Water Sediment Tissue Analyte Method MDL RL MDL RL MDL RL Carbazole SOP (GC/MS) cis Decalin SOP 5 157

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1 Carbazole SOP (GC/MS) cis Decalin SOP (GC/MS) trans Decalin SOP (GC/MS) Benzo(b)thiophene SOP (GC/MS) ,4 Dichlorobenzene SOP (GC/MS) Naphthalene SOP (GC/MS) Chloronaphthalene SOP (GC/MS) Methylnaphthalene SOP (GC/MS) Methylnaphthalene SOP (GC/MS) ,6 dimethylnaphthalene SOP (GC/MS) ,3,5 trimethylnaphthalene SOP (GC/MS) Biphenyl SOP (GC/MS) Acenaphthylene SOP (GC/MS) Acenaphthene SOP (GC/MS) Dibenzofuran SOP (GC/MS) Fluorene SOP (GC/MS) Anthracene SOP (GC/MS) Phenanthrene SOP (GC/MS) Methylphenanthrene SOP (GC/MS) Methylphenanthrene SOP (GC/MS) Dibenzothiophene SOP (GC/MS) Fluoranthene SOP (GC/MS) Pyrene SOP (GC/MS) Benzo(a)anthracene SOP (GC/MS) Chrysene SOP (GC/MS) Benzo(b)fluoranthene SOP (GC/MS) Benzo(k)fluoranthene SOP (GC/MS) Benzo(e)pyrene SOP (GC/MS) Benzo(a)pyrene SOP (GC/MS) Perylene SOP (GC/MS) Indeno(1,2,3 cd)pyrene SOP (GC/MS) Dibenz(a,h)anthracene SOP (GC/MS) Benzo(g,h,i)perylene SOP (GC/MS) Isophorone SOP (GC/MS) Retene SOP (GC/MS) Benzo(b)naphtho(2,1 d)thiophene SOP (GC/MS) Cholestane SOP (GC/MS)

2 n Octane (GC/FID) n Nonane (GC/FID) n Decane (GC/FID) n Undecane (GC/FID) n Dodecane (GC/FID) n Tridecane (GC/FID) Isoprenoid RRT (GC/FID) n Tetradecane (GC/FID) Isoprenoid RRT (GC/FID) n Pentadecane (GC/FID) n Hexadecane (GC/FID) Norpristane (1650) (GC/FID) n Heptadecane (GC/FID) Pristane (GC/FID) n Octadecane (GC/FID) Phytane (GC/FID) n Nonadecane (GC/FID) n Eicosane (GC/FID) n Heneicosane (GC/FID) n Docosane (GC/FID) n Tricosane (GC/FID) n Tetracosane (GC/FID) n Pentacosane (GC/FID) n Hexacosane (GC/FID) n Heptacosane (GC/FID) n Octacosane (GC/FID) n Nonacosane (GC/FID) n Triacontane (GC/FID) n Hentriacontane (GC/FID) n Dotriacontane (GC/FID) n Tritriacontane (GC/FID) n Tetratriacontane (GC/FID) n Pentatriacontane (GC/FID) n Hexatriacontane (GC/FID) n Heptatriacontane (GC/FID) n Octatriacontane (GC/FID) n Nonatriacontane (GC/FID)

