Maxum. PD PA AP Maxum II Official Product Specifications. Specifications Overview 1. Maxum II Common Specifications 2. Airbath or Airless Oven 3

Transcription

1 Specifications Overview 1 Maxum II Common Specifications 2 Maxum PD PA AP Maxum II Official Product Specifications Brochure Airbath or Airless Oven 3 Modular Oven 4 Ovens 5 Detectors and Associated Devices 6 Valve Specifications 7 Network Access Unit 8 Appendix - Change Log A These specifications supercede applicable information in previous manuals. May 2018 A5E Rev04 ECO# DP5A

2 Legal information Warning notice system This manual contains notices you have to observe in order to ensure your personal safety, as well as to prevent damage to property. The notices referring to your personal safety are highlighted in the manual by a safety alert symbol, notices referring only to property damage have no safety alert symbol. These notices shown below are graded according to the degree of danger. DANGER indicates that death or severe personal injury will result if proper precautions are not taken. WARNING indicates that death or severe personal injury may result if proper precautions are not taken. CAUTION indicates that minor personal injury can result if proper precautions are not taken. NOTICE indicates that property damage can result if proper precautions are not taken. If more than one degree of danger is present, the warning notice representing the highest degree of danger will be used. A notice warning of injury to persons with a safety alert symbol may also include a warning relating to property damage. Qualified Personnel The product/system described in this documentation may be operated only by personnel qualified for the specific task in accordance with the relevant documentation, in particular its warning notices and safety instructions. Qualified personnel are those who, based on their training and experience, are capable of identifying risks and avoiding potential hazards when working with these products/systems. Proper use of Siemens products Note the following: Trademarks WARNING Siemens products may only be used for the applications described in the catalog and in the relevant technical documentation. If products and components from other manufacturers are used, these must be recommended or approved by Siemens. Proper transport, storage, installation, assembly, commissioning, operation and maintenance are required to ensure that the products operate safely and without any problems. The permissible ambient conditions must be complied with. The information in the relevant documentation must be observed. All names identified by are registered trademarks of Siemens AG. The remaining trademarks in this publication may be trademarks whose use by third parties for their own purposes could violate the rights of the owner. Disclaimer of Liability We have reviewed the contents of this publication to ensure consistency with the hardware and software described. Since variance cannot be precluded entirely, we cannot guarantee full consistency. However, the information in this publication is reviewed regularly and any necessary corrections are included in subsequent editions. Siemens AG Division Process Industries and Drives Postfach NÜRNBERG GERMANY Document order number: A5E P 05/2018 Subject to change Copyright Siemens AG All rights reserved

3 Table of contents 1 Specifications Overview Maxum II Common Specifications Airbath or Airless Oven Modular Oven Ovens Detectors and Associated Devices Valve Specifications Model 50 Valve Specifications Model 20 Valve Specifications Model 20 High Temperature Valve Specifications Model 11 Valve Specifications Model 11 Low Dead Volume Valve (LDV) Specifications Siemens Liquid Injection Valve Valco A4 C6UWE Valve Specifications Network Access Unit...31 A Appendix - Change Log...35 A.1 January 2018 Changes...35 Brochure, May 2018, A5E Rev04 ECO# DP5A

4 Table of contents 4 Brochure, May 2018, A5E Rev04 ECO# DP5A

5 Specifications Overview 1 The specifications in this document are provided to assist in product comparison and selection. See the product documentation for more details. Note Specifications Are Application-Dependent The specifications given in this document reflect the performance of the component when used in a Maxum II Gas Chromatograph as a typical system. Performance may vary between individual installations. Note See Individual Documentation Package Each analyzer is shipped with an Individual Documentation Package that includes drawings, specifications and certifications for the individual unit that supersede the information in this document. Brochure, May 2018, A5E Rev04 ECO# DP5A

6 Specifications Overview 6 Brochure, May 2018, A5E Rev04 ECO# DP5A

7 Maxum II Common Specifications 2 Table 2-1 General Temperature control ±0.02 C (±0.05 F) Calibration Comparison measurement with external standard Type Manual or automatic Zero value Automatic baseline correction Span Standard sample cylinder (single or multipoint calibration possible) Table 2-2 Measuring Response Sensitivity (depending on application) Linearity (depending on application) Effects of vibrations Repeatability in % of full scale (Depending on application) ±0.5% of span ±2% of span Negligible Range Value 2 and 100% ±0.5% 0.05 and 2% ±1%; 50 and 500 ppm ±2% 5 and 50 ppm ±3% 0.5 and 5 ppm ±5% Table 2-3 Climatic conditions Ambient temperature and humidity Altitude -18 to 50 C (0 to 122 F) application-dependent Specific installations may require additional environmental constraints. See the custom documentation package. Note: If the Maxum II is exposed to high condensing humidity with the electronics open or without dry purge air applied, then it must be allowed to re-stabilize at the above stated conditions for at least 8 hours before electrical power is applied. Note: Depending on application characteristics such as number of detectors, oven temperature, and electronic loading, the acceptable ambient temperature range may be reduced. For application-specific detail, contact Siemens through the Siemens Industry Online Support (SIOS) website: Up to 2000m (6561') for analyzers using 230VAC Supply Up to 3000m (9842') for analyzers using 115VAC Supply Brochure, May 2018, A5E Rev04 ECO# DP5A

