River Water Intake Collected: 20 June WW Loading Collected: 20 June 2018

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Crystal Anthony
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1 Analyte CAS No Unit 537 (modified) PFAS HFPO DA µg/l ,600 2,900 1,300 F1 J Table 3 SOP PEPA N/A µg/l <0.10 H <1000 H <1000 H <1000 Table 3 SOP PFECA G µg/l <0.096 H <960 H <960 H <960 Table 3 SOP PFESA BP µg/l <0.12 H <1200 H 53,350 H 26,000 Table 3 SOP PFESA BP µg/l <0.095 H 5,345 H 4,700 H 2,500 Table 3 SOP PFMOAA µg/l <0.095 H 763,500 H 960,000 H 810,000 Table 3 SOP PFO2HxA µg/l <0.092 H 207,500 H 290,000 H 233,500 Table 3 SOP PFO3OA µg/l <0.088 H 67,150 H 97,150 H 81,000 Table 3 SOP PFO4DA µg/l <0.097 H 16,550 H 27,000 H F1 18,200 Table 3 SOP PMPA µg/l <0.084 H 1,330 J H J 2,105 H 1,805 J J Table 3 SOP TAF µg/l <0.11 H 4,635 H 5,600 H 4, (modified) PFAS 4:2 FTS µg/l <0.020 <50 <52 < (modified) PFAS 6:2 FTS µg/l <0.020 <0.19 <0.20 < (modified) PFAS 8:2 FTS µg/l <0.020 <19 <20 < (modified) PFAS ADONA µg/l < <0.018 <0.019 < (modified) PFAS F 53B N/A µg/l < <0.031 <0.032 F1 <0.031 F1 537 (modified) PFAS F 53B Major µg/l < <0.023 F1 <0.024 < (modified) PFAS F 53B Minor µg/l < <0.031 <0.032 F1 <0.031 F1 537 (modified) PFAS NaDONA N/A µg/l < <0.018 <0.019 < (modified) PFAS N ethyl perfluorooctane sulfonamidoacetic acid (NEtFOSAA) µg/l <0.020 <0.18 <0.19 < (modified) PFAS N methyl perfluorooctane sulfonamidoacetic acid (NMeFOSAA) N/A µg/l <0.020 <0.30 <0.31 < (modified) PFAS Perfluorobutanesulfonic acid (PFBS) µg/l <1.9 < J 537 (modified) PFAS Perfluorobutanoic acid (PFBA) µg/l <3.4 <3.5 < (modified) PFAS Perfluorodecanesulfonic acid (PFDS) µg/l < <0.031 <0.032 <0.031 F1 537 (modified) PFAS Perfluorodecanoic acid (PFDA) µg/l < F F1 <0.030 F1 537 (modified) PFAS Perfluorododecanoic acid (PFDoA) µg/l < <0.053 <0.055 < (modified) PFAS Perfluoroheptanesulfonic Acid (PFHpS) µg/l < <0.018 F1 <0.019 F1 <0.019 F1 537 (modified) PFAS Perfluoroheptanoic acid (PFHpA) µg/l (modified) PFAS Perfluorohexanesulfonic acid (PFHxS) µg/l <0.016 F1 <0.017 F1 <0.017 F1 537 (modified) PFAS Perfluorohexanoic acid (PFHxA) µg/l (modified) PFAS Perfluoro n hexadecanoic acid (PFHxDA) µg/l < <0.086 <0.088 < (modified) PFAS Perfluoro n octadecanoic acid (PFODA) µg/l < <0.045 <0.046 < (modified) PFAS Perfluorononanesulfonic acid (PFNS) µg/l < <0.016 F1 <0.016 F1 <0.016 F1 537 (modified) PFAS Perfluorononanoic acid (PFNA) µg/l < (modified) PFAS Perfluorooctane Sulfonamide (FOSA) µg/l < <0.034 F1 <0.035 <0.034 F1 537 (modified) PFAS Perfluorooctanesulfonic acid (PFOS) µg/l <0.052 <0.054 < (modified) PFAS Perfluorooctanoic acid (PFOA) µg/l (modified) PFAS Perfluoropentanesulfonic acid (PFPeS) µg/l < <2.9 <3.0 < (modified) PFAS Perfluoropentanoic acid (PFPeA) µg/l (modified) PFAS Perfluorotetradecanoic acid (PFTeA) µg/l < <0.028 F1 <0.029 F1 <0.028 F1 537 (modified) PFAS Perfluorotridecanoic Acid (PFTriA) µg/l < <0.13 <0.13 < (modified) PFAS Perfluoroundecanoic acid (PFUnA) µg/l <

2 Analyte CAS No Unit Rev 4.4 Metals (ICP) Aluminum µg/l 340 J 480 NV Rev 4.4 Metals (ICP) Antimony µg/l <5.2 <26 NV Rev 4.4 Metals (ICP) Arsenic µg/l <4.4 <22 NV Rev 4.4 Metals (ICP) Barium µg/l NV Rev 4.4 Metals (ICP) Beryllium µg/l <0.47 <0.47 NV Rev 4.4 Metals (ICP) Boron µg/l 29 J J 50 J NV Rev 4.4 Metals (ICP) Cadmium µg/l <0.45 <2.3 NV Rev 4.4 Metals (ICP) Calcium µg/l 4,600 1,100 NV Rev 4.4 Metals (ICP) Chromium µg/l 0.77 J J 180 NV Rev 4.4 Metals (ICP) Cobalt µg/l 1.2 J J <6.2 NV Rev 4.4 Metals (ICP) Copper µg/l < J NV Rev 4.4 Metals (ICP) Iron µg/l 1,100 1,400 NV Rev 4.4 Metals (ICP) Lead µg/l <2.7 <14 NV Rev 4.4 Metals (ICP) Lithium µg/l < NV Rev 4.4 Metals (ICP) Magnesium µg/l J NV Rev 4.4 Metals (ICP) Manganese µg/l NV Rev 4.4 Metals (ICP) Molybdenum µg/l < J NV Rev 4.4 Metals (ICP) Nickel µg/l < J NV Rev 4.4 Metals (ICP) Phosphorus µg/l 170 J J 3,600 J NV Rev 4.4 Metals (ICP) Potassium µg/l 3,600 8,700,000 NV Rev 4.4 Metals (ICP) Selenium µg/l <6.3 <32 NV Rev 4.4 Metals (ICP) Silicon µg/l 3,200 15,000 NV Rev 4.4 Metals (ICP) Silver µg/l <0.93 <4.7 NV Rev 4.4 Metals (ICP) SiO2, Silica µg/l 6,900 31,000 NV Rev 4.4 Metals (ICP) Sodium µg/l 11,000 B 11,000,000 NV Rev 4.4 Metals (ICP) Strontium µg/l NV Rev 4.4 Metals (ICP) Thallium µg/l <4.9 <25 NV Rev 4.4 Metals (ICP) Thorium µg/l <8.3 <42 NV Rev 4.4 Metals (ICP) Tin µg/l <5.8 <29 NV Rev 4.4 Metals (ICP) Titanium µg/l 5.2 J J 19 J NV Rev 4.4 Metals (ICP) Vanadium µg/l 2.8 J J <5.6 NV Rev 4.4 Metals (ICP) Zinc µg/l < NV Metals, Mercury (CVAA) Mercury µg/l < J F1 NV 7196A Hexavalent Cr (Colorimetric) Chromium, Hexavalent mg/l J UJ 0.01 J H NV Metals, Hexavalent Cr Chromium, Hexavalent µg/l <0.02 UJ 38 J General Chemistry Bromide mg/l < NV General Chemistry Cyanide, Total mg/l J F1 B * ^ B < NV General Chemistry Nitrate as N mg/l J H NV General Chemistry Total Phenols mg/l < NV 6850 Perchlorate Perchlorate µg/l J I J 1.9 J NV

