Asphalt Binder Quality Test (ABQT)

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1 Asphalt Binder Quality Test (ABQT) Binder Expert Task Group September, 2017 Infrastructure Materials Team, TFHRC 1

2 Why develop a Quality control Test for Asphalt Binder? - Refresher Need a portable, quick and easy test method for day-to-day QA of production asphalt binder during a pavement construction project UTAH DOT Several methods have been tried without success! UTAH DOT Dynamic Shear Rheometer quick version Melt Indexer A single test method that can take you from mix-design to production

3 Asphalt Binder Quality Tester

4 Schematic of NOZZLE with Air Jet & Laser

5 Test Results for Gel and Sol Type Asphalts AAD AAG Deflection, mm Recovery = 29% Deflection, mm Recovery = 3.2% Time, s -0.2 Time, s

6 Quality Control

7 repeatability of qc data Binder ID Number of QCT Max. Deflection, mm QCT % Recovery Binder Type Replicates Average Std. Dev COV % Average Std. Dev COV % 200/300 Pen #1 PG PG UnModified PG #2 PG PG PMA PG PG Crumb #1 PG Rubber #2 PG Modified #3 PG Pooled Average 3 3

8 ABQT Verfication Kit

9 Quality Assurance

10 Prediction of Continuous PG Grades AASHTO M320 Continuous PG grades are predicted using creep recovery data on unaged binder Standard test protocol A proprietary Algorithm was developed to predict continuous PG grades Based on models that use artificial neural network learning algorithms Training database of more than 500 asphalt binders Different crude sources including Europe Greater than 95% accuracy of prediction of PG grades Accuracy will be better as more data gets added Models are tailored to variation in PG specification For example: Utah dot MSCR grades can also be predicted AASHTO M332

11 -16.0 All Binders Low PG Predicted Low PG, o C Measured Low PG, o C

12 88.0 All Binders High PG (G*/sin δ = 1.0 kpa) All Binders High PG (G*/sin δ = 1.0 kpa) Predicted High PG, o C Predicted High PG, o C Measured High PG, o C Measured High PG, o C

13 76 UDOT (1.3kPa) High PG Temp Predicted High Temperature Continuous PG y = x R² = Measured High Temperature Continuous PG

14 Predicted Low Temperature Continuous PG UDOT (1.3kPa) Low PG Temp y = x R² = Measured Low Temperature Continuous PG

15 Validation of model Effect of database size

16 82 AMRL_Post_Trng AMRL_B4_Trng WCTG_Post_rng WCTG_B4_Trng OCTG_B4_Trng OCTG_Post_Trng Predicted High PG, o C Measured High PG, o C

17 ABQT STATE AGENCY VALIDATION DATA

18 Continuous High PG Grade 82 IDAHO_B4_Trng IDAHO_After_Trng CDOT_B4_Trng CDOT_After_Trng Predicted Grade by ANN Model, o C Measured Grade, o C

19 Continuous Low PG Grade -22 IDAHO_B4_Trng IDAHO_Asphalt_Trng CDOT_B4_Trng CDOT_After_Trng Predicted Grade by ANN Model, o C Measured Grade, o C

20 Predicted High PG Continuous Grade, o C Continuous High PG Grade PennDOT_B4_Trng PennDOT_After_Trng Measured High PG Continuous Grade, o C

21 -22 Continuous Low PG Grade PennDOT_B4_Trng PennDOT_After_Trng Predicted Low PG Continuous Grade, o C Measured Low PG Continuous Grade, o C

22 Potential Applications Quick Screening of Binders Identify Presence of Contaminants Monitor Addition of Additives/asphalt blending Relationship to MSCR Monitor Binder During Paving UTAH DOT 2015 Season Characterize Crumb Rubber Modified Binders High crumb rubber content Granite binders FHWA Terminal blend binders

23 Summary and future Developed quick easy to use QC/QA test that measures loading and recovery characteristics of Binders (and mixes) PREDICTS Continuous PG Grade Accurately (95% Accuracy) Predicts MSCR Grades Asphalt Binder QUALITY Test is ready for use

24 Delta Tc Range and Magnitude Binder Expert Task Group September, 2017 Infrastructure Materials Team, TFHRC

25 SHRP Premise Background No lower limit to S(60s) value 0 to 300 MPa allowed A minimum of m-value is required as long as S is lower than or equal to 300 Mpa Delta Tc = Tc (S =300) Tc (m = 0.3) was not considered Delta Tc = Positive indicates S controlled binders Delta Tc = Negative indicates m controlled binders

26 FHWA s Approach at TFHRC Collect State DOT Low Temperature BBR Validation Data Calculate Delta Tc using Data Mining Techniques Consider performance relation where available Make Recommendations Perhaps an acceptable Delta Tc OR Specify S where m-value is 0.3

27 FHWA s Approach at TFHRC Calculate Delta Tc using Data Mining Techniques Challenge State validation data contains BBR info. at only one temperature! To calculate Delta Tc Need BBR S and m-value data at two temperatures! Approach Determine prediction algorithms to calculate Delta Tc. Delta Tc Prediction from single point BBR data Average of all PG specific changes in S and m-value ANN approach

28 Predicted Delta Tcr (Method 2), o C Method 2 Validation (177 samples) Idaho Binders CDOT Penn DOT AMRL WCTG OCTG Other m-value CONTROL S CONTROL Measured Delta Tcr, o C

