overs through todays lecture Know the reactions Play cards Please practice.old

More information

Grignard Reaction * Mary McHale. 1 Lab 3: Grignard Reaction

Grignard Reaction * Mary McHale. 1 Lab 3: Grignard Reaction OpenStax-CNX module: m15245 1 Grignard Reaction * Mary McHale This work is produced by OpenStax-CNX and licensed under the Creative Commons Attribution License 2.0 1 Lab 3: Grignard Reaction 1.1 Objective

More information

Chemistry 222 Fall 2012

Chemistry 222 Fall 2012 Experiment 2: Grignard Reaction Report Sheet Last Name: Siva First Name: Krishnaa Date: September 27, 2012 Section Number: 005 Objective: 1 mark (What is the purpose of this experiment?) The purpose of

More information

Grignard Reaction. John Goodwin. Since Victor Grignard discovered his Grignard reagent 110 years ago, these

Grignard Reaction. John Goodwin. Since Victor Grignard discovered his Grignard reagent 110 years ago, these Grignard Reaction John Goodwin Abstract Since Victor Grignard discovered his Grignard reagent 110 years ago, these organomagnesium compounds have been highly utilized in synthetic organic chemistry. These

More information

Pyrrole Chemistry. Part XII. The Mechanism of the Reaction Between the Pyrrole Grignard Reagent and Acylating Agents1

Pyrrole Chemistry. Part XII. The Mechanism of the Reaction Between the Pyrrole Grignard Reagent and Acylating Agents1 Pyrrole Chemistry. Part XII. The Mechanism of the Reaction Between the Pyrrole Grignard Reagent and Acylating Agents1 C. E. LOADER AND HUGH J. ANDERSON Department of Chemistry, Memorial University, St.

More information

Material Safety Data Sheet (MSDS) Barium Chlorate

Material Safety Data Sheet (MSDS) Barium Chlorate Material Safety Data Sheet (MSDS) Section 1: Chemical Product Product Name: CAS Number: Synonym: Chemical Name: Chemical Formula: 13477-00-4 Chloric Acid Barium Salt Ba(ClO3)2 Composition: Section 2: Composition

More information

Name:. Correct Questions = Wrong Questions =.. Unattempt Questions = Marks =

Name:. Correct Questions = Wrong Questions =.. Unattempt Questions = Marks = Name:. Correct Questions = Wrong Questions =.. Unattempt Questions = Marks = Lab Problem 1 Design and carry out an experiment to determine the density of the plastic object you have been given. You may

More information

N,N-Dimethyl-p-phenylenediamine Sulfate

N,N-Dimethyl-p-phenylenediamine Sulfate MSDS Number: D6371 * * * * * Effective Date: 11/10/05 * * * * * Supercedes: 02/18/03 N,N-Dimethyl-p-phenylenediamine Sulfate 1. Product Identification Synonyms: None CAS No.: 60160-75-0 Molecular Weight:

More information

Optima Chemical Group LLC Revision : 1 Page 1 Product Name: Tert-butylmagnesium Chloride in DEE of 5 Material Safety Data Sheet Effective Date: 5/10

Optima Chemical Group LLC Revision : 1 Page 1 Product Name: Tert-butylmagnesium Chloride in DEE of 5 Material Safety Data Sheet Effective Date: 5/10 Optima Chemical Group LLC Revision : 1 Page 1 Section 1 Chemical Product and Company Identification MSDS Name: Tert-butylmagnesium Chloride in DEE Chemical Family: Grignard Reagent Molecular Formula: C

More information

Part 1: Distillation and Analysis of an Unknown Alcohol Mixture

Part 1: Distillation and Analysis of an Unknown Alcohol Mixture Experiment DE: Part 1 Experiment DE has multiple goals, including -separation and quantification of a 2-component mixture (fractional distillation and GC); preliminary ID of both components -preparation

More information

Chemical Class Standard Operating Procedures. Pyrophoric Chemicals (PYR) & Water Reactive Chemicats (WRC) Diethylzinc

Chemical Class Standard Operating Procedures. Pyrophoric Chemicals (PYR) & Water Reactive Chemicats (WRC) Diethylzinc Chemical Class Standard Operating Procedures Pyrophoric Chemicals (PYR) & Water Reactive Chemicats (WRC) Diethylzinc Department: Chemistry Date SOP was written: April 16, 2014 Principal Investigator: Dr.