8 Maxum II Common Specifications Table 2-4 Gas Requirements α Type Quality γ Pressure Approximate Consumption Instrument air ISO :2010 [3:2:3] [ 3 : - : - ] Dust filtering down to 1 μm [ - : 2 : - ] Dew point of -40 C [ - : - : 3 ] Total hydrocarbon below 1 mg per cubic meter (appr. 0.8 ppmw) Application and valve-model dependent. See analyzer Custom Documentation and valve specifications. Carrier gas Hydrogen 4.6 ( 99,996%) 500 to 825 kpa (72.5 to 120 Nitrogen psig) Helium Argon Synthetic air Industry standard Combustion gas Hydrogen 5.0 ( 99,999%) 500 to 825 kpa (72.5 to 120 psig) Combustion air Synthetic air Hydrocarbon free 500 to 825 kpa (72.5 to 120 psig) Actuation air Instrument air Discharge Gas for PDD Dopant Gas for PDECD Purge Gas for PDD Purge air (py purge) Purge air (px purge) Valve gas (for Model 50 β ) Oven heating (for Airbath oven) Helium 3% Xenon in Helium catalytically purified, 5.0 ( 99,999 %) catalytically purified, 5.0 ( 99,999 %) 85 l/min per oven 50 to 150 ml/min/train 30 to 50 ml/min/fid 100 ml/min/fpd 400 ml/min/fid 100 ml/min/fpd 200 to 300 kpa (30 to 72 psig) 30 to 40 ml/m 200 to 300 kpa (30 to 72 psig) 3 ml/m Helium 5.0 ( 99,999 %) 200 to 300 kpa (30 to 72 psig) 25 to 35 ml/m Instrument air or Nitrogen Instrument air or Nitrogen Instrument air 400 to 1655 kpa (58 to 240 psig) Initial purge: 65l/min Operating purge: 3.5 l/min Instrument air 400 to 600 kpa (58 to 87 psig) Initial purge: 60 to 80 l/min Instrument air 650 to 1650 kpa (95 to 240 psig) (Lower values application dependent) Instrument air 400 to 600 kpa (58 to 87 psig) 85 l/min/oven Operating purge: 12 to 18 l/min Vortex cooler Instrument air 300 to 600 kpa (43.5 to 87 psig) 130 to 170 l/min PTGC Instrument air 400 to 600 kpa (58 to 87 psig) 210 l/min PTGC + Vortex Instrument air 400 to 600 kpa (58 to 87 psig) 575 l/min Strip gas Nitrogen 5.0 ( 99,999%) 400 to 600 kpa (58 to 87 psig) 6 to 8 l/h α These are general parameters that vary depending on the individual application and configuration. β See Model 50 Valve Specifications (Page 25) γ For more information see specifications from industrial gas suppliers for "4.6" and "5.0" in Europe, and "pure" and "ultra-pure" in the U.S. 8 Brochure, May 2018, A5E Rev04 ECO# DP5A

9 Maxum II Common Specifications Table 2-5 Influencing variables Effects of ambient temperature Negligible with electronic pressure control. Different effects with mechanical pressure control (depending on application) Table 2-6 Corrosion protection Corrosion protection Purging with dry air to protect the electronics Airbath oven with stainless steel lining Airless oven made of aluminum Steel lining painted on outside (epoxy powder coating) Table 2-7 Mounting Clearance Mounting clearance Clearance on left: 460 mm (18") from walls and other devices Clearance on right: 460 mm (18") in all cases Clearance at front: 654 mm (26") in all cases Center-to-center: 1,120 mm (44") in all cases Table 2-8 Electronic Pressure Controller Parameter Maximum inlet pressure Pressure output range Minimum differential between EPC inlet and outlet Value 825 kpa (120 psig) 35 to 700 kpa (5 to 100 psig) 35 kpa (5 psi) Flow range from EPC (see note below) 5 to 500 cm 3 /s Controlled pressure stability over temperature range Short-term pressure stability Typical response time for step change in setpoint. ±0.5% of setpoint kpa (± psi) over 30-second interval Stable to within 0.1% of final value within 0.5 seconds (For hydrogen the response time is approximately 1 second). Note When running applications with column flow rates of less than 5 cm 3 /s, a separate bleed flow path is recommended in order to reduce the time required to achieve pressure stability when variable setpoints are used. Depending on the volume involved, a bleed flow rate of 5-10 cm 3 /s is recommended. Brochure, May 2018, A5E Rev04 ECO# DP5A

10 Maxum II Common Specifications 10 Brochure, May 2018, A5E Rev04 ECO# DP5A

11 Airbath or Airless Oven 3 Table 3-1 Dimensions Weight Overall Dimensions (including mounting hardware) 77 kg (170 lbs.) application dependent Height: mm (41.5 ) Width: 752 mm (26.6 ) Depth: mm (16.4 ) Dimensions are application dependent and may not include space required for externally-mounted options. Figure 3-1 Maxum II Airless/Airbath Dimensions Brochure, May 2018, A5E Rev04 ECO# DP5A