3 n Tetracontane (GC/FID) TPH (GC/FID) NA NA NA n Pentane SOP (GC/MS) NA NA n Hexane SOP (GC/MS) NA NA n Heptane SOP (GC/MS) NA NA n Octane SOP (GC/MS) NA NA n Nonane SOP (GC/MS) NA NA n Decane SOP (GC/MS) NA NA n Undecane SOP (GC/MS) NA NA Isopentane SOP (GC/MS) NA NA 2,2 Dimethylbutane SOP (GC/MS) NA NA 2,3 Dimethylbutane SOP (GC/MS) NA NA 2 Methylpentane SOP (GC/MS) NA NA 3 Methylpentane SOP (GC/MS) NA NA 2,2 Dimethylpentane SOP (GC/MS) NA NA 2,4 Dimethylpentane SOP (GC/MS) NA NA 2,2,3 trimethylbutane SOP (GC/MS) NA NA 3,3 dimethylpentane SOP (GC/MS) NA NA 2 Methylhexane SOP (GC/MS) NA NA 2,3 Dimethylpentane SOP (GC/MS) NA NA 3 Methylhexane SOP (GC/MS) NA NA 3 ethylpentane SOP (GC/MS) NA NA 2,2,4 Trimethylpentane/1 heptene SOP (GC/MS) NA NA 2,2 dimethylhexane SOP (GC/MS) NA NA 2,5 Dimethylhexane/2,2,3 trimethylpentane SOP (GC/MS) NA NA 2,4 Dimethylhexane SOP (GC/MS) NA NA 2,3,4 Trimethylpentane SOP (GC/MS) NA NA 2,3,3 Trimethylpentane SOP (GC/MS) NA NA 2,3 Dimethylhexane SOP (GC/MS) NA NA 2 Methylheptane SOP (GC/MS) NA NA 4 Methylheptane SOP (GC/MS) NA NA 3 Methylheptane SOP (GC/MS) NA NA 3 ethylhexane SOP (GC/MS) NA NA 2,2 Dimethylheptane SOP (GC/MS) NA NA 2,2,4 Trimethylhexane SOP (GC/MS) NA NA 2,4 Dimethylheptane SOP (GC/MS) NA NA 2,6 Dimethylheptane SOP (GC/MS) NA NA

4 2,5 dimethylheptane SOP (GC/MS) NA NA 3,3 dimethylheptane/3,5 dimethylheptane SOP (GC/MS) NA NA 2,3 Dimethylheptane SOP (GC/MS) NA NA 3,4 Dimethylheptane (D) SOP (GC/MS) NA NA 3,4 Dimethylheptane (L) SOP (GC/MS) NA NA 4 Methyloctane SOP (GC/MS) NA NA 2 Methyloctane SOP (GC/MS) NA NA 3 Methyloctane SOP (GC/MS) NA NA 3,3 Diethylpentane SOP (GC/MS) NA NA 2,2 Dimethyloctane SOP (GC/MS) NA NA 3,3 Dimethyloctane SOP (GC/MS) NA NA 2,3 Dimethyloctane SOP (GC/MS) NA NA 2 methylnonane SOP (GC/MS) NA NA 3 ethyloctane SOP (GC/MS) NA NA 3 Methylnonane SOP (GC/MS) NA NA Benzene SOP (GC/MS) NA NA Toluene SOP (GC/MS) NA NA Ethylbenzene SOP (GC/MS) NA NA m Xylene SOP (GC/MS) NA NA p Xylene SOP (GC/MS) NA NA o Xylene SOP (GC/MS) NA NA Isopropylbenzene SOP (GC/MS) NA NA Propylbenzene SOP (GC/MS) NA NA 1 Methyl 3 Ethylbenzene SOP (GC/MS) NA NA 1 Methyl 4 Ethylbenzene SOP (GC/MS) NA NA 1,3,5 Trimethylbenzene SOP (GC/MS) NA NA 1 Methyl 2 Ethylbenzene SOP (GC/MS) NA NA tert butylbenzene SOP (GC/MS) NA NA 1,2,4 Trimethylbenzene SOP (GC/MS) NA NA isobutylbenzene SOP (GC/MS) NA NA sec Butylbenzene SOP (GC/MS) NA NA m cymene SOP (GC/MS) NA NA 1,2,3 Trimethylbenzene SOP (GC/MS) NA NA p Cymene SOP (GC/MS) NA NA Indane SOP (GC/MS) NA NA o cymene SOP (GC/MS) NA NA 1,3 Diethylbenzene SOP (GC/MS) NA NA