More information

Ceftriaxone for Injection, USP 500mg Vial: 1g Vial: 2g Vial: 10g Vial:

Ceftriaxone for Injection, USP 500mg Vial: 1g Vial: 2g Vial: 10g Vial: 1. PRODUCT AND COMPANY INFORMATION Distributed By: 120 Route 17 North Suite 115 Paramus, NJ 07652 USA Product Name: Product Code: Common / Trade Name: 500mg Vial: 1g Vial: 2g Vial: 10g Vial: 44567-700-25

More information

General Chemistry I Percent Yield of Hydrogen Gas From Magnesium and HCl

General Chemistry I Percent Yield of Hydrogen Gas From Magnesium and HCl Introduction For chemical reactions involving gases, gas volume measurements provide a convenient means of determining stoichiometric relationships. A gaseous product is collected in a long, thin graduated

More information

Phytodeket Test Kit. Phytodeket Test Kit (all PDK catalog numbers) contains the following components:

Phytodeket Test Kit. Phytodeket Test Kit (all PDK catalog numbers) contains the following components: Phytodeket Test Kit DRAFT: 1-Dec-217 Phytodeket Test Kit (all PDK catalog numbers) contains the following components: Stick Controls and Standards Coated Plates Phytodetek tracer, liquid Component SDS

More information

Alfa Aesar/Avocado Organics Material Safety Data Sheet A10559

Alfa Aesar/Avocado Organics Material Safety Data Sheet A10559 1. IDENTIFICATION OF SUBSTANCE AND SUPPLIER Name On Label : Methyl iodide Product Number : A10559 Supplier : Johnson Matthey Catalog Company Inc. 30 Bond Street, Ward Hill, Massachusetts, 01835 8099 Emergency

More information

For laboratory research use only, not for diagnostics or therapeutics in humans or animals

For laboratory research use only, not for diagnostics or therapeutics in humans or animals MSDS ELISA Kits For laboratory research use only, not for diagnostics or therapeutics in humans or animals Contacts: FIVEphoton Biochemicals 4907 Morena Blvd, Ste 1403 San Diego, CA 92117 Tel: 800.462.4507

More information

Figure. Experimental set up of catalyst, reactants and product syringes.

Figure. Experimental set up of catalyst, reactants and product syringes. Construction and Use of the Gas Reaction Catalyst Tube** As shown in the figures, the experimental apparatus consists of a 60 ml syringe containing the gaseous reactants connected to a gas phase catalyst

More information

CH 2 CH 2 CHO CH 3. (d) C H PCC PCC H 3 O + LiAlH PCC CH 2 Cl 2 CH 3 CH 2 CH 2 CH 2 CHO

CH 2 CH 2 CHO CH 3. (d) C H PCC PCC H 3 O + LiAlH PCC CH 2 Cl 2 CH 3 CH 2 CH 2 CH 2 CHO hem 226 Problem Set #9 Fundamentals of rganic hemistry, 4 th edition, John McMurry. hapter 9 2. Name the following aldehydes and ketones. 3 2 ( 3 ) 2 (c) 3 2 2 2 2 3 2 2 (d) 3 2-methyl-3-pentanone, 3-phenylpropanal,

More information

MINIMUM SAFETY REGULATIONS

MINIMUM SAFETY REGULATIONS MINIMUM SAFETY REGULATIONS These rules are intended to apply to all students, postdoctoral fellows, and staff engaged in laboratory work in a working lab. A working laboratory is a room used for any purpose

More information

Ceftriaxone for Injection, USP

Ceftriaxone for Injection, USP 1. PRODUCT AND COMPANY INFORMATION Distributed By: 120 Route 17 North Suite 115 Paramus, NJ 07652 USA Product Name: Active Ingredient/Primary Component: Structure: Chemical Name: (1) 5-Thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylic

More information

D. De La Matter 2004 Swimming Pool Chemistry STUDENT ACTIVITIES:

D. De La Matter 2004 Swimming Pool Chemistry STUDENT ACTIVITIES: D. De La Matter 2004 Swimming Pool Chemistry STUDENT ACTIVITIES: Good News! Flinn Scientific Inc. has developed a classroom kit of experiments based on these activities. The Kit Catalog # is AP6599. Ordering

More information

Working correctly with gas

Working correctly with gas Working correctly with gas When working with a reactive gas in a cylinder, there is an inherent risk. Special care has to be taken to allow safe handling. This example is with HCl. 1) Fixing the gas bottle.

More information

Date Prepared February 26 th, 2013 Signature of Preparer

Date Prepared February 26 th, 2013 Signature of Preparer Material Safety Data Sheet Used to comply with OSHA s Hazard Communication Standard 29 CFR 1910.1200 IDENTITY (As used on label or list) Inorganic Glass: Red, Orange and Yellow colors Note: Blank spaces

More information

Ring-Closing Metathesis Approaches for the Solid- Phase Synthesis of Cyclic Peptoids

Ring-Closing Metathesis Approaches for the Solid- Phase Synthesis of Cyclic Peptoids Supporting Information (SI) Ring-Closing Metathesis Approaches for the Solid- Phase Synthesis of Cyclic Peptoids Sharaf awaz Khan, Arim Kim, Robert. Grubbs, and Yong-Uk Kwon*, Department of Chemistry and

More information

Physical Pharmacy. Solubility. Khalid T Maaroof MSc. Pharmaceutical sciences School of pharmacy Pharmaceutics department

