Calmag Precipitates from water 8th report
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1 PLIVA CROATIA Ltd. TAPI Research and Development Physical R&D Dr. Sc. Želimir Jelčić Report No./ Izvješće br.: PLIVA CROATIA Ltd calmag 8th report arial.doc: /ŽJ/žj/ Calmag Precipitates from water 8th report Report No./ Izvješće br.: / Data provided by: Dr. sc. Želimir Jelčić Users: Boris Morožin 1/30
2 Precipitate Samples 1. Uzorak sa grijača-perilica rublja 1; 42M ⁰6 (N2+2N)+(S1+1S) x 3 u bubnju 101 pranje sa deterđentom i rubljem 2. Uzorak sa grijača-perilica rublja 4; 42M ⁰14 (N2+2N)+(S1+1S) u križ na dovodu 101 pranje sa deterđentom i rubljem 3. Uzorak sa bubnja-perilica rublja 1; 42M ⁰6 (N2+2N)+(S1+1S) x 3 u bubnju 101 pranje sa deterđentom i rubljem 4. Uzorak sa bubnja-perilica rublja 4; 42M ⁰14 (N2+2N)+(S1+1S) u križ na dovodu 101 pranje sa deterđentom i rubljem Methods SEM Jeol JSM-5800 scanning microscope Sputtered with gold by Edwards S150 sputter coater X-ray mapping by Link Tetra and Oxford link Pentafet model /30
3 Uzorak sa grijača-perilica rublja 1; 42M ⁰6 (N2+2N)+(S1+1S) x 3 u bubnju 101 pranje sa deterđentom i rubljem Magnificatio n (x) /30
4 /30
5 2000 5/30
6 Uzorak sa grijača-perilica rublja 4; 42M ⁰14 (N2+2N)+(S1+1S) u križ na dovodu 101 pranje sa deterđentom i rubljem Magnificatio n (x) /30
7 /30
8 2000 8/30
9 Uzorak sa bubnja-perilica rublja 1; 42M ⁰6 (N2+2N)+(S1+1S) x 3 u bubnju 101 pranje sa deterđentom i rubljem Magnificatio n (x) /30
10 /30
11 /30
12 Uzorak sa bubnja-perilica rublja 4; 42M ⁰14 (N2+2N)+(S1+1S) u križ na dovodu 101 pranje sa deterđentom i rubljem Magnificatio n (x) /30
13 /30
14 /30
15 Uzorak sa grijača-perilica rublja 1; 42M ⁰6 (N2+2N)+(S1+1S) x 3 u bubnju 101 pranje sa deterđentom i rubljem 15/30
16 Uzorak sa grijača-perilica rublja 1; 42M ⁰6 (N2+2N)+(S1+1S) x 3 u bubnju 101 pranje sa deterđentom i rubljem (a) (c) (b) (d) (e) (f) Figure 1 Uzorak sa grijača-perilica rublja 1; 42M ⁰6 (N2+2N)+(S1+1S) x 3 u bubnju 101 pranje sa deterđentom i rubljem: (a) X-ray spectrum; (b) SEM image, magnification 4000x; (c) Calcium (Ca) elemental map (d) overlay; (e) silizium (Si, sodium (Na) and oxygen (O) elemental maps added; (f) overlay 16/30
17 Uzorak sa grijača-perilica rublja 1; 42M ⁰6 (N2+2N)+(S1+1S) x 3 u bubnju 101 pranje sa deterđentom i rubljem 17/30
18 Uzorak sa grijača-perilica rublja 1; 42M ⁰6 (N2+2N)+(S1+1S) x 3 u bubnju 101 pranje sa deterđentom i rubljem (a) (c) (b) (d) (e) (f) Figure 2 Uzorak sa grijača-perilica rublja 1; 42M ⁰6 (N2+2N)+(S1+1S) x 3 u bubnju 101 pranje sa deterđentom i rubljem: (a) X-ray spectrum; (b) SEM image, magnification 4000x; (c) Calcium (Ca) elemental map (d) overlay; (e) silizium (Si, sodium (Na) and oxygen (O) elemental maps added; (f) overlay 18/30
19 Uzorak sa grijača-perilica rublja 4; 42M ⁰14 (N2+2N)+(S1+1S) u križ na dovodu 101 pranje sa deterđentom i rubljem 19/30