5 1 methyl 3 n propylbenzene SOP (GC/MS) NA NA 1 methyl 4 n propylbenzene/1,4 Diethylbenzene SOP (GC/MS) NA NA butyl benzene SOP (GC/MS) NA NA 1,3 Dimethyl 5 Ethylbenzene SOP (GC/MS) NA NA 1,2 Diethylbenzene SOP (GC/MS) NA NA 1 Methyl 2 n Propylbenzene SOP (GC/MS) NA NA 1,4 dimethyl 2 ethylbenzene SOP (GC/MS) NA NA 1 ethyl 2,4 dimethylbenzene SOP (GC/MS) NA NA 1,2 Dimethyl 4 Ethylbenzene SOP (GC/MS) NA NA 1,3 Dimethyl 2 Ethylbenzene SOP (GC/MS) NA NA 1,2 dimethyl 3 ethylbenzene SOP (GC/MS) NA NA 1,2,4,5 Tetramethylbenzene SOP (GC/MS) NA NA 2 methylbutylbenzene SOP (GC/MS) NA NA 1,2,3,5 Tetramethylbenzene SOP (GC/MS) NA NA 1,2,3,4 Tetramethylbenzene SOP (GC/MS) NA NA n Pentylbenzene SOP (GC/MS) NA NA tert 1 butyl 3,5 dimethylbenzene SOP (GC/MS) NA NA tert 1 butyl 4 ethylbenzene SOP (GC/MS) NA NA 1,3,5 triethylbenzene SOP (GC/MS) NA NA 1,2,4 triethylbenzene SOP (GC/MS) NA NA n hexylbenzene SOP (GC/MS) NA NA Cyclopentane SOP (GC/MS) NA NA Methylcyclopentane SOP (GC/MS) NA NA Cyclohexane SOP (GC/MS) NA NA 1,1 dimethylcyclopentane SOP (GC/MS) NA NA Methylcyclohexane SOP (GC/MS) NA NA ethylcyclopentane SOP (GC/MS) NA NA ctc 1,2,4 Trimethylcyclopentane SOP (GC/MS) NA NA ctc 1,2,3 Trimethylcyclopentane SOP (GC/MS) NA NA ctt 1,2,4 Trimethylcyclopentane SOP (GC/MS) NA NA trans 1,4 dimethylcyclohexane SOP (GC/MS) NA NA 1 ethyl 1 methylcyclopentane SOP (GC/MS) NA NA trans 1,2 dimethylcyclohexane SOP (GC/MS) NA NA ccc 1,2,3 trimethylcyclopentane SOP (GC/MS) NA NA Isopropylcyclopentane SOP (GC/MS) NA NA cis 1,2 dimethylcyclohexane SOP (GC/MS) NA NA Ethylcyclohexane/n propylcyclopentane SOP (GC/MS) NA NA