3 Analyte CAS No Unit 624 VOCs (GC/MS) 1,1,1,2 Tetrachloroethane µg/l <0.17 < VOCs (GC/MS) 1,1,1 Trichloroethane µg/l <0.16 < VOCs (GC/MS) 1,1,2,2 Tetrachloroethane µg/l <0.20 < VOCs (GC/MS) 1,1,2 Trichloroethane µg/l <0.32 < VOCs (GC/MS) 1,1 Dichloroethane µg/l <0.16 < VOCs (GC/MS) 1,1 Dichloroethene µg/l <0.14 < VOCs (GC/MS) 1,2,3 Trichloropropane µg/l <0.27 < VOCs (GC/MS) 1,2 Dibromo 3 Chloropropane µg/l <0.81 < VOCs (GC/MS) 1,2 Dichlorobenzene µg/l <0.13 < VOCs (GC/MS) 1,2 Dichloroethane µg/l < J 624 VOCs (GC/MS) 1,2 Dichloroethene, Total µg/l <0.15 < VOCs (GC/MS) 1,2 Dichloropropane µg/l <0.13 < VOCs (GC/MS) 1,3 Dichlorobenzene µg/l <0.16 < VOCs (GC/MS) 1,3 Dichloropropene, Total µg/l <0.16 < VOCs (GC/MS) 1,4 Dichlorobenzene µg/l <0.16 < VOCs (GC/MS) 1,4 Dioxane µg/l <71 < VOCs (GC/MS) 2 Butanone (MEK) µg/l < J J 624 VOCs (GC/MS) 2 Chloroethyl vinyl ether µg/l <0.74 F1 R < VOCs (GC/MS) 2 Hexanone µg/l <1.4 < VOCs (GC/MS) 4 Methyl 2 pentanone (MIBK) µg/l <0.49 < VOCs (GC/MS) Acetone µg/l 4.2 J J 270 E 624 VOCs (GC/MS) Acrolein µg/l <2.8 < VOCs (GC/MS) Acrylonitrile µg/l <1.4 < VOCs (GC/MS) Benzene µg/l <0.16 < VOCs (GC/MS) Bromoform µg/l <0.19 < VOCs (GC/MS) Bromomethane µg/l <0.21 < VOCs (GC/MS) Carbon disulfide µg/l <0.45 < VOCs (GC/MS) Carbon tetrachloride µg/l <0.19 < VOCs (GC/MS) Chlorobenzene µg/l <0.17 < VOCs (GC/MS) Chlorodibromomethane µg/l <0.17 < VOCs (GC/MS) Chloroethane µg/l <0.41 < VOCs (GC/MS) Chloroform µg/l 0.34 J J 3.3 J 624 VOCs (GC/MS) Chloromethane µg/l <0.30 < VOCs (GC/MS) cis 1,2 Dichloroethene µg/l <0.15 < VOCs (GC/MS) cis 1,3 Dichloropropene µg/l <0.16 < VOCs (GC/MS) Dibromomethane µg/l <0.17 < VOCs (GC/MS) Dichlorobromomethane µg/l <0.17 < VOCs (GC/MS) Dichlorodifluoromethane µg/l <0.31 < VOCs (GC/MS) Ethylbenzene µg/l <0.16 < VOCs (GC/MS) Ethylene Dibromide µg/l <0.18 < VOCs (GC/MS) Hexane µg/l <0.42 < VOCs (GC/MS) Methyl tert butyl ether µg/l <0.25 < VOCs (GC/MS) Methylene Chloride µg/l < J 624 VOCs (GC/MS) m Xylene & p Xylene µg/l <0.19 < VOCs (GC/MS) o Xylene µg/l <0.19 < VOCs (GC/MS) Styrene µg/l <0.17 < VOCs (GC/MS) Tetrachloroethene µg/l <0.20 < VOCs (GC/MS) Toluene µg/l < J J 624 VOCs (GC/MS) Total BTEX N/A µg/l < J J 624 VOCs (GC/MS) trans 1,2 Dichloroethene µg/l <0.15 < VOCs (GC/MS) trans 1,3 Dichloropropene µg/l <0.19 < VOCs (GC/MS) Trichloroethene µg/l <0.16 < VOCs (GC/MS) Trichlorofluoromethane µg/l <0.29 < VOCs (GC/MS) Vinyl acetate µg/l <0.94 < VOCs (GC/MS) Vinyl chloride µg/l <0.17 < VOCs (GC/MS) Xylenes, Total µg/l <0.19 <0.19