Physical Pharmacy. Solubility. Khalid T Maaroof MSc. Pharmaceutical sciences School of pharmacy Pharmaceutics department Physical Pharmacy Solubility Khalid T Maaroof MSc. Pharmaceutical sciences School of pharmacy Pharmaceutics department 1 Definition Solubility is the maximum amount of a solid, liquid or a gas solute that

More information

Material Safety Data Sheet

Material Safety Data Sheet 1. Identification Material Safety Data Sheet Product Name: Original Name: Substance: Hydroxypropyl Methylcellulose E464 Hydroxypropyl Methylcellulose Manufacturer s Name: Section: Address: Phone Number:

More information

MATERIAL SAFETY DATA SHEET

MATERIAL SAFETY DATA SHEET reviewed by MC 1. Identification of substance Substance: Clear Seal Supplier: American Wood Oil European Factory Agency Bredestraat 4 B 2000 Antwerp, Belgium E- mail : info@americanwoodoil.com Telephone:

More information

(1) PRODUCT AND COMPANY IDENTIFICATION (2) HAZARDS IDENTIFICATION (EC)

(1) PRODUCT AND COMPANY IDENTIFICATION (2) HAZARDS IDENTIFICATION (EC) . (1) PRODUCT AND COMPANY IDENTIFICATION Identification of the substance or preparation TRADE/MATERIAL NAME: CHEMICAL NAME: SYNONYMS: Graphene Nanoplatelets Graphene Few-layered graphene This SDS is valid

More information

The Determination of the Value for Molar Volume

The Determination of the Value for Molar Volume Name AP Chemistry The Determination of the Value for Molar Volume Objective Using a chemical reaction that produces a gas, measure the appropriate values to allow a determination of the value for molar

More information

Gas Laws. 2 HCl(aq) + CaCO 3 (s) H 2 O(l) + CO 2 (g) + CaCl 2 (aq) HCl(aq) + NaHCO 3 (s) H 2 O(l) + CO 2 (g) + NaCl(aq)

Gas Laws. 2 HCl(aq) + CaCO 3 (s) H 2 O(l) + CO 2 (g) + CaCl 2 (aq) HCl(aq) + NaHCO 3 (s) H 2 O(l) + CO 2 (g) + NaCl(aq) Gas Laws Introduction: Although we cannot see gases, we can observe their behavior and study their properties. For example, we can watch a balloon filled with helium gas floating in air and conclude that

More information

The Determination of the Value for Molar Volume

The Determination of the Value for Molar Volume Objective The Determination of the Value for Molar Volume Using a chemical reaction that produces a gas, measure the appropriate values to allow a determination of the value for molar volume. Brief Overview

More information

CHM 317H1S Winter Section P Procedures and Tables

CHM 317H1S Winter Section P Procedures and Tables CHM 317H1S Winter 2018 Section P Procedures and Tables Procedures Page 1 Standard Operating Procedures Throughout the laboratory portion of this course, you will be required to perform a number of operations

More information

GRADE 6: Materials 1. UNIT 6M.1 7 hours. Solubility. Resources. About this unit. Previous learning. Expectations. Key vocabulary and technical terms

GRADE 6: Materials 1. UNIT 6M.1 7 hours. Solubility. Resources. About this unit. Previous learning. Expectations. Key vocabulary and technical terms GRADE 6: Materials 1 Solubility UNIT 6M.1 7 hours About this unit This is the first of four units on materials in Grade 6. This unit builds on the study of the properties of water in Unit 5M.1. Unit 7M.1

More information

PREPARING GAS SAMPLES IN LARGE PLASTIC SYRINGES

PREPARING GAS SAMPLES IN LARGE PLASTIC SYRINGES PREPARING GAS SAMPLES IN LARGE PLASTIC SYRINGES A wide variety of gases can be prepared safely inside a 60 ml plastic syringe. Here you will practice making carbon dioxide, so that you know the technique

More information

The Safe Use of Pyrophoric Substances

The Safe Use of Pyrophoric Substances The Safe Use of Pyrophoric Substances INTRODUCTION In light of a fatality of a researcher earlier this year at UCLA, The University of Queensland has released a guideline for The Safe Use of Pyrophoric

More information

MATERIAL SAFETY DATA SHEET

MATERIAL SAFETY DATA SHEET MATERIAL SAFETY DATA SHEET SECTION I - Product / Company Identification Product Trade Name: ZINC PHOSPHATE CEMENT - POWDER Part (Item) Number: 35-21-1, 35-31-1, 35-41-1,35-81-1 Manufacturer: DENTAL TECHNOLOGIES,

More information

Safety Data Sheet. (Magnesium Aspartate 20%) DATE PREPARED: 6/15/2015. Section 1. Product and Company Identification