29 Prediction Error in Delta Tcr (Method 2), o C Method 2 Validation (177 Samples) Idaho Binders CDOT Penn DOT AMRL WCTG OCTG Other S CONTROL m-value CONTROL Measured Delta Tcr, o C

30 Oklahoma PG 64-22OK PG 70-28OK PG 76-28OK 10 5 Delta Tc, degrees C Negative Vaues indicate m-controlled Lower Grade 6-Oct-03 2-Jul Mar Dec Sep Jun-17 Date

31 15.0 DELAWARE DOT - PG Delta Tc, o C

32 8.0 DELAWARE DOT - PG Delta Tc, o C

33 15.0 DELAWARE DOT - PG Delta Tc, o C

34 Delta T cr Frequency, -5 C > +5 C Total Samples < -5 C = 4613 Total Samples > +5 C = PG PG PG PG PG PG PG PG PG OK PG 64-22E PG PG PG 64E-28 PG PG PG PG OK PG PG PG PG OK PG 82-22

35 12000 Delta T cr Frequency, -5 o C to +5 o C Total Samples -5 C to +5 C = 68, PG PG PG PG PG PG PG PG PG OK PG 64-22E PG PG PG 64E-28 PG PG PG PG OK PG PG PG PG OK PG 82-22

36 Number of Delta Tc, degrees C Delta T cr Frequency PG Grade Sample Size States Median Minimum Maximum < -5 o C -5 to +5 o C > +5 o C 3 PG PG PG PG PG PG PG PG PG OK PG 64-22E PG PG PG 64E PG PG PG PG OK PG PG PG PG OK PG Totals Percentages All Participating States

37 State ID PG Grade Median Minimum Maximum < -5 o C -5 to +5 o C > -5 o C OK PG OK PG OK OK PG OK OK PG OK Totals Percentages Sample Size OKLOHOMA Delta Tc, degrees C Delta T cr Frequency

38 State ID PG Grade Median Minimum Maximum < -5 o C -5 to +5 o C > -5 o C UT PG UT PG UT PG UT PG UT PG UT PG Totals Percentages Sample Size UTAH Delta Tc, degrees C Delta T cr Frequency

39 State ID DELAWARE Delta Tc, degrees C Delta T cr Frequency PG Grade Median Minimum Maximum < -5 o C -5 to +5 o C > -5 o C DE PG DE PG 64-22E DE PG DE PG DE PG DE PG Totals Percentages Sample Size

40 Predicted Delta Tcr (ANN), o C m-value CONTROL ANN Validation (542 Samples) S CONTROL Measured Delta Tcr, o C

41 Predicted Delta Tcr (ANN), o C Predicted Delta Tcr (ANN), o C ANN Validation (116 Samples) ANN Validation (542 Samples) S CONTROL S CONTROL m-value CONTROL m-value CONTROL Measured Delta Tcr, o C

42 Findings to date Delta Tc may be predicted using simple rules based on PG Averages Error in prediction is within +/- 2 degrees C for most grades and binders ANN can reduce this to within +/- 1 degree C Data mining effort Delta Tc range for over 92% of binders is + 5C There are a considerable number outside this range that should show performance differences Suggests that acceptable Delta Tcs might be related to climatic conditions

43 ΔTc and CTOD variation for the ALF binders Binder Expert Task Group September, 2017 Pavement Materials Team, TFHRC 50

44 ALF Binder Properties Lane Binder PG V Content, level REOB Content, % Delta Tc 1 and A C B C A A D

45 25 Delta (T) (degrees Celsius) and CTOD (millimeters) variation - binder recovered from ALF lanes at 0, 2 and 3-years H2O foam Evotherm H2O foam Evotherm Evotherm Control (64-22) 40%RAP (58-28) 20%RAS (64-22) 20%RAP (64-22) 40%RAP (64-22) 20%RAP (64-22) 20%RAS (58-28) 40%RAP (58-28) 20%RAP (64-22) 40%RAP (58-28) 40%RAP (58-28) Lane 1 recovered Lane 2 recovered Lane 3 recovered Lane 4 recovered Lane 5 recovered Lane 6 recovered Lane 7 recovered Lane 8 recovered Lane 9 recovered Lane 10 recovered Lane 11 recovered Delta T at 0-years Delta T at 2-years Delta T at 3-years CTOD at 0-years CTOD at 2-years CTOD at 3-years 52

46 Final Thoughts Advantages of ANN based prediction software As States begin implementation, each year ANN software gets smarter States can further refine by adding supplier info, performance, etc. Need feedback from States regarding problem binders 53

47 BBR T critical Spread: PG (S)tiffness PG (m)-creep Exploratory Blends Final Blends Holly BP Base +PG REOB Source 1 +REOB Source 2 +REOB Source 3 PAV 2 X PAV PAV 2 X PAV -2.0 o C o C o C o C o C 0% / 20% o C 0% / 30% o C 20% / 20% o C 25% / 30% o C 10% o C 20% / 20% o C 10% o C 15% / 20% o C 15% / 0% o C 2.5% o C 6% o C 15% / 20% o C 15% / 0% o C 2.5% o C 6%

48

49 WRI/ARC Field Validation Sitesupdate Five sites remain: AZ (2), MN, MB (2) Pecking order for AZ sections maintained

50 Thank You. Questions? 63

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