6 ccc 1,3,5 trimethylcyclohexane SOP (GC/MS) NA NA 1,1,4 Trimethylcyclohexane SOP (GC/MS) NA NA ctt 1,2,4 Trimethylcyclohexane SOP (GC/MS) NA NA ctc 1,2,4 Trimethylcyclohexane SOP (GC/MS) NA NA 1,1,2 Trimethylcyclohexane SOP (GC/MS) NA NA isobutylcyclopentane SOP (GC/MS) NA NA Isopropylcyclohexane SOP (GC/MS) NA NA n Butylcyclopentane SOP (GC/MS) NA NA isobutylcyclohexane SOP (GC/MS) NA NA tert 1 methyl 2 propylcyclohexane SOP (GC/MS) NA NA tert 1 methyl 2 (4MP)cyclopentane SOP (GC/MS) NA NA 3 methyl 1 butene SOP (GC/MS) NA NA 1 Pentene SOP (GC/MS) NA NA 2 Methyl 1 Butene SOP (GC/MS) NA NA 2 methyl 1,3 butadiene SOP (GC/MS) NA NA trans 2 Pentene SOP (GC/MS) NA NA cis 2 Pentene SOP (GC/MS) NA NA 4 methylpentene 1 SOP (GC/MS) NA NA 1 Hexene SOP (GC/MS) NA NA trans 2 Hexene SOP (GC/MS) NA NA 2 Methylpentene 2 SOP (GC/MS) NA NA cis 2 Hexene SOP (GC/MS) NA NA 2 Methyl 1 Hexene/trans 1,2 dimethylcyclopentane SOP (GC/MS) NA NA trans 3 Heptene SOP (GC/MS) NA NA cis 3 Heptene SOP (GC/MS) NA NA trans 2 Heptene SOP (GC/MS) NA NA cis 2 Heptene SOP (GC/MS) NA NA 1 Octene SOP (GC/MS) NA NA trans 2 Octene SOP (GC/MS) NA NA Cis 2 octene SOP (GC/MS) NA NA 1 Nonene SOP (GC/MS) NA NA trans 3 Nonene SOP (GC/MS) NA NA cis 3 Nonene SOP (GC/MS) NA NA trans 2 Nonene SOP (GC/MS) NA NA cis 2 Nonene SOP (GC/MS) NA NA 1 Decene SOP (GC/MS) NA NA 1,2 Dichloroethane SOP (GC/MS) NA NA

7 1,2 Dibromoethane SOP (GC/MS) NA NA Methyl tert butyl ether SOP (GC/MS) NA NA Di isopropyl ether SOP (GC/MS) NA NA Ethyl tert butyl ether SOP (GC/MS) NA NA Tert amyl methyl ether SOP (GC/MS) NA NA 1,2 Dichloroethylene (trans) SOP (GC/MS) NA NA 1,2 Dichloroethylene (cis) SOP (GC/MS) NA NA 1,1,1 Trichloroethane SOP (GC/MS) NA NA Trichloroethylene SOP (GC/MS) NA NA Tetrachloroethylene SOP (GC/MS) NA NA Styrene SOP (GC/MS) NA NA Thiophene SOP (GC/MS) NA NA 2 Methylthiophene SOP (GC/MS) NA NA 3 Methylthiophene SOP (GC/MS) NA NA 2 Ethylthiophene SOP (GC/MS) NA NA Benzo(b)thiophene SOP (GC/MS) NA NA Naphthalene SOP (GC/MS) NA NA ethanol SOP (GC/MS) NA NA t Butanol SOP (GC/MS) NA NA MMT SOP (GC/MS) NA NA n Dodecane SOP (GC/MS) NA NA 2,4' DDD SOP (GC/ECD) ,4' DDE SOP (GC/ECD) ,4' DDT SOP (GC/ECD) ,4' DDD SOP (GC/ECD) ,4' DDE SOP (GC/ECD) ,4' DDT SOP (GC/ECD) ,4' DDMU SOP (GC/ECD) aldrin SOP (GC/ECD) a chlordane SOP (GC/ECD) g chlordane SOP (GC/ECD) a BHC SOP (GC/ECD) b BHC SOP (GC/ECD) d BHC SOP (GC/ECD) Lindane SOP (GC/ECD) cis nonachlor SOP (GC/ECD) trans nonachlor SOP (GC/ECD)