Safety Data Sheet. (Magnesium Aspartate 20%) DATE PREPARED: 6/15/2015. Section 1. Product and Company Identification Section 1. Product and Company Identification Product Name Magnesium Aspartate 20% CAS Number 7018-07-7 Parchem - fine & specialty chemicals 415 Huguenot Street New Rochelle, NY 10801 (914) 654-6800 (914)

More information

Gas Laws. 2 HCl(aq) + CaCO 3 (s) H 2 O(l) + CO 2 (g) + CaCl 2 (aq) HCl(aq) + NaHCO 3 (s) H 2 O(l) + CO 2 (g) + NaCl(aq)

Gas Laws. 2 HCl(aq) + CaCO 3 (s) H 2 O(l) + CO 2 (g) + CaCl 2 (aq) HCl(aq) + NaHCO 3 (s) H 2 O(l) + CO 2 (g) + NaCl(aq) Gas Laws Introduction: Although we cannot see gases, we can observe their behavior and study their properties. For example, we can watch a balloon filled with helium gas floating in air and conclude that

More information

MATERIAL SAFETY DATA SHEET HIGH SPEED DIESEL

MATERIAL SAFETY DATA SHEET HIGH SPEED DIESEL MATERIAL SAFETY DATA SHEET HIGH SPEED DIESEL 1. Chemical Identification Chemical Name : Diesel Oil Chemical classification : Flammable Liquid Synonyms : Automotive Diesel Oil Trade name : HSD Formula :

More information

1. Product Identification

1. Product Identification POTASSIUM CHLORIDE TECHNICAL GRADE 1. Product Identification Synonyms: Potassium monochloride CAS No.: 7447-40-7 Molecular Weight: 74.55 Chemical Formula: KCl 2. Composition/Information on Ingredients

More information

Guidelines for Handling Dry Materials

Guidelines for Handling Dry Materials Guidelines for Handling Dry Materials What is Today s Focus? Dry chemicals or materials that could pose a hazard due to physical and toxicological characteristics. Can be natural or manmade, but will focus

More information

MSDS Number: M0140 * * * * * Effective Date: 08/02/07 * * * * * Supercedes: 11/16/04 MAGNESIUM CARBONATE

MSDS Number: M0140 * * * * * Effective Date: 08/02/07 * * * * * Supercedes: 11/16/04 MAGNESIUM CARBONATE MSDS Number: M0140 * * * * * Effective Date: 08/02/07 * * * * * Supercedes: 11/16/04 MAGNESIUM CARBONATE 1. Product Identification Synonyms: Magnesium carbonate hydroxide; Magnesium carbonate basic CAS

More information

2-AMINOANTHRACENE HAZARDS IDENTIFICATION Classification: According to regulation (EC) No 1272/2008 Labelling and

2-AMINOANTHRACENE HAZARDS IDENTIFICATION Classification: According to regulation (EC) No 1272/2008 Labelling and 2-AMINOANTHRACENE 1. IDENTIFICATION OF SUBSTANCE / PREPARATION AND THE COMPANY UNDERTAKING Chemical name: Product code: PPC-AA01, PPC-AA02 Synonyms: 2-Anthramine Recommended uses: For R&D purposes Supplier:

More information

Safety Data Sheet. Kit summary

Safety Data Sheet. Kit summary 1 Safety Data Sheet Kit summary Following components used as mixtures in the kit are defined as hazardous chemical according to the Regulation (EC) N 1272/2008. Component EC-No CAS-No % weight Classification

More information

Material Safety Data Sheet

Material Safety Data Sheet 1/5 1 PRODUCT AND COMPANY IDENTIFICATION Product Name Product Code FSQ-301, 301S SUPPLIER Name Address TOYOBO Co., Ltd. 2-8 Dojima Hama 2-chome, Kita-Ku OSAKA 530-8230 JAPAN Department Life Science Department

More information

Laboratory Standard Operating Procedure: Acutely Toxic Substances

Laboratory Standard Operating Procedure: Acutely Toxic Substances I. CONTACT INFORMATION Procedure Title Procedure Author Date of Creation/Revision: April 12, 2013 Name of Responsible Person Location of Procedure (The PI, Lab Supervisor, or Autonomous Researcher) (Building

More information

Safe Use of Solvent Stills

Safe Use of Solvent Stills Safe Use of Solvent Stills Introduction: o The following guide is intended to describe the minimum requirements for using the hot pot distillation technique. o Lab workers who intend to use the hot pot

More information

: Magnetic Latent print Powder, White, Disposable

: Magnetic Latent print Powder, White, Disposable SECTION 1: Identification of the substance/mixture and of the company/undertaking 1.1. Product identifier Product form Product name. Product code : Mixture : : M116LD 1.2. Relevant identified uses of the

More information

A SIMPLE TITRATION METHOD FOR DETERMINING THE SPECIFIC GRAVITY ON ONE DROP OF URINE

A SIMPLE TITRATION METHOD FOR DETERMINING THE SPECIFIC GRAVITY ON ONE DROP OF URINE J. clin. Path. (1951), 4, 491. A SIMPLE TITRATION METHOD FOR DETERMINING THE SPECIFIC GRAVITY ON ONE DROP OF URINE BY From the Pathological Laboratory, the Peace Memorial Hospital, Watford (RECEIVED FOR