12 Airbath or Airless Oven Table 3-2 Configuration Oven options Single isothermal airbath oven or divided airbath oven with two independent isothermal zones Single oven or two independent, airless ovens in separate oven areas. Programmable-temperature (PTGC) oven Detector options Thermal conductivity Flame ionization Flame photometric Pulse discharge detector in Helium ionization mode Pulse discharge detector in Photo-ionization mode Pulse discharge detector in Electron capture mode Number of detectors 1, 2 or 3 in any combination of detector module types for airbath ovens (max. 2 FPDs) Sampling and column valves Diaphragm valves Valveless option Column options Regulation of gas supply 1, or 2 in any combination of detector module types for airless ovens, up to 3 in special configurations Diaphragm plunger valves Rotary valves Liquid injection valve Live switching Packed, micropacked or capillary columns Up to 8 electronic pressure regulator channels and up to 6 mechanical pressure regulators Table 3-3 Enclosure Protection Ingress protection IP54 Explosion protection Standard configurations: Certified according to ATEX with air or nitrogen purging for Zone 1 (II2G Ex... IIB + H2... Gb) Suitable for use in non-hazardous areas and with non-dangerous conditions Certified according to CSA C/US for use in Class 1, Div. 1, Groups B, C, D with air or nitrogen purging Certified according to CSA C/US for use in Class 1, Div. 2, Groups B, C, D. Important note! Purging of the electronics area with instrument air or nitrogen is recommended to maintain optimum measurement performance. The PDD is not certified for hazardous areas. EMI/RFI design CE-compatible; in conformity with 2014/30/EU (EMC directive) CE-compatible; in conformity with 2014/35/EU (low-voltage directive) Tested according to EN / IEC Table 3-4 Electrical characteristics Power supply Single-phase AC, 100 to 130 V or 195 to 260 V (dependent on configuration), 47 to 63 Hz 12 Brochure, May 2018, A5E Rev04 ECO# DP5A

13 Airbath or Airless Oven Table 3-5 Electrical inputs and outputs Standard input and output 2 analog outputs Card slots for optional inputs and outputs via internal I 2 C bus 4 digital outputs (1 for output of system faults, 3 are user-configurable) 4 digital inputs; 2 Input and output cards I2C_AIO: 8 analog outputs, 8 analog inputs, 2 digital inputs I2C_DIO: 6 digital inputs and 8 digital outputs I2C_ADIO: 4 digital inputs and 4 digital outputs, 4 analog inputs and 4 analog outputs Digital inputs Optically coupled with a common for all inputs. Digital outputs Analog inputs Analog outputs Termination Self-powered floating-contact input, or configurable for sinking or sourcing current. Sourcing current mode: 24 V internal isolated supply, with positive terminal of supply at common. Sinking current mode: 5 V internal isolated supply, with negative terminal of supply at common. Floating double-throw contacts, maximum contact load rating 1 A at 30 V (AC or DC). External diode shunt suppression should be used for inductive DC loads, preferably at the load -20 to 20 ma into 50 Ω or -10 to 10 V R in = 0.1 MΩ With alternate insulation up to 10 V 0/4 to 20 ma into max. 750 Ω, common negative pole, electrically isolated from ground; freely connectable to ground SYSCON-based I/O: Terminal strip for braided or solid cable with maximum section of 1.5 mm 2 (16AWG) Expansion board-based I/O: Screw terminal for shielded or solid cable with a maximum area of 0.82 mm 2 (18AWG) Table 3-6 Communication Serial ports 4 RS232/RS485 ports, e.g. Modbus Ethernet Standard 10/100 BaseT Ethernet with 4 RJ45 connectors e.g. Modbus TCP IP or OPC Optional ESBF board Fiber-optic 100Base FX multimode with ST connection 3 x RJ45 and 1 x optical (Optical port uses LED instead of laser for safer diffusedenergy fiber link; less than 40μW at approximately 1300nm) Gas sample inlet conditions depend on application and valve choice. See also Valve Specifications (Page 25) Brochure, May 2018, A5E Rev04 ECO# DP5A

14 Airbath or Airless Oven Table 3-7 Combustion gas supply Combustion gas Hydrogen with a purity of % Typical consumption quantity: l/month per detector module Combustion air Reference air (< 1 ppm THC, O 2 concentration 20 to 21%). Synthetic air, or supply through instrument air with catalytic purification (optional). Typical consumption quantity: l/month 14 Brochure, May 2018, A5E Rev04 ECO# DP5A

15 Modular Oven 4 Table 4-1 Dimensions Weight Overall Dimensions (including mounting hardware) 60 kg (132 lbs.) application dependent Height: mm (28.75") Width: 752 mm (26.6 ) Depth: mm (16.4") Dimensions are application dependent and may not include space required for externally-mounted options. Figure 4-1 Maxum II Modular Oven Dimensions Table 4-2 Configuration (application dependent) Oven options Single airless oven or two independent, airless ovens. Detector module type Optionally small oven for one small analytical module, large oven for two small analytical modules or one large analytical module. Two small ovens, two large ovens or any combination of two ovens is possible. Dual-oven version has two independent ovens with separate doors. Thermal conductivity Number of detector modules One 4-cell TCD for small analytical modules One or two 4-cell TCD for large analytical modules Sampling and column valves One Model 50 diaphragm valve in small analytical module One, two, or three Model 50 diaphragm valves in large analytical module Brochure, May 2018, A5E Rev04 ECO# DP5A