20 Uzorak sa grijača-perilica rublja 4; 42M ⁰14 (N2+2N)+(S1+1S) u križ na dovodu 101 pranje sa deterđentom i rubljem (a) (c) (b) (d) (e) (f) Figure 3 Uzorak sa grijača-perilica rublja 4; 42M ⁰14 (N2+2N)+(S1+1S) u križ na dovodu 101 pranje sa deterđentom i rubljem: (a) X-ray spectrum; (b) SEM image, magnification 4000x; (c) Calcium (Ca) elemental map (d) overlay; (e) silizium (Si, sodium (Na) and oxygen (O) elemental maps added; (f) overlay 20/30
21 Uzorak sa grijača-perilica rublja 4; 42M ⁰14 (N2+2N)+(S1+1S) u križ na dovodu 101 pranje sa deterđentom i rubljem 21/30
22 Uzorak sa grijača-perilica rublja 4; 42M ⁰14 (N2+2N)+(S1+1S) u križ na dovodu 101 pranje sa deterđentom i rubljem (a) (c) (b) (d) (e) (f) Figure 4 Uzorak sa grijača-perilica rublja 4; 42M ⁰14 (N2+2N)+(S1+1S) u križ na dovodu 101 pranje sa deterđentom i rubljem: (a) X-ray spectrum; (b) SEM image, magnification 4000x; (c) Calcium (Ca) elemental map (d) overlay; (e) silizium (Si, sodium (Na) and oxygen (O) elemental maps added; (f) overlay 22/30
23 Uzorak sa bubnja-perilica rublja 1; 42M ⁰6 (N2+2N)+(S1+1S) x 3 u bubnju 101 pranje sa deterđentom i rubljem 23/30
24 Uzorak sa bubnja-perilica rublja 1; 42M ⁰6 (N2+2N)+(S1+1S) x 3 u bubnju 101 pranje sa deterđentom i rubljem (a) (c) (b) (d) (e) (f) Figure 5 Uzorak sa bubnja-perilica rublja 1; 42M ⁰6 (N2+2N)+(S1+1S) x 3 u bubnju 101 pranje sa deterđentom i rubljem: (a) X-ray spectrum; (b) SEM image, magnification 4000x; (c) Calcium (Ca) elemental map (d) overlay; (e) silizium (Si, sodium (Na) and oxygen (O) elemental maps added; (f) overlay 24/30
25 Uzorak sa bubnja-perilica rublja 1; 42M ⁰6 (N2+2N)+(S1+1S) x 3 u bubnju 101 pranje sa deterđentom i rubljem 25/30
26 Uzorak sa bubnja-perilica rublja 1; 42M ⁰6 (N2+2N)+(S1+1S) x 3 u bubnju 101 pranje sa deterđentom i rubljem (a) (c) (b) (d) (e) (f) Figure 6 Uzorak sa bubnja-perilica rublja 1; 42M ⁰6 (N2+2N)+(S1+1S) x 3 u bubnju 101 pranje sa deterđentom i rubljem: (a) X-ray spectrum; (b) SEM image, magnification 4000x; (c) Calcium (Ca) elemental map (d) overlay; (e) silizium (Si, sodium (Na) and oxygen (O) elemental maps added; (f) overlay 26/30
27 Uzorak sa bubnja-perilica rublja 4; 42M ⁰14 (N2+2N)+(S1+1S) u križ na dovodu 101 pranje sa deterđentom i rubljem 27/30
28 Uzorak sa bubnja-perilica rublja 4; 42M ⁰14 (N2+2N)+(S1+1S) u križ na dovodu 101 pranje sa deterđentom i rubljem (a) (c) (b) (d) (e) (f) Figure 7 Uzorak sa bubnja-perilica rublja 4; 42M ⁰14 (N2+2N)+(S1+1S) u križ na dovodu 101 pranje sa deterđentom i rubljem: (a) X-ray spectrum; (b) SEM image, magnification 4000x; (c) Calcium (Ca) elemental map (d) overlay; (e) silizium (Si, sodium (Na) and oxygen (O) elemental maps added; (f) overlay 28/30
29 Uzorak sa bubnja-perilica rublja 4; 42M ⁰14 (N2+2N)+(S1+1S) u križ na dovodu 101 pranje sa deterđentom i rubljem 29/30
30 Uzorak sa bubnja-perilica rublja 4; 42M ⁰14 (N2+2N)+(S1+1S) u križ na dovodu 101 pranje sa deterđentom i rubljem (a) (c) (b) (d) (e) (f) Figure 8 Uzorak sa bubnja-perilica rublja 4; 42M ⁰14 (N2+2N)+(S1+1S) u križ na dovodu 101 pranje sa deterđentom i rubljem : (a) X-ray spectrum; (b) SEM image, magnification 2000x; (c) Calcium (Ca) elemental map (d) overlay; (e) silizium (Si, sodium (Na) and oxygen (O) elemental maps added; (f) overlay 30/30
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