More information

Material Safety Data Sheet

Material Safety Data Sheet Material Safety Data Sheet BNP Fragment (Nt-proBNP 8-29) ELISA Catalog Number: 04-BI-20852 SAFETY DATA SHEET 1. Identification of product and company Product Name: BNP Fragment EIA 96t Catalogue Nr.: Normal

More information

SAFETY DATA SHEET ZERO VALENT IRON POWDER

SAFETY DATA SHEET ZERO VALENT IRON POWDER SAFETY DATA SHEET ZERO VALENT IRON POWDER Revision Date 2/24/2017 1. PRODUCT AND COMPANY IDENTIFICATION 1.1 Product identifiers Product name Zero valent iron powder Brand Compass Remediation Chemicals

More information

CALCIUM CARBONATE. 2. Composition/Information on Ingredients Ingredient CAS No Percent Hazardous. Calcium Carbonate % Yes

CALCIUM CARBONATE. 2. Composition/Information on Ingredients Ingredient CAS No Percent Hazardous. Calcium Carbonate % Yes CALCIUM CARBONATE H.M.S. Beagle 180 English Landing Drive Suites 110-120 Parkville, MO 64152 816-587-9998 www.hms-beagle.com 1. Product Identification Synonyms: Carbonic acid calcium salt; calcite; aragonite;

More information

Laboratory Standard Operating Procedure: Carcinogens

Laboratory Standard Operating Procedure: Carcinogens I. THIS STANDARD OPERATING PROCEDURE (SOP) IS FOR A: Specific laboratory procedure or experiment Examples: synthesis of chemiluminescent esters, folate functionalization of polymeric micelles, etc. Generic

More information

PRE LABORATORY ASSIGNMENT: Lab Section Score: /10 READ THE LAB TEXT BEFORE ATTEMPTING THESE PROBLEMS!

PRE LABORATORY ASSIGNMENT: Lab Section Score: /10 READ THE LAB TEXT BEFORE ATTEMPTING THESE PROBLEMS! EXPERIMENT # 6 Name: PRE LABORATORY ASSIGNMENT: Lab Section Score: /10 READ THE LAB TEXT BEFORE ATTEMPTING THESE PROBLEMS! 1. Calculate the height of a corresponding column of mercury (in mm) that is at

More information

Material Safety Data Sheet. ACS Material Silicon/Silicon Dioxide Wafer

Material Safety Data Sheet. ACS Material Silicon/Silicon Dioxide Wafer Material Safety Data Sheet ACS Material Silicon/Silicon Dioxide Wafer Table of contents 1 Product and Company Identification 9 Physical and Chemical Properties 2 Composition / Information on Ingredients

More information

NAME: HYDROGEN PEROXIDE 3% USP FOR 55 GAL DRUM

NAME: HYDROGEN PEROXIDE 3% USP FOR 55 GAL DRUM Revised: 5/23/16 SAFETY DATA SHEET Page 1 of 5 Humco Holding Group, Inc. 7400 Alumax Dr Texarkana TX 75501 USA 800-662-3435 cs@humco.com www.humco.com 24-Hour Emergency Number (CHEMTREC) USA- 800-424-9300

More information

Measurements of k L a. Steady-State Mass Balance Method:

Measurements of k L a. Steady-State Mass Balance Method: Measurements of k a Steady-State Mass Balance Method: In theory, the K a in an apparatus that is operating continuously under steady-state conditions could be evaluated from the flow rates and the concentrations

More information

Safety Data Sheet SUPER RID ICE

Safety Data Sheet SUPER RID ICE Section 1: Identification Product Name: Other means of identification: Recommended Use: Safety Data Sheet SUPER RID ICE None Ice melt Manufacturer BCA Products 24399 225th Avenue P.O. Box 429 Sleepy Eye,

More information

S A F E T Y D A T A S H E E T

S A F E T Y D A T A S H E E T SECTION 1 - SUBSTANCE IDENTITY AND COMPANY INFORMATION Product Name: Various Animal Cell Cultures at Biosafety Level 1 or 2 ATCC Catalog #: Various COMPANY INFORMATION: AMERICAN TYPE CULTURE COLLECTION

More information

3 Solubility and Concentration

3 Solubility and Concentration CHAPTER 8 SECTION Solutions 3 Solubility and Concentration KEY IDEAS As you read this section, keep these questions in mind: What is solubility? What happens when you add more solute to a saturated solution?