16 Modular Oven Columns Regulation of gas supply Packed, micropacked or metal capillary columns Up to 6 electronic pressure regulator channels and up to 4 mechanical pressure regulators Table 4-3 Enclosure Protection Ingress protection IP54, Category 1 Explosion protection Standard configurations: Certified according to IECEx with air or nitrogen purging for Zone 1 (IIC T4 Gb) Certified according to ATEX with air or nitrogen purging for Zone 1 (II2G Ex... IIC... Gb) Suitable for use in non-hazardous areas and with non-dangerous conditions Certified according to CSA C/US for use in Class 1, Div. 1, Groups A, B, C, D with air or nitrogen purging Certified according to CSA C/US for use in Class 1, Div. 2, Groups A, B, C, D. Important note! Purging of the electronics area with instrument air or nitrogen is recommended to maintain optimum measurement performance. EMI/RFI design CE-compatible; in conformity with 2014/30/EU (EMC directive) CE-compatible; in conformity with 2014/35/EU (low-voltage directive) Tested according to EN / IEC Table 4-4 Electrical characteristics Power supply Single-phase AC, 85 to 264 V, 47 to 63 Hz Max. 655 VA, nominal 280 VA Optional: External 24 V DC ±10% 10 A with 32 V voltage limiting Max. 100 mv residual ripple and interferences minimum to maximum at 20 MHz Fusing at max. 20 A External 24 V supply must accept minus to ground Table 4-5 Electrical inputs and outputs CIM-based IO 2 digital outputs Card slots for optional inputs and outputs via internal I 2 C bus 4 slots, maximum 2 IO cards (in IO tray) Input and output cards I2C_AIO: 8 analog outputs, 8 analog inputs, 2 digital inputs I2C_DIO: 6 digital inputs and 8 digital outputs I2C_ADIO: 4 digital inputs and 4 digital outputs, 4 analog inputs and 4 analog outputs Digital inputs Optically coupled with a common for all inputs. Self-powered floating-contact input, or configurable for sinking or sourcing current. Sourcing current mode: 24 V internal isolated supply, with positive terminal of supply at common. Sinking current mode: 5 V internal isolated supply, with negative terminal of supply at common. 16 Brochure, May 2018, A5E Rev04 ECO# DP5A

17 Modular Oven Digital outputs Analog inputs Analog outputs Termination Floating double-throw contacts, maximum contact load rating 1 A at 30 V (AC or DC). External diode shunt suppression should be used for inductive DC loads, preferably at the load -20 to 20 ma into 50 Ω or -10 to 10 V R in = 0.1 MΩ With alternate insulation up to 10 V 0/4 to 20 ma into max. 750 Ω, common negative pole, electrically isolated from ground; freely connectable to ground SYSCON-based I/O: Terminal strip for braided or solid cable with maximum section of 1.5 mm 2 (16AWG) Expansion board-based I/O: Spring contacts for shielded or solid cable with a maximum area of 0.82 mm 2 (18AWG) Table 4-6 Communication Serial ports 2 Serial Port 1: RS232/RS485 selectable Serial Port 2: RS485 mode only Ethernet Standard 10/100 BaseT Ethernet with 2 RJ45 connectors e.g. Modbus TCP IP or OPC Optional ESBF board Fiber-optic 100Base FX multimode with ST connection 3 x RJ45 and 1 x optical (Optical port uses LED instead of laser for safer diffusedenergy fiber link; less than 40μW at approximately 1300nm) Table 4-7 Gas sample inlet conditions Sample flow Sample filter size Minimum sample pressure Maximum sample pressure Maximum sample temperature Materials in contact with sample 5 to 100 ml/min (depending on application) 0.1 μm with gaseous samples 35 kpa (5 psig) standard 200 kpa (29 psig) standard 80 C (176 F) standard; higher temperature as option Stainless steel, aluminum, Viton, polyimide and Teflon Brochure, May 2018, A5E Rev04 ECO# DP5A

18 Modular Oven 18 Brochure, May 2018, A5E Rev04 ECO# DP5A

19 Ovens 5 Table 5-1 Oven Characteristics Oven Temperature Range (application dependent) Temperature Control Oven Type Airless* Airbath* Airbath PTCG* Modular ± 0.02 C (± 0.05 F) Temperature Range (dependent on T-rating) 50 to 260 C (122 to 535 F) 5 to 225 C (40 to 440 F) 5 to 330ºC (40 to 625 F) 60 to 80 C (140 to 176 F) * Note: 10 C (18 F) differential above ambient is required for control in all cases unless equipped with a vortex tube. Table 5-2 Approximate Internal Dimensions Oven Type Width Height Depth Air Bath 580mm (22 13 / 16 ") 378mm (14 7 / 8 ") 267mm (10 1 / 2 ") Airless 226mm (8 7 / 8 ") 346mm (13 5 / 8 ") 257mm (10 1 / 8 ") Table 5-3 Power supply options: 100 to 130 VAC 48 to 63 Hz 195 to 260 VAC 48 to 63 Hz 24 VDC (Modular oven system only) Table 5-4 Approximate oven electrical characteristics (application and ambient temperature dependent): Oven configuration Power (W) External fuse Heat-up Operation 230 VAC 115 VAC 24 VDC Airless single oven A 16 A N/A Airless dual oven A 16 A Airbath single oven 650 or A 16 A Airbath dual oven A 2x 16 A Airbath PTGC A 2x 16 A Modular oven system (24 VDC) Two small ovens A 6 A 20 A Two large ovens Brochure, May 2018, A5E Rev04 ECO# DP5A