8 Chlorpyrifos SOP (GC/ECD) oxychlordane SOP (GC/ECD) dieldrin SOP (GC/ECD) endosulfan I SOP (GC/ECD) endosulfan II SOP (GC/ECD) endosulfan sulfate SOP (GC/ECD) endrin SOP (GC/ECD) endrin aldehyde SOP (GC/ECD) endrin ketone SOP (GC/ECD) heptachlor SOP (GC/ECD) heptachlor epoxide SOP (GC/ECD) Hexachlorobenzene SOP (GC/ECD) methoxychlor SOP (GC/ECD) Mirex SOP (GC/ECD) Cl2(8) SOP (GC/ECD) Cl3(18) SOP (GC/ECD) Cl3(28) SOP (GC/ECD) Cl4(44) SOP (GC/ECD) Cl4(49) SOP (GC/ECD) Cl4(52) SOP (GC/ECD) Cl4(66) SOP (GC/ECD) Cl4(77) SOP (GC/ECD) Cl5(87) SOP (GC/ECD) Cl5(101) SOP (GC/ECD) Cl5(105) SOP (GC/ECD) Cl5(110) SOP (GC/ECD) Cl5(118) SOP (GC/ECD) Cl5(126) SOP (GC/ECD) Cl6(128) SOP (GC/ECD) Cl6(129) SOP (GC/ECD) Cl6(138) SOP (GC/ECD) Cl6(153) SOP (GC/ECD) Cl6(169) SOP (GC/ECD) Cl7(170) SOP (GC/ECD) Cl7(180) SOP (GC/ECD) Cl7(183) SOP (GC/ECD) Cl7(184) SOP (GC/ECD)

9 Cl7(187) SOP (GC/ECD) Cl8(195) SOP (GC/ECD) Cl9(206) SOP (GC/ECD) Cl10(209) SOP (GC/ECD) ,4' DDMU SOP (GC/MS) ,4' DDE SOP (GC/MS) ,4' DDE SOP (GC/MS) ,4' DDD SOP (GC/MS) ,4' DDD SOP (GC/MS) ,4' DDT SOP (GC/MS) ,4' DDT SOP (GC/MS) Biphenyl SOP (GC/MS) Cl1(1) SOP (GC/MS) Cl1(3) SOP (GC/MS) Cl2(4) SOP (GC/MS) Cl2(5) SOP (GC/MS) Cl2(6) SOP (GC/MS) Cl2(7) SOP (GC/MS) Cl2(8) SOP (GC/MS) Cl2(9) SOP (GC/MS) Cl2(11) SOP (GC/MS) Cl2(12) SOP (GC/MS) Cl2(13) SOP (GC/MS) Cl2(15) SOP (GC/MS) Cl3(16) SOP (GC/MS) Cl3(17) SOP (GC/MS) Cl3(18) SOP (GC/MS) Cl3(19) SOP (GC/MS) Cl3(22) SOP (GC/MS) Cl3(24) SOP (GC/MS) Cl3(25) SOP (GC/MS) Cl3(26) SOP (GC/MS) Cl3(27) SOP (GC/MS) Cl3(28) SOP (GC/MS) Cl3(29) SOP (GC/MS) Cl3(30) SOP (GC/MS) Cl3(31) SOP (GC/MS)

10 Cl3(32) SOP (GC/MS) Cl3(33) SOP (GC/MS) Cl3(37) SOP (GC/MS) Cl4(40) SOP (GC/MS) Cl4(41) SOP (GC/MS) Cl4(42) SOP (GC/MS) Cl4(43) SOP (GC/MS) Cl4(44) SOP (GC/MS) Cl4(45) SOP (GC/MS) Cl4(46) SOP (GC/MS) Cl4(47) SOP (GC/MS) Cl4(48) SOP (GC/MS) Cl4(49) SOP (GC/MS) Cl4(50) SOP (GC/MS) Cl4(51) SOP (GC/MS) Cl4(52) SOP (GC/MS) Cl4(53) SOP (GC/MS) Cl4(54) SOP (GC/MS) Cl4(56) SOP (GC/MS) Cl4(60) SOP (GC/MS) Cl4(63) SOP (GC/MS) Cl4(64) SOP (GC/MS) Cl4(66) SOP (GC/MS) Cl4(67) SOP (GC/MS) Cl4(70) SOP (GC/MS) Cl4(71) SOP (GC/MS) Cl4(74) SOP (GC/MS) Cl4(75) SOP (GC/MS) Cl4(77) SOP (GC/MS) Cl4(80) SOP (GC/MS) Cl4(81) SOP (GC/MS) Cl5(82) SOP (GC/MS) Cl5(83) SOP (GC/MS) Cl5(84) SOP (GC/MS) Cl5(85) SOP (GC/MS) Cl5(87) SOP (GC/MS) Cl5(91) SOP (GC/MS)