More information

SAFETY DATA SHEET. Pink Dishwash Detergent. 1. Product and Company Identification. 2. Hazards Identification

SAFETY DATA SHEET. Pink Dishwash Detergent. 1. Product and Company Identification. 2. Hazards Identification Product Code: Product Name: Company Name: Web site address: 255 Genlabs 5568 Schaefer Ave. Chino, CA 9171 1. Product and Company Identification www.genlabscorp.com Phone Number: 1 (99)591-8451 Emergency

More information

Safety data sheet DEGADECK POLYMER CONCRETE FILLER Revision date : 2009/03/18 Page: 1/6

Safety data sheet DEGADECK POLYMER CONCRETE FILLER Revision date : 2009/03/18 Page: 1/6 Revision date : 2009/03/18 Page: 1/6 1. Substance/preparation and company identification Company BASF Construction Chemicals 100 Campus Drive Florham Park, NJ 07932 24 Hour Emergency Response Information

More information

PO Box 12205, Shawnee, KS Phone: or ; Fax: or

PO Box 12205, Shawnee, KS Phone: or ; Fax: or SAFETY DATA SHEET PhytoTechnology Laboratories 1. CHEMICAL IDENTIFICATION AND COMPANY INFORMATION PRODUCT NAME: PRODUCT NUMBER: COMPANY INFO: Glycine G503 PhytoTechnology Laboratories PO Box 12205, Shawnee,

More information

Objective To identify a pure liquid substance using the physical properties of solubility, density, and boiling point.

Objective To identify a pure liquid substance using the physical properties of solubility, density, and boiling point. Chemistry 1020 Identification of an Unknown Liquid Objective To identify a pure liquid substance using the physical properties of solubility, density, and boiling point. Text reference solubility, density,

More information

I. Colorimetric Determination of Trimethylamine as the

I. Colorimetric Determination of Trimethylamine as the Amines in Fish Muscle I. Colorimetric Determination of Trimethylamine as the Picrate Salt I ABSTRACT 1 A sensitive accurate colorimetric method for trimethylamine determination is presented, based on the

More information

: NICOTINIC ACID IMPURITY MIXTURE CRS

: NICOTINIC ACID IMPURITY MIXTURE CRS Date of issue: 27/06/2013 Revision date: 27/06/2013 Supersedes: 17/12/2009 Version: 2.0 SECTION 1: Identification of the substance/mixture and of the company/undertaking 1.1. Product identifier Product

More information

1. The Safe Use of Pyrophoric Reagents

1. The Safe Use of Pyrophoric Reagents Rubin s group laboratory operating procedure series 1. The Safe Use of Pyrophoric Reagents REVISION RECORD Rev.# Date By Description 1 August 17, 2009 Mitsuharu Suzuki Initial release APPROVED (Signature

More information

This product is intended for research and laboratory use only. This product is not to be used as human or

This product is intended for research and laboratory use only. This product is not to be used as human or 1 Identification Product Name: Catalog Number: Glycine G007 Company: Caisson Laboratories Address: 836 South 100 East, Smithfield, UT 84335 Telephone: 435.755.7615 Fax: 435.755.7617 Emergency Contact:

More information

PPH CERKAMED Material Safety Data Sheet SYNTEX PASTE A -

PPH CERKAMED Material Safety Data Sheet SYNTEX PASTE A - Page 1 of 5 MSDS is prepared in accordance with REGULATION (EC) No 1272/2008 OF THE EUROPEAN PARLIAMENT AND OF THE COUNCIL of 16 December 2008 on classification, labelling and packaging of substances and

More information

MATERIAL SAFETY DATA SHEET D5-[60]PCBM (99.5%)

MATERIAL SAFETY DATA SHEET D5-[60]PCBM (99.5%) MATERIAL SAFETY DATA SHEET D5-[60]PCBM (99.5%) Section 1 Product and Manufacturer Information Product Identifier: [6,6]-Pentadeuterophenyl-C61-butyric acid methyl ester Product Code: d-060995 Identified

More information

M a t e r i a l S a f e t y D a t a S h e e t

M a t e r i a l S a f e t y D a t a S h e e t Page 1 of 5 SECTION #1 PRODUCT AND COMPANY IDENTIFICATION Product: Phoenix Brands Consumer Service Telephone Number: 1-866-794-0800 2855 N. Franklin Rd., #7 Emergency Contact: PROSAR IPC Indianapolis,

More information

Slide 1. Slide 2. Slide 3 What do YOU know about oxygen? Dissolved Oxygen. Oxygen. I can t breath in the water but the fish can!

Slide 1. Slide 2. Slide 3 What do YOU know about oxygen? Dissolved Oxygen. Oxygen. I can t breath in the water but the fish can! Slide 1 Dissolved Oxygen I can t breath in the water but the fish can! Slide 2 Oxygen Oxygen is one of the fundamental resources required by life forms on Earth. Aquatic ecosystems have a wide assortment

More information

9/28/2017 OBJ: SWBAT determine the solubility of 10 compounds. 1. What makes Magic Sand hydrophobic?