20 Ovens 20 Brochure, May 2018, A5E Rev04 ECO# DP5A

21 Detectors and Associated Devices 6 The detector specifications given in this section depend on the specific application in which they are installed, and reflect the performance of the component when used in a Maxum II Gas Chromatograph as a system. Table 6-1 Thermal Conductivity Detector (TCD) Parameter Target Components Measurement Type Value All Concentration Smallest Measuring Range (at 60 C oven temperature) 0 to 20 ppm ±5% Typical Measuring Range (at 60 C oven temperature) Dynamic Range 10 5 Linear Range 10 4 Selectivity 0 to 500 ppm ±2% FS up to 0 to 100% ±0.5% FS None Temperature Range (Thermistor bead detector inside oven compartment) 5 to 120 C Temperature Range (Filament detector inside oven compartment) 5 to 180 C Table 6-2 Flame Ionization Detector (FID) Parameter Target Components Measurement Type Value Carbon Mass Smallest Measuring Range (at 60 C oven temperature) 0 to 1 ppm ±3% Typical Measuring Range (at 60 C oven temperature) Dynamic Range 10 7 Linear Range 10 6 Selectivity 0 to 100 ppm ±1% FS up to 0 to 100% ±0.5% FS Combustible Components Temperature Range 105 to 260 C Table 6-3 Air Treater Dimensions Approximately 210 x 210 x 300 mm (8 1 / 4 " x 8 1 / 4 " x 11 3 / 4 ") (w x d x h) Weight Power requirements Installation Construction A minimum of 400 mm (15 3 / 4 ") total clearance is required in depth for removal of the bottom cover 10.5 kg (23 pounds) 115 or 230 VAC, 50 watts Panel, rack, or wall mounted near the analyzer 300 Series Stainless Steel in contact with the treated air. Mounted in an explosion proof aluminum enclosure Brochure, May 2018, A5E Rev04 ECO# DP5A

22 Detectors and Associated Devices Input air quality Meet or exceed ISO (Class 3) requirements. Maximum total hydrocarbon content less than 1 ppm and Dew point -20 C (-4 F) Input air flow 250 to 1500 ml/min (depending on requirements) Input pressure Warm-up time Treated air purity Catalyst life 34 to 1034 kpa (5 to 150 psig), depending on flow rate desired Approximately 90 minutes Up to 95% of the trace hydrocarbons typically found in instrument quality air are removed by the air treater Catalyst is not consumed as part of the air treatment so the life is indefinite. However the catalyst can be poisoned when exposed to sulfur compounds. Safety CSA certified for use in Class I, Division 1, Groups B, C, D Hazardous Locations for US and Canada ATEX certified for use in Zone 1 or 2, gas group IIB + H2 explosive atmosphere (II 2 G) (Ex d IIB+H2 T5 Gb) Temperature Class Rating: T5 Table 6-4 Methanator Parameter Value Non-Ex Methanator Ex Methanator Classification n/a Ex d IIB+H2 Maximum Operation Temperature 400 C 400 C Heater 115 or 230 VAC 115 or 230 VAC Gas Supply H 2, ml/minute H 2, ml/minute Ambient operating temperature for Methanator-equipped Maxum II 0-50 C Table 6-5 Flame Photometric Detector (FPD) Parameter Target Components Measurement Type Value Sulfur Mass Smallest Measuring Range (at 60 C oven temperature) 0 to 1 ppm ±5% Typical Measuring Range (at 60 C oven temperature) Dynamic Range 10 2 Linear Range 0 to 10 ppm ±3% FS up to 0 to 500 ppm ±2% FS 70 (70:1) linearized Selectivity 10 4 to 1 Sulfur to Carbon Temperature Range 105 to 150 C Ignition type Electrical Data Glow Plug 2V at 3A (Maximum, only for flame ignition) 22 Brochure, May 2018, A5E Rev04 ECO# DP5A

23 Detectors and Associated Devices Table 6-6 Pulse Discharge Detector, Helium Ionization Mode Parameter Target Components Measurement Type Value All Mass Smallest Measuring Range (at 60 C oven temperature) 0 to 2 ppm ±5% Typical Measuring Range (at 60 C oven temperature) Dynamic Range Linear Range Selectivity 0 to 5 ppm ±5% FS 10 3 at fixed attenuation 10 3 at fixed attenuation None without He and Ne Temperature Range C (higher temperature ranges on request; system configuration dependent) Table 6-7 Pulse Discharge Detector, Electron Capture Mode Parameter Target Components Measurement Type Value Components with electron affinity Mass Smallest Measuring Range (at 60 C oven temperature) 0 to 2 ppm ±5% Typical Measuring Range (at 60 C oven temperature) Dynamic Range Linear Range 0 to 5 ppm ±5% FS 10 3 at fixed attenuation 10 3 at fixed attenuation Selectivity Components with electron affinity to carbon 10 3 Temperature Range C (higher temperature ranges on request; system configuration dependent) to 1 Table 6-8 Pulse Discharge Detector, Photoionization Mode Parameter Target Components Measurement Type Value Photon sensitive components Mass Smallest Measuring Range (at 60 C oven temperature) 0 to 2 ppm ±5% Typical Measuring Range (at 60 C oven temperature) Dynamic Range Linear Range Selectivity 0 to 5 ppm ±5% FS 10 3 at fixed attenuation 10 3 at fixed attenuation Photon sensitive components (example: benzene to hexane 10 3 to 1) Temperature Range C (higher temperature ranges on request; system configuration dependent) Brochure, May 2018, A5E Rev04 ECO# DP5A