4 Analyte CAS No Unit 624 VOCs (GC/MS) Tentative Identification: Acetic acid, 2 ethylhexyl ester N/A µg/l 1.7 T J N J 624 VOCs (GC/MS) Tentative Identification: Unknown N/A µg/l 5.4 T J J 624 VOCs (GC/MS) Tentative Identification: Unknown N/A µg/l 2.3 T J J 624 VOCs (GC/MS) Tentative Identification: Unknown N/A µg/l 180 T J J 624 VOCs (GC/MS) Tentative Identification: Unknown N/A µg/l 6.9 T J J 624 VOCs (GC/MS) Tentative Identification: Unknown N/A µg/l 250 T J J 624 VOCs (GC/MS) Tentative Identification: Unknown N/A µg/l 780 T J J 624 VOCs (GC/MS) Tentative Identification: Unknown N/A µg/l 15 T J J 624 VOCs (GC/MS) Tentative Identification: Unknown N/A µg/l 3.6 T J J 625 SVOCs (GC/MS) 1,2,4 Trichlorobenzene µg/l <0.28 <0.27 NV 625 SVOCs (GC/MS) 1,2 Diphenylhydrazine(as Azobenzene) µg/l <0.23 <0.22 NV 625 SVOCs (GC/MS) 2,2' Oxybis(1 chloropropane) µg/l <0.28 <0.27 NV 625 SVOCs (GC/MS) 2,4,6 Trichlorophenol µg/l <0.29 <0.28 NV 625 SVOCs (GC/MS) 2,4 Dichlorophenol µg/l <0.64 <0.61 NV 625 SVOCs (GC/MS) 2,4 Dimethylphenol µg/l <0.58 <0.55 NV 625 SVOCs (GC/MS) 2,4 Dinitrophenol µg/l <10 <9.5 NV 625 SVOCs (GC/MS) 2,4 Dinitrotoluene µg/l <1.7 <1.6 NV 625 SVOCs (GC/MS) 2,6 Dinitrotoluene µg/l <1.9 <1.8 NV 625 SVOCs (GC/MS) 2 Chloronaphthalene µg/l <0.26 <0.25 * NV 625 SVOCs (GC/MS) 2 Chlorophenol µg/l <2.0 <1.9 NV 625 SVOCs (GC/MS) 2 Methylphenol µg/l <0.98 <0.93 NV 625 SVOCs (GC/MS) 2 Nitrophenol µg/l <0.39 <0.37 NV 625 SVOCs (GC/MS) 3 & 4 Methylphenol µg/l <0.80 <0.76 NV 625 SVOCs (GC/MS) 3,3' Dichlorobenzidine µg/l <2.0 <1.9 NV 625 SVOCs (GC/MS) 4,6 Dinitro 2 methylphenol µg/l <4.0 <3.8 NV 625 SVOCs (GC/MS) 4 Bromophenyl phenyl ether µg/l <0.43 <0.41 NV 625 SVOCs (GC/MS) 4 Chloro 3 methylphenol µg/l <2.4 <2.3 NV 625 SVOCs (GC/MS) 4 Chlorophenyl phenyl ether µg/l <1.7 <1.6 NV 625 SVOCs (GC/MS) 4 Nitrophenol µg/l <1.2 <1.2 NV 625 SVOCs (GC/MS) Acenaphthene µg/l <0.28 <0.27 NV 625 SVOCs (GC/MS) Acenaphthylene µg/l <0.49 <0.47 NV 625 SVOCs (GC/MS) Anthracene µg/l <0.42 <0.40 NV 625 SVOCs (GC/MS) Benzidine µg/l <50 F1 R <48 NV 625 SVOCs (GC/MS) Benzo[a]anthracene µg/l <0.35 <0.33 NV 625 SVOCs (GC/MS) Benzo[a]pyrene µg/l <0.31 <0.29 NV 625 SVOCs (GC/MS) Benzo[b]fluoranthene µg/l <0.53 <0.50 NV 625 SVOCs (GC/MS) Benzo[g,h,i]perylene µg/l <0.50 <0.48 NV 625 SVOCs (GC/MS) Benzo[k]fluoranthene µg/l <0.46 <0.44 NV 625 SVOCs (GC/MS) Bis(2 chloroethoxy)methane µg/l <0.97 <0.92 NV 625 SVOCs (GC/MS) Bis(2 chloroethyl)ether µg/l <0.41 <0.39 NV 625 SVOCs (GC/MS) Bis(2 ethylhexyl) phthalate µg/l < J B NV 625 SVOCs (GC/MS) Butyl benzyl phthalate µg/l <1.0 <0.95 NV 625 SVOCs (GC/MS) Chrysene µg/l <0.54 <0.51 NV 625 SVOCs (GC/MS) Dibenz(a,h)anthracene µg/l <0.51 <0.48 NV 625 SVOCs (GC/MS) Diethyl phthalate µg/l <0.38 <0.36 NV 625 SVOCs (GC/MS) Dimethyl phthalate µg/l <0.21 <0.20 NV 625 SVOCs (GC/MS) Di n butyl phthalate µg/l <1.2 <1.1 NV 625 SVOCs (GC/MS) Di n octyl phthalate µg/l <0.35 <0.33 NV 625 SVOCs (GC/MS) Fluoranthene µg/l <0.20 <0.19 NV 625 SVOCs (GC/MS) Fluorene µg/l <0.31 <0.29 NV 625 SVOCs (GC/MS) Hexachlorobenzene µg/l <0.66 <0.63 NV 625 SVOCs (GC/MS) Hexachlorobutadiene µg/l <3.3 <3.1 NV 625 SVOCs (GC/MS) Hexachlorocyclopentadiene* µg/l <1.5 <1.5 NV 625 SVOCs (GC/MS) Hexachloroethane µg/l <2.1 <2.0 NV 625 SVOCs (GC/MS) Indeno[1,2,3 cd]pyrene µg/l <0.65 <0.62 NV 625 SVOCs (GC/MS) Isophorone µg/l <0.21 <0.20 NV 625 SVOCs (GC/MS) Naphthalene µg/l <0.29 <0.28 NV

5 Analyte CAS No Unit 625 SVOCs (GC/MS) Nitrobenzene µg/l <0.81 <0.77 NV 625 SVOCs (GC/MS) N Nitrosodimethylamine µg/l <0.29 <0.28 NV 625 SVOCs (GC/MS) N Nitrosodi n propylamine µg/l <0.35 <0.33 NV 625 SVOCs (GC/MS) N Nitrosodiphenylamine µg/l <0.44 <0.42 NV 625 SVOCs (GC/MS) Pentachlorophenol µg/l <20 <19 NV 625 SVOCs (GC/MS) Phenanthrene µg/l <0.26 <0.25 NV 625 SVOCs (GC/MS) Phenol µg/l <2.0 <1.9 NV 625 SVOCs (GC/MS) Pyrene µg/l <0.37 <0.35 NV 625 SVOCs (GC/MS) Tentative Identification: 1 Propene, 1,2,3 trichloro, (Z) N/A µg/l 9.6 T J N J 625 SVOCs (GC/MS) Tentative Identification: Unknown N/A µg/l 390 T J J 625 SVOCs (GC/MS) Tentative Identification: 3 Buten 2 one, 3 methyl N/A µg/l 19 T J N J 625 SVOCs (GC/MS) Tentative Identification: Unknown N/A µg/l 7.9 T J J 625 SVOCs (GC/MS) Tentative Identification: Cyclohexane N/A µg/l 29 T J N J 625 SVOCs (GC/MS) Tentative Identification: Unknown N/A µg/l 100 T J J 625 SVOCs (GC/MS) Tentative Identification: Unknown N/A µg/l 34 T J J 625 SVOCs (GC/MS) Tentative Identification: Unknown N/A µg/l 25 T J J 625 SVOCs (GC/MS) Tentative Identification: 1,4 Dioxane N/A µg/l 1.9 J J 625 SVOCs (GC/MS) Tentative Identification: Unknown N/A µg/l 34 T J J 625 SVOCs (GC/MS) Tentative Identification: Dimethyl Sulfoxide N/A µg/l 110 T J N J 625 SVOCs (GC/MS) Tentative Identification: Unknown N/A µg/l 