9/28/2017 OBJ: SWBAT determine the solubility of 10 compounds. 1. What makes Magic Sand hydrophobic? 9/28/2017 OBJ: SWBAT determine the solubility of 10 compounds 1. What makes Magic Sand hydrophobic? Solutions Pure Substances & Mixtures o What's the matter? o Pure Substances have a definite set of physical

More information

Rollei ATP DC Entwickler

Rollei ATP DC Entwickler Page: 1/1 1. Substance/ Indications for Preparation and Producer/ Distributor a) Product Details: Trade name: Rollei ATP DC Developer b) Producer and Distributor: Producer: Distributor: SPUR, Dipl.-Ing

More information

SAFETY DATA SHEET 1. PRODUCT AND COMPANY IDENTIFICATION. Manufacturer LANCO MFG.CORP. URB. APONTE # 5

SAFETY DATA SHEET 1. PRODUCT AND COMPANY IDENTIFICATION. Manufacturer LANCO MFG.CORP. URB. APONTE # 5 SAFETY DATA SHEET DATE PRINTED 5/19/2016 SDS REF. No : DE-716 1. PRODUCT AND COMPANY IDENTIFICATION Product Name: Product Code: DUREX SUPER WHITE DE-716 Manufacturer LANCO MFG.CORP. URB. APONTE # 5 SAN

More information

ULTRA GRO, LLC MATERIAL SAFETY DATA SHEET. Emergency Phone: (559) CHEMTREC: (800) MSDS Reference: ULTRA GRO, LLC (Rev.

ULTRA GRO, LLC MATERIAL SAFETY DATA SHEET. Emergency Phone: (559) CHEMTREC: (800) MSDS Reference: ULTRA GRO, LLC (Rev. ULTRA GRO, LLC MATERIAL SAFETY DATA SHEET Emergency Phone: (559) 661-0977 CHEMTREC: (800) 424-9300 MSDS Reference: ULTRA GRO, LLC (Rev. 12-16-08) SECTION I - IDENTIFICATION ** WARNING - MAY CAUSE EYE IRRITATION!!

More information

MATERIAL SAFETY DATA SHEET

MATERIAL SAFETY DATA SHEET Product name: ETHYLENEIMINE Page : 1 of 6 1 IDENTIFICATION OF THE SUBSTANCE Commercial tradename Application Manufacturer : ETHYLENEIMINE : Intermediate for a broad spectrum of industry, adhesives, coatings,

More information

Chemistry Promo 119W 800 766 5676 www.wilkem.com Free Shipping Solvents List Price Promo Price 190764-4X4L 2-PROPANOL, >=99.5%, A.C.S. REAGENT $ 497.00 $ 148.20 190764-18L-CS 2-PROPANOL, >=99.5%, A.C.S.

More information

DIAMOND CLEANER POWDER

DIAMOND CLEANER POWDER Material Safety Data Sheet DIAMOND CLEANER POWDER Section 1: Chemical Product and Company Identification Trade name: Product type and use: Supplier: Diamond Cleaner Low reactive powder for diamonds Emergency

More information

Laboratory Standard Operating Procedure: Sensitizers

Laboratory Standard Operating Procedure: Sensitizers I. CONTACT INFORMATION Procedure Title Procedure Author Date of Creation/Revision: April 12, 2013 Name of Responsible Person Location of Procedure (The PI, Lab Supervisor, or Autonomous Researcher) (Building

More information

MATERIAL SAFETY DATA SHEET - MSDS Quality Assurance Code:

MATERIAL SAFETY DATA SHEET - MSDS Quality Assurance Code: DENATONIUM BENZOATE Rev.: 02 07.14.06 Page 1 de 5 1. IDENTIFICATION of the SUBSTANCE and of the COMPANY Substance: DENATONIUM BENZOATE Company: NORTEC QUÍMICA S.A. Rua Dezessete, 200-25250-000 Xerém. Distrito

More information

R: The Ideal Gas Constant Pre-Lab Assignment

R: The Ideal Gas Constant Pre-Lab Assignment R: The Ideal Gas Constant Pre-Lab Assignment Read the entire laboratory investigation and the relevant pages in your textbook, then answers the questions that follow in the space provided below. 1 Describe

More information

1 Identification of the substance/preparation and of the company/undertaking

1 Identification of the substance/preparation and of the company/undertaking EC Safety data sheet page 1 from 5 1 Identification of the substance/preparation and of the company/undertaking 1.1 Identification of the substance or preparation: Crystaljelly Metallic Colours e-2185

More information

MATERIAL SAFETY DATA SHEET

MATERIAL SAFETY DATA SHEET MATERIAL SAFETY DATA SHEET 1. Product Identification Magnesium Chloride, Hexahydrate Synonyms: Magnesium chloride; Magnesium chloride, 6-hydrate, crystal CAS No.: 7791-18-6 Molecular Weight: 203.30 Chemical

More information

Testosterone Enanthate (Cas No ) Specification USP/BP. testosterone enanthate. Raw Material / Chemicals Index. Taj Pharmaceuticals Ltd.