24 Detectors and Associated Devices 24 Brochure, May 2018, A5E Rev04 ECO# DP5A

25 Valve Specifications 7 Table 7-1 Gas sample inlet conditions Sample flow Sample filter size Minimum sample pressure Maximum sample pressure Maximum sample temperature Materials in contact with sample 5 to 100 ml/min (depending on application) 0.1 to 5 μm with gaseous samples (depending on type of valve) 35 kpa (5 psig) standard 200 kpa (29 psig) standard, higher pressure as option 121 C (250 F) standard; higher temperature as option Stainless steel and Teflon; other materials as option 7.1 Model 50 Valve Specifications Table 7-2 Configuration Valve Type Number of Ports 10 Double-acting, pneumatically operated Flow Paths On state: flow between ports 1 & 10, 2 & 3, 4 & 5, 8 & 9 Off state: flow between ports 1 & 2, 3 & 4, 5 & 6, 7 & 8, 9 & 10 Note: flow between ports 6 & 7 is always blocked Table 7-3 Performance and Requirements Sample Types Actuation Gas Switching Time Sample Filtration Maximum Actuation Pressure Minimum Actuation Pressure Maximum Port Pressure (Carrier or Sample) Minimum Port Pressure (Carrier or Sample) Pressure Drop Maximum Temperature Vapor samples only, free of particulates Inert gas, particulate free 20 ms (Typical in Maxum gas chromatographs.) In other uses, actual switching time is dependent on the type of solenoids used to deliver the pneumatic signal to the valve and the size of the pneumatic tubing to the valve. 5 micron 690 kpa (100 psig) kpa (20-25 psig) higher than maximum carrier gas or sample gas pressure 515 kpa (75 psig); contact factory for higher pressure options 35 kpa (5 psi) < 35 kpa (5 psi) for 200 scc/min (air) Pressure drop was measured in air at room temperature with flow from port to port. Actual pressure drop will vary with temperature and gas type. Pressure drop through the sample loop is dependent on the inside diameter and length of the sample loop. 120 C (248 F); contact factory for higher temperature options Brochure, May 2018, A5E Rev04 ECO# DP5A

26 Valve Specifications 7.2 Model 20 Valve Specifications Carrier Gas Flow Mean Time Between Failures 0.3 ml/min to 40 ml/min; contact factory for higher flow options >10 7 cycles at 60 C (140 F); > cycles at 150 C (300 F). Valve failure is typically caused by particulates preventing the diaphragms from sealing against the center plate or long term wear resulting in deformation of the diaphragms. Table 7-4 Dimensions Mounting Actuation & Sample Connections 2 clearance holes for mounting screws (mounting brackets available as separate spare part if desired) 1.6 mm ( 1 / 16 ") OD tubing with Valco or Swagelok fittings Dimensions Height: 33 mm (1 5 / 16 ") Body Diameter: 38 mm (1 1 / 2 ") Outside Diameter: 50 mm (2") Weight Materials of Construction 0.25 kg (0.5 lb) Body: 316 stainless steel Diaphragms: Teflon coated stainless steel See also Maxum II Common Specifications (Page 7) 7.2 Model 20 Valve Specifications Internal loop sample size: External loop sample size: Sample filter: Maximum operating temperature: Maximum sample pressure: Minimum sample pressure: Maximum leak rate between ports: Material in contact with sample: Connection size and type: Actuating air: Total switching time: Body size: Mounting: Other: 2 μl standard. (Other sizes are available on special request.) 170 μl standard. (Other sizes are available on special request.) 5 μm recommended (not furnished with valve). 122 C (250 F) standard 1380 kpa (200 psi) gage instrument air standard kpa (1500 psi) gage with kpa (80psi) gage air signals. Higher operating pressure available on special request kpa (5 psig) Less than 1 μl per minute between ports. 316 stainless steel and Teflon, standard. Other materials are available on special request. 1.6 mm ( 1 / 16 ") O. D. tubing, with Swagelok fittings 345 kpa to 550 kpa (50 to 80 psig) instrument air standard. 550 kpa (80 psig) maximum. Helium or nitrogen may be substituted for air. 150 ms (total time from initiation of command signal to completion of change in valve state) 70 mm (2 3 / 4 ") diameter by 70 mm (2 3 / 4 ") height Clamp type A carrier purge (helium, hydrogen, or nitrogen) may be used (an external lowpressure gas supply is required). 26 Brochure, May 2018, A5E Rev04 ECO# DP5A

27 Valve Specifications 7.4 Model 11 Valve Specifications 7.3 Model 20 High Temperature Valve Specifications Internal loop sample size: External loop sample size: Sample filter: Maximum operating temperature: Maximum leak rate between ports: Material in contact with sample: Connection size and type: Actuating air: Total switching time: Body size: Mounting: Other: 2 μl standard. (Other sizes are available on special request.) 170 μl standard. (Other sizes are available on special request.) 5 μm recommended (not furnished with valve). 150 C (300 F) at 3450 kpa (500 psig) maximum standard 234 C (450 F) at 690 kpa (100 psig) maximum for special applications Less than 1 μl per minute between ports. 316 stainless steel. Other materials are available on special request. 1.6 mm ( 1 / 16 ") O. D. tubing, with Swagelok fittings 345 kpa (50 psig) instrument air standard. 550 kpa (80 psig) required for operating pressure above 1380 kpa (200 psig). Helium or nitrogen may be substituted for air. 150 ms (total time from initiation of command signal to completion of change in valve state) 70 mm (2 3 / 4 ") diameter by 70 mm (2 3 / 4 ") height Clamp type A helium, hydrogen, or nitrogen purge may be used (an external supply of low pressure helium is required). 7.4 Model 11 Valve Specifications Internal loop sample size: External loop sample size: Sample filter: Cap screw (33) Torque Setting: Base Screw (12) Torque Setting: Maximum operating temperature: 0.5, 10, 20 μl standard. Other sizes on special request. 15 μl and larger. 170 μl is standard. 5 μm recommended (not furnished with valve). 3.95±0.11 Nm (35±1 inch-pounds) 0.73±0.11 Nm (6.5±1 inch-pounds) 122 C (250 F) standard 66 C (150 F) Maximum sample pressure: Up to 2068 kpa (300 psig). Up to 414 kpa (60 psig) Minimum sample pressure before it is necessary to apply vacuum assistance to lower chamber: Maximum leak rate between ports: Material in contact with sample: Connection size and type: Actuating air: (Lower port on manifold) Lower Seal Disc Purge Gas: (Upper 2 ports on the manifold) Total switching time: 34.5 kpa (5 psig) Less than 1 μl per minute 316 stainless steel and TFE, standard. Monel and Teflon, or Hastelloy and Teflon available on request. PFA available on request. 1.6 mm ( 1 / 16 ") O. D. tubing, with Swagelok fittings Max. 345 kpa (50 psig) instrument air standard. Helium or nitrogen may be substituted for air. 20 ml (at standard temperature and pressure) of actuating air required for each valve operation. 5 cc/min of (typically) same gas as carrier 150 ms (total time from initiation of command signal to completion of change in valve state) Brochure, May 2018, A5E Rev04 ECO# DP5A