48 T J J 625 SVOCs (GC/MS) Tentative Identification: Dimethyl Sulfoxide N/A µg/l 26 T J N J 625 SVOCs (GC/MS) Tentative Identification: Unknown N/A µg/l 41 T J J 625 SVOCs (GC/MS) Tentative Identification: Unknown N/A µg/l 20 T J J 625 SVOCs (GC/MS) Tentative Identification: 1 Nonadecene N/A µg/l 33 T J N J 625 SVOCs (GC/MS) Tentative Identification: 1 Heneicosyl formate N/A µg/l 34 T J N J 625 SVOCs (GC/MS) Tentative Identification: Unknown N/A µg/l 430 T J J 625 SVOCs (GC/MS) Tentative Identification: 5 Tetradecene, (E) N/A µg/l 22 T J N J 625 SVOCs (GC/MS) Tentative Identification: Unknown N/A µg/l 28 T J J 625 SVOCs (GC/MS) Tentative Identification: Dimethyl Sulfoxide N/A µg/l 3,400 T J N J 625 SVOCs (GC/MS) Tentative Identification: Unknown N/A µg/l 200 T J J 625 SVOCs (GC/MS) Tentative Identification: Unknown N/A µg/l 51 T J J 625 SVOCs (GC/MS) Tentative Identification: Dimethyl Sulfoxide N/A µg/l 140 T J N J 625 SVOCs (GC/MS) Tentative Identification: Unknown N/A µg/l 760 T J J 625 SVOCs (GC/MS) Tentative Identification: Unknown N/A µg/l 1,100 T J J 625 SVOCs (GC/MS) Tentative Identification: Unknown N/A µg/l 18 T J J 625 SVOCs (GC/MS) Tentative Identification: Unknown N/A µg/l 850 T J J 625 SVOCs (GC/MS) Tentative Identification: Unknown N/A µg/l 180 T J J

6 Analyte CAS No Unit 608 OC Pesticides and PCBs 4,4' DDD µg/l < < NV 608 OC Pesticides and PCBs 4,4' DDE µg/l < < NV 608 OC Pesticides and PCBs 4,4' DDT µg/l <0.014 <0.014 NV 608 OC Pesticides and PCBs Aldrin µg/l < < NV 608 OC Pesticides and PCBs alpha BHC µg/l < < NV 608 OC Pesticides and PCBs beta BHC µg/l < F1 UJ < NV 608 OC Pesticides and PCBs Chlordane (technical) µg/l < < NV 608 OC Pesticides and PCBs cis Chlordane µg/l < < NV 608 OC Pesticides and PCBs delta BHC µg/l < UJ < NV 608 OC Pesticides and PCBs Dieldrin µg/l < F2 < NV 608 OC Pesticides and PCBs Endosulfan I µg/l < < NV 608 OC Pesticides and PCBs Endosulfan II µg/l < < NV 608 OC Pesticides and PCBs Endosulfan sulfate µg/l < < NV 608 OC Pesticides and PCBs Endrin µg/l < < NV 608 OC Pesticides and PCBs Endrin aldehyde µg/l < < NV 608 OC Pesticides and PCBs gamma BHC (Lindane) µg/l < < NV 608 OC Pesticides and PCBs Heptachlor µg/l < < NV 608 OC Pesticides and PCBs Heptachlor epoxide µg/l < < NV 608 OC Pesticides and PCBs PCB µg/l <0.12 <0.12 NV 608 OC Pesticides and PCBs PCB µg/l <0.21 <0.21 NV 608 OC Pesticides and PCBs PCB µg/l <0.16 <0.16 NV 608 OC Pesticides and PCBs