11 Cl5(92) SOP (GC/MS) Cl5(95) SOP (GC/MS) Cl5(97) SOP (GC/MS) Cl5(99) SOP (GC/MS) Cl5(100) SOP (GC/MS) Cl5(101) SOP (GC/MS) Cl5(104) SOP (GC/MS) Cl5(105) SOP (GC/MS) Cl5(110) SOP (GC/MS) Cl5(114) SOP (GC/MS) Cl5(115) SOP (GC/MS) Cl5(118) SOP (GC/MS) Cl5(123) SOP (GC/MS) Cl5(124) SOP (GC/MS) Cl5(125) SOP (GC/MS) Cl5(126) SOP (GC/MS) Cl5(127) SOP (GC/MS) Cl6(128) SOP (GC/MS) Cl6(130) SOP (GC/MS) Cl6(131) SOP (GC/MS) Cl6(134) SOP (GC/MS) Cl6(135) SOP (GC/MS) Cl6(136) SOP (GC/MS) Cl6(137) SOP (GC/MS) Cl6(138) SOP (GC/MS) Cl6(139) SOP (GC/MS) Cl6(140) SOP (GC/MS) Cl6(141) SOP (GC/MS) Cl6(144) SOP (GC/MS) Cl6(146) SOP (GC/MS) Cl6(149) SOP (GC/MS) Cl6(151) SOP (GC/MS) Cl6(153) SOP (GC/MS) Cl6(154) SOP (GC/MS) Cl6(155) SOP (GC/MS) Cl6(156) SOP (GC/MS) Cl6(157) SOP (GC/MS)

12 Cl6(158) SOP (GC/MS) Cl6(163) SOP (GC/MS) Cl6(164) SOP (GC/MS) Cl6(166) SOP (GC/MS) Cl6(167) SOP (GC/MS) Cl6(169) SOP (GC/MS) Cl7(170) SOP (GC/MS) Cl7(171) SOP (GC/MS) Cl7(172) SOP (GC/MS) Cl7(173) SOP (GC/MS) Cl7(174) SOP (GC/MS) Cl7(175) SOP (GC/MS) Cl7(176) SOP (GC/MS) Cl7(177) SOP (GC/MS) Cl7(178) SOP (GC/MS) Cl7(179) SOP (GC/MS) Cl7(180) SOP (GC/MS) Cl7(183) SOP (GC/MS) Cl7(184) SOP (GC/MS) Cl7(185) SOP (GC/MS) Cl7(187) SOP (GC/MS) Cl7(188) SOP (GC/MS) Cl7(189) SOP (GC/MS) Cl7(190) SOP (GC/MS) Cl7(191) SOP (GC/MS) Cl7(193) SOP (GC/MS) Cl8(194) SOP (GC/MS) Cl8(195) SOP (GC/MS) Cl8(197) SOP (GC/MS) Cl8(198) SOP (GC/MS) Cl8(199) SOP (GC/MS) Cl8(200) SOP (GC/MS) Cl8(201) SOP (GC/MS) Cl8(202) SOP (GC/MS) Cl8(203) SOP (GC/MS) Cl8(205) SOP (GC/MS) Cl9(206) SOP (GC/MS)

13 Cl9(207) SOP (GC/MS) Cl9(208) SOP (GC/MS) Cl10(209) SOP (GC/MS)

Fish were collected in April September 2013 by the Fisheries and Wildlife Division staff at DOEE.

Fish were collected in April September 2013 by the Fisheries and Wildlife Division staff at DOEE. US EPA Guidance for Assessing Chemical Contaminant Data for Use in Fish Advisories Volume 1: Fish Sampling