28 Valve Specifications 7.6 Siemens Liquid Injection Valve Body size: Mounting: 57.2 mm (2 1 / 4 ") diameter by 76.2 mm (3") height Clamp type 7.5 Model 11 Low Dead Volume Valve (LDV) Specifications Internal loop sample size: External loop sample size: Sample filter: Cap screw (33) Torque Setting: Base Screw (12) Torque Setting: Maximum operating temperature: 2 and 5 μl standard. Other sizes on special request. 15 μl and larger. 170 μl is standard. 5 μm recommended (not furnished with valve). 3.95±0.11 Nm (35±1 inch-pounds) 0.73±0.11 Nm (6.5±1 inch-pounds) 122 C (250 F) standard 66 C (150 F) Maximum sample pressure: Up to 2068 kpa (300 psig). Up to 414 kpa (60 psig) Minimum sample pressure before it is necessary to apply vacuum assistance to lower chamber: Maximum leak rate between ports: Construction material in contact with sample: Connection size and type: Actuating air: (Lower port on manifold) Lower Seal Disc Purge Gas: (Upper 2 ports on the manifold) Total switching time: Body size: Mounting: 34.5 kpa (5 psig) Less than 1 μl per minute 316 stainless steel and Teflon, standard. Monel and Teflon, or Hastelloy and Teflon available on request. 1.6 mm ( 1 / 16 ") O. D. tubing, with Swagelok fittings Max. 345 kpa (50 psig) instrument air standard. Helium or nitrogen may be substituted for air. 20 ml (at standard temperature and pressure) of actuating air required for each valve operation. 5 cc/min of carrier (normally helium) 150 ms (total time from initiation of command signal to completion of change in valve state) 57.2 mm (2.25") diameter by 76.2 mm (3") height Clamp type 7.6 Siemens Liquid Injection Valve Table 7-5 Configuration Valve Type Vaporization System Pneumatically operated piston actuating a moving liquid-injection tappet Temperature-controlled vaporization system Table 7-6 Siemens Liquid Injection Valve Vaporization temperature Injection volume Sample temperature Material in Contact with Sample 60 to 350 C (140 to 662 F) depending on application and temperature class 0.1 to 9.5 μl -20 to +150 C (-4 to 302 F) Stainless steel, mat. no , Hastelloy, Monel, Rulon, Teflon or special materials 28 Brochure, May 2018, A5E Rev04 ECO# DP5A

29 Valve Specifications 7.7 Valco A4 C6UWE Valve Specifications Control pressure Sample pressure Connections for pipe 400 to 600 kpa (58 to 87 psig) Max kpa (870 psig), recommended 50 to 100 kpa (7.25 to 14.5 psig) 3.14 mm ( 1 / 8 ") outer diameter Table 7-7 Liquid sample inlet conditions Sample Flow Sample Filtration Minimum Sample Pressure Maximum Sample Pressure Maximum Sample Temperature 5-20 cc/min (application dependent) micron (sample valve dependent) 35 kpa (5 psig), lower pressure optional 2070 kpa (300 psig) standard; higher pressure optional 121 C (250 F) standard; higher temperature optional 7.7 Valco A4 C6UWE Valve Specifications Many of the parameters for these valves are application dependent. See the custom documentation package for your analyzer and obtain the applicable specifications for your specific application at the Valco Instruments Co. Inc. web site, Maximum operating temperature (valve body only): Connection size and type: Actuating air: 225 C (437 F) 1.6 mm ( 1 / 16 ") O. D. tubing, with Valco fittings kpa (50 psig) instrument air standard. Brochure, May 2018, A5E Rev04 ECO# DP5A

30 Valve Specifications 7.7 Valco A4 C6UWE Valve Specifications 30 Brochure, May 2018, A5E Rev04 ECO# DP5A

31 Network Access Unit 8 Table 8-1 Dimensions Mounting Options Rack-mount case Wall-mount case Weight 15 kg (33 lbs.) Figure 8-1 Rack Mount Cabinet Table 8-2 Rack Mount Cabinet Dimensions Label Description Metric mm U.S. inches A Rack Height B Rack Total Width C Rack Mounting Holes Spacing D Rack Depth Case Only E Rack Handle F Rack Depth with Handles G Case Width Brochure, May 2018, A5E Rev04 ECO# DP5A