PCB µg/l <0.10 <0.10 NV 608 OC Pesticides and PCBs PCB µg/l <0.088 <0.088 NV 608 OC Pesticides and PCBs PCB µg/l <0.11 <0.11 NV 608 OC Pesticides and PCBs PCB µg/l <0.15 <0.15 NV 608 OC Pesticides and PCBs Toxaphene µg/l <0.35 <0.35 NV 608 OC Pesticides and PCBs trans Chlordane µg/l < < NV L211 Diethylstilbestrol (DES) ng/l <0.5 UJ <50 UJ L211 17alpha Estradiol ng/l <0.5 UJ <50 UJ L211 17beta Estradiol ng/l <0.5 UJ <50 UJ L211 Estriol ng/l <0.5 UJ <50 UJ L211 Estrone ng/l <0.5 UJ <50 UJ L211 17alpha Ethynyl estradiol ng/l <0.5 UJ <50 UJ L211 Progesterone ng/l <0.1 UJ <10 UJ L211 cis Testosterone ng/l <0.1 UJ <10 UJ L211 trans Testosterone ng/l <0.1 UJ <10 UJ L200 Bisphenol A µg/l <0.1 UJ <10 UJ L200 Nonylphenol, isomer mix µg/l <0.5 UJ <50 UJ L200 4 n Octylphenol µg/l <0.5 UJ <50 UJ L200 4 tert Octylphenol µg/l <0.5 UJ <50 UJ L200 Pentachlorophenol µg/l <0.1 UJ <10 UJ L200 Phenylphenol µg/l <0.1 UJ <10 UJ L200 Tetrabromobisphenol A µg/l <0.1 UJ <10 UJ L200 2,4,6 Trichlorophenol µg/l <0.1 UJ <10 UJ

7 Analyte CAS No Unit L220 Acetaminophen µg/l <0.005 UJ <0.5 UJ L220 Antipyrine µg/l <0.001 UJ <0.1 UJ L220 Atenolol µg/l J <0.1 UJ L220 Azithromycin µg/l <0.005 UJ <0.5 UJ L220 Caffeine µg/l <0.05 UJ <5 UJ L220 Carbadox µg/l <0.005 UJ <0.5 UJ L220 Carbamazepine µg/l J <0.1 UJ L220 Cotinine µg/l J <0.1 UJ L220 DEET µg/l J <0.5 UJ L220 Dexamethasone µg/l <0.005 UJ <0.5 UJ L220 Diazepam µg/l <0.001 UJ <0.1 UJ L220 Diltiazem µg/l < UJ <0.01 UJ L220 Erythromycin µg/l <0.001 UJ <0.1 UJ L220 Fluoxetine (Prozac) µg/l <0.001 UJ <0.1 UJ L220 Iopromide µg/l <0.05 UJ <5 UJ L220 Lincomycin µg/l J <0.01 UJ L220 Meprobamate µg/l J <0.1 UJ L220 Monensin µg/l <0.001 UJ <0.1 UJ L220 Narasin µg/l <0.001 UJ <0.1 UJ L220 Nicotine µg/l <0.01 UJ 1.9 J L220 Oleandomycin µg/l <0.001 UJ <0.1 UJ L220 Paraxanthine µg/l J J L220 Primidone µg/l J <0.5 UJ L220 Roxithromycin µg/l <0.001 UJ <0.1 UJ L220 Salinomycin µg/l < UJ <0.01 UJ L220 Sulfadiazine µg/l <0.001 UJ <0.1 UJ L220 Sulfadimethoxine µg/l J <0.01 UJ L220 Sulfamethazine µg/l <0.001 UJ <0.1 UJ L220 Sulfamethizole µg/l <0.001 UJ <0.1 UJ L220 Sulfamethoxazole µg/l 0.02 J <0.1 UJ L220 Sulfasalazine µg/l <0.005 UJ <0.5 UJ L220 Sulfathiazole µg/l <0.001 UJ <0.1 UJ L220 Theobromine µg/l <0.05 UJ <5 UJ L220 Trimethoprim µg/l <0.001 UJ <0.1 UJ L220 Tris(2 chloroethyl) phosphate µg/l <0.01 UJ <1 UJ L220 Tris(chloropropyl) phosphate µg/l 0.11 J <1 UJ L220 Tylosin µg/l <0.001 UJ <0.1 UJ L220 Virginiamycin M µg/l <0.001 UJ <0.1 UJ