Testosterone Enanthate (Cas No ) Specification USP/BP. testosterone enanthate. Raw Material / Chemicals Index. Taj Pharmaceuticals Ltd. Testosterone Enanthate (Cas No 315-37-7) Specification USP/BP Taj Active Pharmaceuticals Ingredients TAJCPG-DCYHEAPAZQ www.tajapi.com Raw Material / Chemicals Index Taj Pharmaceuticals Ltd. Testosterone

More information

MATERIAL SAFETY DATA SHEET

MATERIAL SAFETY DATA SHEET Purafil Select Media MSDS Page 1 of 5 MATERIAL SAFETY DATA SHEET 1. IDENTIFICATION OF THE PREPARATION AND OF THE COMPANY Product Identification: Purafil Select Media Product Synonyms: Purafil Select Chemisorbant

More information

NEODYMIUM SAFETY DATA SHEET DATE OF LAST REVISION: 06/30/15. Section 1: Identification

NEODYMIUM SAFETY DATA SHEET DATE OF LAST REVISION: 06/30/15. Section 1: Identification Section 1: Identification DATE OF LAST REVISION: 06/30/15 Product Name: Neodymium CAS Number: 7440-00-8 / EC Number: 231-109-3 Company: Angstrom Sciences, Inc. 40 South Linden Street Duquesne, PA 15110

More information

Motor Oil SAE 10W Safety Data Sheet 1. IDENTIFICATION OF THE SUBSTANCE/PREPARATION AND OF THE COMPANY/UNDERTAKING

Motor Oil SAE 10W Safety Data Sheet 1. IDENTIFICATION OF THE SUBSTANCE/PREPARATION AND OF THE COMPANY/UNDERTAKING Safety Data Sheet 1. IDENTIFICATION OF THE SUBSTANCE/PREPARATION AND OF THE COMPANY/UNDERTAKING 1.1 Identification of the substance or preparation Motor Oil SAE 10W 1.2 Relevant identified uses of the

More information

GAS LAW WORKSHEET 1 KEY

GAS LAW WORKSHEET 1 KEY 377 GAS LAW WORKSHEET 1 KEY 1. A sample of oxygen gas occupies a volume of 436. ml at 1.0 atm. If the temperature is held constant, what would the pressure of this gas be when the gas is compressed to

More information

Material Safety Data Sheet

Material Safety Data Sheet 1. SUBSTANCE IDENTITY AND COMPANY INFORMATION PRODUCT NAME: CATALOG #: Human Bone Marrow Mesenchymal Stem Cells BMMSC001C, BMMSC002C COMPANY INFORMATION: StemExpress 1743 Creekside Drive, Suite 200 Folsom,

More information

Noxious Fumes and Gases

Noxious Fumes and Gases Noxious Fumes and Gases The tissues of the body require oxygen 0 2 for normal metabolic processes (ie. the oxidation of food to produce energy). They must also eliminate CO, which is the waste product

More information

MATERIAL SAFETY DATA SHEET

MATERIAL SAFETY DATA SHEET 1. IDENTIFICATION CATALOG NO. Detector AP Chemiluminescent Blotting Kit 54-30-01, 54-30-02 Issue Date:21 March, 2006 Revision Date: 21 January, 2004 Reagents That Contain Hazardous Materials Catalog No.

More information

Name:. Correct Questions = Wrong Questions =.. Unattempt Questions = Marks =

Name:. Correct Questions = Wrong Questions =.. Unattempt Questions = Marks = Name:. Correct Questions = Wrong Questions =.. Unattempt Questions = Marks = Lab Problem 1 One way of using solar energy is to capture heat from the sun in a reservoir to be released later. You have been

More information

Date Printed: 06/09/2006 Date Updated: 01/27/2006 Version 1.5 PHOSPHATE BUFFERED SALINE, PH 7.4, TRU- MEASURE CHEMICAL

Date Printed: 06/09/2006 Date Updated: 01/27/2006 Version 1.5 PHOSPHATE BUFFERED SALINE, PH 7.4, TRU- MEASURE CHEMICAL SIGMA-ALDRICH MATERIAL SAFETY DATA SHEET Date Printed: 06/09/2006 Date Updated: 01/27/2006 Version 1.5 Section 1 - Product and Company Information Product Name Product Number Brand PHOSPHATE BUFFERED SALINE,

More information

SAFETY DATA SHEET. Thermal Poly 32 Floor Finish. 1. Product and Company Identification. 2. Hazards Identification

SAFETY DATA SHEET. Thermal Poly 32 Floor Finish. 1. Product and Company Identification. 2. Hazards Identification Product Code: Product Name: Company Name: Web site address: 993 Genlabs 5568 Schaefer Ave. Chino, CA 9171 1. Product and Company Identification www.genlabscorp.com Phone Number: 1 (99)591-8451 Emergency

More information