32 Network Access Unit Figure 8-2 Wall Mount Cabinet Table 8-3 Wall Mount Cabinet Dimensions Label Description Metric mm U.S. inches A Wall Width B Wall Mount Holes Horizontal Spacing C Wall Mount Holes Vertical Spacing D Wall Height Including Cable Housing E Wall Height w/o Cable Housing F Wall Mount Total Depth G Wall Mount Depth Case Only Table 8-4 Enclosure Protection Explosion protection Standard configurations: Suitable for use in non-hazardous areas and with non-dangerous conditions Certified according to CSA C/US for use in Class 1, Div. 2, Groups A, B, C, D. EMI/RFI design CE-compatible; in conformity with 2014/30/EU (EMC directive) CE-compatible; in conformity with 2014/35/EU (low-voltage directive) Tested according to EN / IEC Table 8-5 Electrical characteristics Power supply Single-phase AC, V or V (selectable), Hz 300 W G fuse element per IEC 127-2, 4A rating, slow-blow Power wiring must conform to local installation codes and requirements. If conformance to CE certified installation requirements is required, power cable must be shielded or installed in conduit. 32 Brochure, May 2018, A5E Rev04 ECO# DP5A

33 Network Access Unit Table 8-6 Electrical inputs and outputs Standard input and output 2 analog outputs Card slots for optional inputs and outputs via internal I 2 C bus 4 digital outputs (1 for output of system faults, 3 are user-configurable) 4 digital inputs; 7 Input and output cards I2C_AIO 8: 8 analog outputs, 8 analog inputs, 2 digital inputs I2C_DIO: 6 digital inputs and 8 digital outputs I2C_ADIO: 4 digital inputs and 4 digital outputs, 4 analog inputs and 4 analog outputs Digital inputs Optically coupled with a common for all inputs. Digital outputs Analog inputs Analog outputs Self-powered floating-contact input, or configurable for sinking or sourcing current. Sourcing current mode: 24V internal isolated supply, with positive terminal of supply at common. Sinking current mode: 5V internal isolated supply, with negative terminal of supply at common. Floating double-throw contacts, maximum contact load rating 1A at 30V (AC or DC). External diode shunt suppression should be used for inductive DC loads, preferably at the load -20 to +20mA into 50Ω or -10 to +10V R in = 0.1MΩ, alternate insulation up to 10V 0/4 to 20 ma into max. 750 Ω, common negative pole, electrically isolated from ground; freely connectable to ground Termination SYSCON-based I/O: Terminal strip for braided or solid cable with maximum section of 16AWG (1.5mm 2 ) Expansion board-based I/O: Spring contacts for shielded or solid cable with a maximum area of 18AWG or 0.82 mm 2 Table 8-7 Communication Serial ports 4 RS232/RS485 ports, e.g. Modbus Ethernet Standard 10/100 BaseT Ethernet with 4 RJ45 connectors e.g. Modbus TCP IP or OPC Optional ESBF board Fiber-optic 100Base FX multimode with ST connection 3 x RJ45 and 1 x optical (Optical port uses LED instead of laser for safer diffusedenergy fiber link; less than 40μW at approximately 1300nm) Brochure, May 2018, A5E Rev04 ECO# DP5A

34 Network Access Unit 34 Brochure, May 2018, A5E Rev04 ECO# DP5A

35 Appendix - Change Log A A.1 January 2018 Changes 1. Added change-log appendix. 2. Combined Gas Supply and Typical Gas Consumption tables to create Gas Requirements (Page 8) table. This table includes EPC inlet limits and other new parameters. 3. Added note about the effect of externally-mounted options in analyzer dimension descriptions. 4. Removed mention of "Sliding-plate valves" from Airbath or Airless Oven model Configuration table (Page 12). 5. Moved power consumption items to Ovens section (Page 19). 6. Added statement about light-source energy limits to Communication tables, ESBF descriptions in the Airbath or Airless (Page 13), Modular Oven (Page 17), and the NAU (Page 33) sections. 7. Moved Sample Inlet Conditions table to Valves section (Page 25). 8. Added section for Electronic Pressure Controller (EPC) (Page 7). 9. Added statement, "Certified according to IECEx with air or nitrogen purging for Zone 1 (IIC T4 Gb)" to Modular Oven Enclosure Protection section (Page 16). 10.Added oven approximate internal dimensions (Page 19). 11.Added information on fuse values and warmup power consumption to Ovens section (Page 19) 12.Added Minimum Actuation Pressure parameter for Model 50 valves (Page 25). 13.Added Methanator specifications (Page 22). 14.Air Treater specifications (Page 21) moved to be near FID specifications. 15.Added Ignition Type and Electrical Data to FPD specifications (Page 22). 16.Added note for example Valco valve (Page 29). See also Airbath or Airless Oven (Page 11) Modular Oven (Page 15) Network Access Unit (Page 31) Modular Oven (Page 15) Detectors and Associated Devices (Page 21) Detectors and Associated Devices (Page 21) Brochure, May 2018, A5E Rev04 ECO# DP5A

36 Appendix - Change Log A.1 January 2018 Changes Maxum II Common Specifications (Page 7) Airbath or Airless Oven (Page 11) Airbath or Airless Oven (Page 11) Valve Specifications (Page 25) Model 50 Valve Specifications (Page 25) 36 Brochure, May 2018, A5E Rev04 ECO# DP5A