Aliphatic Polycarbonates and Poly(ester carbonate)s from Fatty Acid Derived Monomers
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1 Supporting Information for Aliphatic Polycarbonates and Poly(ester carbonate)s from Fatty Acid Derived Monomers Arvind S. More, a,b Dnyaneshwar V. Palaskar, a,b Eric Cloutet, a,b Benoit Gadenne, c Carine Alfos, c and Henri Cramail* a,b a Université de Bordeaux, Laboratoire de Chimie des Polyméres Organiques, UMR 5629, IPB/ENSCBP, 16 avenue Pey-Berland,F-33607, Pessac cedex, France. b Centre National de la Recherche Scientifique, Laboratoire de Chimie des Polyméres Organiques, F-33607, Pessac cedex, France. c ITERG, 11 rue Gaspard Monge, Parc Industriel, Pessac Cedex, F-33600, France. Corresponding author. address: cramail@enscbp.fr
2 Figure S1. 1 H-NMR spectrum of Oleyl Carbonate
3 Figure S2. 1 H-NMR spectrum of Epoxidised Oleyl Carbonate
4 f c b d a e Figure S3. 13 C-NMR spectrum of ethyl(10(9)-hydroxy-9(10)-methoxy octadecyl)carbonate (EHMOC, 4/4 ) (AB-self condensable monomer)
5 Figure S4. 1 H-NMR spectrum of 4-Hydroxybutyl-12-hydroxyoctadec-9-enoate (HBHOE)
6 Figure S5. 13 C-NMR spectrum of 4-[(ethoxycarbonyl)oxy] butyl-12-[(ethoxycarbonyl)oxy]octadec-9- enoate (EOBEOE)
7 ppm Figure S6. 13 C-NMR spectrum polycarbonate (PC-I) derived by self polycondensation of EHMOC
8 Figure S7. SEC traces of polycarbonates and poly(ester carbonate)s
9 ppm Figure S8. 1 H and 13 C-NMR spectra of poly(ester carbonate) (PEC-III) derived by polycondensation of EOBEOE and Hexanediol
10 ppm Figure S9. 13 C-NMR spectrum of poly(ester carbonate) (PEC-IV) derived by polycondensation of EOBEOE and PEG200
11 ppm Figure S10. 1 H and 13 C-NMR spectra of poly(ester carbonate) (PEC-V) derived by polycondensation of EOBEOE and PPG400
12 ppm Figure S11. 1 H and 13 C-NMR spectra of poly(ester carbonate) (PEC-VI) derived by polycondensation of EOBEOE and PCL1250
13 ppm Figure S12. 1 H and 13 C-NMR spectra of poly(ester carbonate) (PEC-VII) derived by polycondensation of EOBEOE and Isosorbide
14 a b a b ppm ppm Figure S13. 1 H and 13 C-NMR spectra of PEC-VIII derived by polycondensation of HBHOE and DEC
15 Figure S14. MALDI-TOF mass spectrum of polycarbonate (PC-I) derived by self-polycondensation of EHMOC
16 Figure S15. MALDI-TOF mass spectrum of poly(ester carbonate) (PEC-III) derived by polycondensation of EOBEOE and Hexanediol
17 Figure S16. MALDI-TOF mass spectrum of poly(ester carbonate) (PEC-IV) derived by polycondensation of EOBEOE and PEG200
18 Figure S17. MALDI-TOF mass spectrum of poly(ester carbonate) (PEC-V) derived by polycondensation of EOBEOE and PPG400
19 Figure S18. MALDI-TOF mass spectrum of poly(ester carbonate) (PEC-VI) derived by polycondensation of EOBEOE and PCL1250
20 Figure S19. MALDI-TOF mass spectrum of poly(ester carbonate) (PEC-VII) derived by polycondensation of EOBEOE and Isosorbide
21 Figure S20. DSC curves of polycarbonates and poly(ester carbonate)s derived from EHMOC and EOBEOE, respectively
22 Figure S21. TGA curves of polycarbonates and poly(ester carbonate)s derived from EHMOC and EOBEOE, respectively
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