8 Analyte CAS No Unit L221 Acesulfame K µg/l 0.4 J <1.00 UJ L221 Bezafibrate µg/l < UJ < UJ L221 Chloramphenicol µg/l <0.005 UJ <0.500 UJ L221 Chlorotetracycline µg/l <0.05 UJ <5.00 UJ L221 Clofibric acid µg/l < UJ < UJ L221 Diclofenac µg/l < UJ < UJ L221 Dilantin µg/l <0.002 UJ <0.200 UJ L221 Gemfibrozil µg/l < UJ < UJ L221 Ibuprofen µg/l <0.05 UJ <5.00 UJ L221 Levothyroxine (Synthroid) µg/l <0.002 UJ <0.200 UJ L221 Naproxen µg/l <0.002 UJ <0.200 UJ L221 Penicillin G µg/l <0.002 UJ <0.200 UJ L221 Penicillin V µg/l <0.002 UJ <0.200 UJ L221 Prednisone µg/l <0.002 UJ <0.200 UJ L221 Salicylic acid µg/l <0.05 UJ <5.00 UJ L221 Sucralose µg/l 2.4 J <2.500 UJ L221 Theophylline µg/l <0.005 UJ <0.500 UJ L221 Triclocarban µg/l < UJ < UJ L221 Triclosan µg/l <0.05 UJ <5.000 UJ Notes: s: 1. The maximum concentration for HFPO Dimer Acid and Table 3 SOP compounds are reported here. * RPD of the LCS and LCSD exceeds the control limits These compounds are analyzed twice by the laboratory as a quality control measured. ^ Instrument related QC is outside acceptance limits, see lab report for details. no value available B Compound was found in the blank and sample. < data were not detected above the reporting limit. F1 MS and/or MSD Recovery is outside acceptance limits. µg/l micrograms per liter F2 MS/MSD RPD exceeds control limits CAS No chemical abstracts service number H Sample was prepped or analyzed beyond the specified holding time Cr chromium J is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. CVAA cold vapor atomic absorption N Presumptive evidence of material. GC/MS gas chromatography / mass spectrometry T is a tentatively identified compound (TIC) and an estimated value. ICP inductively coupled plasma LCS / LCSD laboratory control spike / laboratory control spike duplicate MDL method detection limit mg/l milligrams per liter MS / MSD matrix spike / matrix spike duplicate N/A not available ng/l nanograms per liter NV Data not validated so no validation qualifiers available OC Pesticides organochlorine pesticides PCBs polychlorinated biphenyls PFAS per and polyfluorinated alkyl substances QC quality control RL reporting limit RPD relative percentage difference SOP standard operating procedure SVOCs semi volatile organic compounds TIC tentatively identified compound VOCs volatile organic compounds

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